scholarly journals Towards Generalized Noise-Level Dependent Crystallographic Symmetry Classifications of More or Less Periodic Crystal Patterns

Symmetry ◽  
2018 ◽  
Vol 10 (5) ◽  
pp. 133 ◽  
Author(s):  
Peter Moeck
Keyword(s):  
Noise Level ◽  
Crystallographic Symmetry ◽  
Periodic Crystal

scholarly journals How to assign a (3 + 1)-dimensional superspace group to an incommensurately modulated biological macromolecular crystal

2017 ◽  
Vol 50 (4) ◽  
pp. 1200-1207 ◽  
Author(s):  
Jason Porta ◽  
Jeff Lovelace ◽  
Gloria E. O. Borgstahl
Keyword(s):  
Crystal Structure ◽  
Three Dimensional ◽  
Real Life ◽  
Group Symmetry ◽  
Protein Crystal ◽  
3D Space ◽  
Structure Solution ◽  
Crystallographic Symmetry ◽  
Aperiodic Crystals ◽  
Periodic Crystal

Periodic crystal diffraction is described using a three-dimensional (3D) unit cell and 3D space-group symmetry. Incommensurately modulated crystals are a subset of aperiodic crystals that need four to six dimensions to describe the observed diffraction pattern, and they have characteristic satellite reflections that are offset from the main reflections. These satellites have a non-integral relationship to the primary lattice and requireqvectors for processing. Incommensurately modulated biological macromolecular crystals have been frequently observed but so far have not been solved. The authors of this article have been spearheading an initiative to determine this type of crystal structure. The first step toward structure solution is to collect the diffraction data making sure that the satellite reflections are well separated from the main reflections. Once collected they can be integrated and then scaled with appropriate software. Then the assignment of the superspace group is needed. The most common form of modulation is in only one extra direction and can be described with a (3 + 1)D superspace group. The (3 + 1)D superspace groups for chemical crystallographers are fully described in Volume C ofInternational Tables for Crystallography. This text includes all types of crystallographic symmetry elements found in small-molecule crystals and can be difficult for structural biologists to understand and apply to their crystals. This article provides an explanation for structural biologists that includes only the subset of biological symmetry elements and demonstrates the application to a real-life example of an incommensurately modulated protein crystal.

scholarly journals Towards Generalized Noise-level Dependent Crystallographic Symmetry Classifications of More or Less Periodic Crystal Patterns

2018 ◽  
Author(s):  
Peter Moeck
Keyword(s):  
Noise Level ◽  
Information Criteria ◽  
Geometric Feature ◽  
The Novel ◽  
Symmetry Classes ◽  
Geometric Feature Extraction ◽  
Crystallographic Symmetry ◽  
Real World Applications ◽  
The Common ◽  
2D Images

Geometric Akaike Information Criteria (G-AICs) for generalized noise-level dependent crystallographic symmetry classifications of two-dimensional (2D) images that are more or less periodic in either two or one dimensions as well as Akaike weights for multi-model inferences and predictions are reviewed. Such novel classifications do not refer to a single crystallographic symmetry class exclusively in a qualitative and definitive way. Instead, they are quantitative, spread over a range of crystallographic symmetry classes, and provide opportunities for inferences from all classes (within the range) simultaneously. The novel classifications are based on information theory and depend only on information that has been extracted from the images themselves by means of maximal likelihood approaches so that these classifications are objective. This is in stark contrast to the common practice whereby arbitrarily set thresholds or null hypothesis tests are employed to force crystallographic symmetry classifications into apparently definitive/exclusive states, while the geometric feature extraction results on which they depend are never definitive in the presence of generalized noise, i.e. in all real world applications. Thus, there is unnecessary subjectivity in the currently practiced ways of making crystallographic symmetry classifications, which can be overcome by the approach outlined in this review.

Electron Microscopy in Molecular Biology

1967 ◽  
Vol 25 ◽  
pp. 2-3
Author(s):  
Cecil E. Hall
Keyword(s):  
Electron Microscopy ◽  
Molecular Biology ◽  
Noise Level ◽  
Molecular Structures ◽  
Material Structure ◽  
The Arts ◽  
Shadow Casting ◽  
Electron Image ◽  
High Degree ◽  
Very High

The visualization of organic macromolecules such as proteins, nucleic acids, viruses and virus components has reached its high degree of effectiveness owing to refinements and reliability of instruments and to the invention of methods for enhancing the structure of these materials within the electron image. The latter techniques have been most important because what can be seen depends upon the molecular and atomic character of the object as modified which is rarely evident in the pristine material. Structure may thus be displayed by the arts of positive and negative staining, shadow casting, replication and other techniques. Enhancement of contrast, which delineates bounds of isolated macromolecules has been effected progressively over the years as illustrated in Figs. 1, 2, 3 and 4 by these methods. We now look to the future wondering what other visions are waiting to be seen. The instrument designers will need to exact from the arts of fabrication the performance that theory has prescribed as well as methods for phase and interference contrast with explorations of the potentialities of very high and very low voltages. Chemistry must play an increasingly important part in future progress by providing specific stain molecules of high visibility, substrates of vanishing “noise” level and means for preservation of molecular structures that usually exist in a solvated condition.

Detection of a point defect in a silicon single crystal by high-resolution TEM

1995 ◽  
Vol 53 ◽  
pp. 466-467
Author(s):  
M. Awaji
Keyword(s):  
High Resolution ◽  
Single Crystal ◽  
Point Defect ◽  
Point Defects ◽  
Noise Level ◽  
Dark Field ◽  
Silicon Single Crystal ◽  
High Resolution Image ◽  
Dark Field Imaging ◽  
Field Imaging

It is necessary to improve the resolution, brightness and signal-to-noise ratio(s/n) for the detection and identification of point defects in crystals. In order to observe point defects, multi-beam dark-field imaging is one of the useful methods. Though this method can improve resolution and brightness compared with dark-field imaging by diffuse scattering, the problem of s/n still exists. In order to improve the exposure time due to the low intensity of the dark-field image and the low resolution, we discuss in this paper the bright-field high-resolution image and the corresponding subtracted image with reference to a changing noise level, and examine the possibility for in-situ observation, identification and detection of the movement of a point defect produced in the early stage of damage process by high energy electron bombardment.The high-resolution image contrast of a silicon single crystal in the [10] orientation containing a triple divacancy cluster is calculated using the Cowley-Moodie dynamical theory and for a changing gaussian noise level. This divacancy model was deduced from experimental results obtained by electron spin resonance. The calculation condition was for the lMeV Berkeley ARM operated at 800KeV.

Using crystallographic symmetry in diffraction and contrast analysis

1989 ◽  
Vol 47 ◽  
pp. 504-505
Author(s):  
U. Dahmen ◽  
K.H. Westmacott
Keyword(s):  
Electron Microscopy ◽  
High Symmetry ◽  
Two Phase ◽  
Tem Analysis ◽  
Crystallographic Symmetry ◽  
The Matrix ◽  
Contrast Analysis ◽  
Practical Tool ◽  
Convergent Beam ◽  
Beam Diffraction

Despite the increased use of convergent beam diffraction, symmetry concepts in their more general form are not commonly applied as a practical tool in electron microscopy. Crystal symmetry provides an abundance of information that can be used to facilitate and improve the TEM analysis of crystalline solids. This paper draws attention to some aspects of symmetry that can be put to practical use in the analysis of structures and morphologies of two-phase materials.It has been shown that the symmetry of the matrix that relates different variants of a precipitate can be used to determine the axis of needle- or lath-shaped precipitates or the habit plane of plate-shaped precipitates. By tilting to a special high symmetry orientation of the matrix and by measuring angles between symmetry-related variants of the precipitate it is possible to find their habit from a single micrograph.

Evaluation of the accuracy of reconstruction of the electrophysical and geometric parameters of multilayer dielectric coatings by the multi-frequency radio wave method of a slow surface electromagnetic waves

2020 ◽  
pp. 51-58
Author(s):  
Aleksandr I. Kazmin ◽  
Pavel A. Fedjunin
Keyword(s):  
Radio Wave ◽  
Noise Level ◽  
Electromagnetic Waves ◽  
Dielectric Materials ◽  
Geometric Parameters ◽  
Experimental Investigations ◽  
Wave Method ◽  
Dielectric Coatings ◽  
Surface Electromagnetic Waves ◽  
Multilayer Dielectric

One of the most important diagnostic problems multilayer dielectric materials and coatings is the development of methods for quantitative interpretation of the checkout results their electrophysical and geometric parameters. The results of a study of the potential informativeness of the multi-frequency radio wave method of surface electromagnetic waves during reconstruction of the electrophysical and geometric parameters of multilayer dielectric coatings are presented. The simulation model is presented that makes it possible to evaluate of the accuracy of reconstruction of the electrophysical and geometric parameters of multilayer dielectric coatings. The model takes into account the values of the electrophysical and geometric parameters of the coating, the noise level in the measurement data and the measurement bandwidth. The results of simulation and experimental investigations of reconstruction of the structure of relative permittivitties and thicknesses of single-layer and double-layer dielectric coatings with different thicknesses, with different values of the standard deviation (RMS) of the noise level in the measured attenuation coefficients of the surface slow electromagnetic wave are presented. Coatings based on the following materials were investigated: polymethyl methacrylate, F-4D PTFE, RO3010. The accuracy of reconstruction of the electrophysical parameters of the layers decreases with an increase in the number of evaluated parameters and an increase in the noise level. The accuracy of the estimates of the electrophysical parameters of the layers also decreases with a decrease in their relative permittivity and thickness. The results of experimental studies confirm the adequacy of the developed simulation model. The presented model allows for a specific measuring complex that implements the multi-frequency radio wave method of surface electromagnetic waves, to quantify the potential possibilities for the accuracy of reconstruction of the electrophysical and geometric parameters of multilayer dielectric materials and coatings. Experimental investigations and simulation results of a multilayer dielectric coating demonstrated the theoretical capabilities gained relative error permittivity and thickness of the individual layers with relative error not greater than 10 %, with a measurement bandwidth of 1 GHz and RMS of noise level 0,003–0,004.

AN IMPROVED ARMORED VEHICLE KRAZ “FIONA” NOISE SILENCER

2019 ◽  
pp. 21-26
Author(s):  
Volodymyr Fedorov ◽  
Vasyl’ Yanovsky ◽  
Dmytro Kovalshuk
Keyword(s):  
Noise Reduction ◽  
Speed Of Sound ◽  
Acoustic Waves ◽  
Noise Level ◽  
Combustion Engine ◽  
Environmental Aspect ◽  
Exhaust Gases ◽  
Ecological Requirements ◽  
On The Road ◽  
Armored Vehicle

Ecological requirements for cars grow from year to year, both in the world as a whole, and in Ukraine in particular. This is especially true of noise pollution. Additionally, noise reduction becomes relevant, taking into account the conduct of military operations during the last 5 years on the territory of Ukraine. The war has caused a special need for military vehicles for which masking properties are vital. Noise is a serious disincentive factor. Therefore, its reduction for a military vehicle, apart from the environmental aspect, is of a purely military nature, that is, it is extremely important. The car has many sources of noise there are many ways to deal with them. One of the most powerful source of noise is the sleeping bag. This kind of noise is reduced by means of silencers of noise. The vast majority of silencer data in the basis of its design has a reactive (or resonant) muffler. To calculate the jet silencer you must know the speed of sound in the sleeping bags. In order to increase the acoustic efficiency of reactive and resonant mufflers of exhaust gases noise of the ICE of cars, an experimental method was proposed for determining the speed of sound in the sleighs. Implementation of the method is carried out by measuring the attenuation of acoustic waves. The noise level of the bedrooms is measured without silencer and silencer. Based on the data obtained, the noise reduction performance of the residual is established. From the well-known formula, based on the calculation of the efficiency of the silencing of a jet muffler, a formula is obtained for calculating the speed of sound in the sleeping quays. In this formula, all parameters are known: the level of silencer efficiency, the noise level of the sleeping, the ratio of areas of cross sections of the muffler and the inlet pipe and the length of the muffler. The sound speed thus established can continue to be used not only for engines of the type for which measurements and calculations were made, but also with a certain approximation for some other types of engines. This method provides high accuracy for determining the required parameter. In the given work on the example of the armored car KrAZ “Fiona” the calculation of efficiency increase of the reactive silencer is made due to the above-mentioned method. Also, the projected decrease in the external noise level of the KrAZ Armored Vehicle “Fiona” is considered by determining the speed of sound in the recesses on the trunk cycle on the road with acceleration up to speed of 50 km/h (75 km/h) and the movement with this speed, as well as when driving at a speed of 45 km/h. Keywords: transport, armored car, internal combustion engine, exhaust, exhaust gases, noise, source, acoustic efficiency, acoustic efficiency, speed of sound, jet muffler.

Detection of Narrow-Band Signals with Noise Level Assessment

2008 ◽  
Vol 67 (1) ◽  
pp. 33-39
Author(s):  
S. V. Bukharin ◽  
V. P. Litvinenko ◽  
A. N. Glushkov
Keyword(s):  
Noise Level ◽  
Narrow Band

An Examination of the Effects of Noise Level on Methods to Determine Curvature in Range Images

2019 ◽  
Vol 2019 (10) ◽  
pp. 325-1-325-7
Author(s):  
Jacob D Hauenstein ◽  
Timothy S Newman
Keyword(s):  
Noise Level ◽  
Range Images

The Status of Noise Pollution in the Major Traffic Intersections of Khulna Metropolitan City in Bangladesh and its Possible Effect on Noise-Exposed People

2020 ◽  
Vol 1 (5) ◽  
Author(s):  
Aliza Sultana ◽  
Ashok Kumar Paul ◽  
Meher Un Nessa
Keyword(s):  
Noise Level ◽  
Noise Pollution ◽  
Pressure Level ◽  
Pollution Level ◽  
Metropolitan City ◽  
Mixed Area ◽  
Commercial Area ◽  
Significant Difference ◽  
Traffic Intersections ◽  
The Status

This study was conducted in the Khulna metropolitan city to determine the status of noise pollution at major traffic intersections and assess the possible effect of noise on regular noise afflicted people. For this research, five busiest roadways and traffic intersections; two mixed zone and three commercial zones were selected purposively and 'ST-8850 Sound Level Meter' was used to record the noise pressure level. Average noise pressure level and some noise parameters (Leq, L10, L50, L90, and Lnp) were measured at different shifts in each location both on working days and holidays. The result evidently specified that noise level in all major traffic circles of Khulna metropolitan city was much higher than the recommended threshold of acceptable noise level set by the Department of Environment (DOE) of Bangladesh. It was observed that the mixed area (Sonadanga, Gollamari) tends to have a higher average noise level than those of the commercial area (Shibbari, Notunrasta, Dakbangla). The noise pollution level (Lnp) in mixed areas varied from 92.77 dB (A) to 104.74 dB(A) on working days and 86.9 dB(A) to 105.5 dB(A) on holidays. On working days, the highest Leq was observed 92.65 ± 4.15 dB(A) in Sonadanga (mixed area), whereas the lowest was 85.13 ± 2.83 dB(A) in Dakbangla (commercial area). However, on holidays the highest level of Leq was found 90.41 ± 2.25 dB(A) in Sonadanga, while the lowest levels were 80.43 ± 3.20 dB(A) in Dakbangla. One-way ANOVA with LSD post-hoc test results illustrated that on working days there was a significant difference between the noise pollution levels (NPL) in different shifts of day time (F = 8.412, p < .05). The respondents of the study area addressed that they were the most affected by annoyance (70%), headache (62%), and hearing loss (46%) due to regular exposure to the traffic noise. Therefore, it is recommended to enhance awareness regarding the cause and effect of noise pollution among the noise producers and oppressed people. Subsequently, administrative measures have to take to attenuate noise pollution and indemnify the quality health of the citizens.

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