Oilseed residues. Determination of oil content

1999 ◽  
Keyword(s):  
Oil Content ◽  
Residues Determination

Development of a New Method for Determination of the Oil Content from Microalgae Lipid Fraction

2017 ◽  
Vol 68 (4) ◽  
pp. 671-674
Author(s):  
Ana Maria Galan ◽  
Ioan Calinescu ◽  
Elena Radu ◽  
Elena Emilia Oprescu ◽  
Gabriel Vasilievici ◽  
...  
Keyword(s):  
Sunflower Oil ◽  
Oil Content ◽  
Lipid Fraction ◽  
New Method ◽  
Ms Analysis ◽  
Qualitative Determination ◽  
Tga Analysis

The purpose of this study was to develop a method for rapid quantitative and qualitative determination of the oil from microalgae lipid fraction obtained from Nannochloris sp biomass. The lipid fraction was first refluxed with 4% KOH in MeOH (60, 90, 120 min), followed by reaction with 20% BF3 in MeOH, using different times of reflux (90,120, 150 min) for each time of reflux with 4% KOH in MeOH. The FAME samples were analyzed by GC-MS analysis. 120 min reflux with 4% KOH in MeOH, 90 min with 20% BF3 in MeOH and a ratio lipid fraction: 4% KOH in MeOH: 20% BF3 in MeOH=1:20:27, were required to obtain the higher percent of oil in the microalgae lipid fraction. The relevance of the method developed was proved by TGA analysis and by transesterification of a sunflower oil sample in the same conditions.

Oil content of cotton seed in Northern Nigeria: 1. Assessment of nuclear magnetic resonance for the determination of the oil percentage of cotton seed

1977 ◽  
Vol 88 (3) ◽  
pp. 727-729 ◽  
Author(s):  
J. B. Smithson ◽  
H. E. Gridley
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Cotton Seed ◽  
Oil Content ◽  
Northern Nigeria ◽  
Local Varieties ◽  
Oil Percentage ◽  
Conventional Solvent Extraction ◽  
Nuclear Magnetic

SUMMARYThe oil content of a number of introduced and local varieties was determined using three nuclear magnetic resonance oil analysers at different centres and compared with results from conventional solvent extraction. Differences were evident between the three centres and between the techniques but in both cases the rankings were similar.

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