scholarly journals Preparation of Sodium Lignosulfonate/Chitosan Adsorbent and Application of Pb2+ Treatment in Water

2021 ◽  
Vol 13 (5) ◽  
pp. 2997
Author(s):  
Jie Pan ◽  
Jiangwei Zhu ◽  
Fulong Cheng

Industrial wastewater has brought huge disasters to water resources and soil and has seriously affected the growth of animals and plants. There is an urgent need for a green and efficient adsorbent to solve the problem of water pollution. Sodium lignosulfonate and chitosan undergo free radical polymerization to form a lignin/chitosan adsorbent, which is used to treat Pb2+ in water pollution. An orthogonal experiment was used to optimize the content of sodium lignosulfonate, chitosan, cross-linking agent and initiator to obtain the adsorbent with the best adsorption performance. The adsorbents were characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), thermal analysis and zeta potentiometry. The influence of different conditions on the adsorption of heavy metal ions by lignosulfonate/chitosan adsorbent was explored, and a kinetic and isotherm model was established. The results showed that the adsorption capacity of Pb2+ was 345 mg g−1 when the adsorbent was 0.01 g, the concentration of heavy metal ions was 100 mg L−1 and pH was 7. The adsorption process of lignosulfonate/chitosan is a kind of spontaneous adsorption mode, which is mainly composed of electrostatic adsorption and chemical adsorption.

2020 ◽  
Vol 62 (2) ◽  
pp. 243-250
Author(s):  
A. M. Abd El-Hamid ◽  
M. A. Zahran ◽  
Y. M. Z. Ahmed ◽  
S. M. El-Sheikh

RSC Advances ◽  
2015 ◽  
Vol 5 (129) ◽  
pp. 106905-106911 ◽  
Author(s):  
Zeid A. ALOthman ◽  
Erkan Yilmaz ◽  
Mohamed A. Habila ◽  
Ibrahim H. Alsohaimi ◽  
Abdullah M. Aldawsari ◽  
...  

Triethylenetetramine modified multiwalled carbon nanotubes (TETA-MWCNTs) were prepared and used as an efficient adsorbent for the solid phase extraction of heavy metal ions.


2019 ◽  
Vol 138 ◽  
pp. 188-197 ◽  
Author(s):  
Jianzhe Ma ◽  
Muhammad Asim Khan ◽  
Mingzhu Xia ◽  
Chenlu Fu ◽  
Sidi Zhu ◽  
...  

RSC Advances ◽  
2020 ◽  
Vol 10 (16) ◽  
pp. 9693-9703 ◽  
Author(s):  
W. S. Abo El-Yazeed ◽  
Y. G. Abou El-Reash ◽  
L. A. Elatwy ◽  
Awad I. Ahmed

This work reported the preparation of Mg-MOF, Fe-MOF and Fe–Mg MOF by a solvothermal technique and their characterization with FT-IR, XRD, SEM, EDS, TEM and SBET analyses.


RSC Advances ◽  
2016 ◽  
Vol 6 (18) ◽  
pp. 14778-14791 ◽  
Author(s):  
Habibun Nabi Muhammad Ekramul Mahmud ◽  
A. K. Obidul Huq ◽  
Rosiyah binti Yahya

Water pollution caused by heavy metal ions is becoming a serious threat to human and aquatic lives day by day.


2021 ◽  
Vol 10 (3) ◽  
pp. xx-xx
Author(s):  
Thu Le Dieu ◽  
Hoang Tran Vinh

In this study, heavy metal ions or organic in the aqueous solution are removed by adsorbent without filtration or centrifugation as well as incorporate magnetic materials into the adsorbent. A composite film GO/PVA from PVA and self – synthesized GO by co - precipitation method has synthesized successfully. This composite was characterized by XRD, SEM, FT-IR to evaluate the properties of this material. The results showed that there was an interaction between GO and PVA so we have tested the adsorption capacity of this composite with Co(II) ions and the obtained efficiency of this process was 99.5% with the initial concentration of solution is 20 mg.L-1. This film is completely capable of removing heavy metal ions from waste water.


Chemosphere ◽  
2019 ◽  
Vol 214 ◽  
pp. 738-742 ◽  
Author(s):  
Jinyun Liu ◽  
Yu Chen ◽  
Tianli Han ◽  
Mengying Cheng ◽  
Wen Zhang ◽  
...  

e-Polymers ◽  
2016 ◽  
Vol 16 (4) ◽  
pp. 313-322 ◽  
Author(s):  
Dun Chen ◽  
Tunsagnl Awut ◽  
Bin Liu ◽  
Yali Ma ◽  
Tao Wang ◽  
...  

AbstractFe3O4 nanoparticles (MNP) were coated with 3-aminopropyltriethoxy-silane (APTES), resulting in anchoring of primary amine groups on the surface of the particles, then four kinds of novel magnetic adsorbents (Fe3O4@SiO2-NH-HCGs) were formed by grafting of different heterocyclic groups (HCG) on amino groups via substitution reaction. These Fe3O4@SiO2-NH-HCGs were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and energy disperse spectroscopy (EDS). The results confirmed the formation of Fe3O4@SiO2-NH-HCGs nanoparticles and the Fe3O4 core possessed superparamagnetism. Batch experiments were performed to evaluate adsorption conditions of Cu2+, Hg2+, Pb2+ and Cd2+. Under normal temperature and neutral condition, just 20 min, the removal efficiency of any Fe3O4@SiO2-NH-HCGs is more than 96%. In addition, these Fe3O4@SiO2-NH-HCGs have good stability and reusability. Their removal efficiency has no obvious decrease after being used seven times. After the experiments were finished, Fe3O4@SiO2-NH-HCGs were conveniently separated via an external magnetic field due to superparamagnetism. These results indicate that these Fe3O4@SiO2-NH-HCGs are potentially attractive materials for the removal of heavy metal ions from industrial wastewater.


Nanomaterials ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 1114
Author(s):  
Jiajia Li ◽  
Sicong Tan ◽  
Zhaoyang Xu

Currently, the preparation of outstanding adsorbents has attracted public concern in environmentally friendly and sustainable pollutant redress. Herein, we report a directional freeze-drying method to prepare a strong and reusable adsorbent by introducing metal-organic framework which modified by ethylene diamine tetraacetic acid (named UiO-66-EDTA) into cellulose nanofiber (CNF) aerogel. Compared to traditional aerogels, the fabricated adsorbent showed a good flexibility and reusability by forming a homogeneous three-dimensional structure. By controlling the concentration of a crosslinkable carboxymethyl cellulose (CMC) solution, we produced aerogels with different pore structures and fibrillar, columnar, and lamellar morphologies. The obtained UiO-66-EDTA/CNF/CMC aerogel (U-EDTACCA) showed an excellent adsorption performance for a total of nine types of heavy metal ions, as the removal efficiency could reach 91%. Moreover, the aerogels could retain 88% of their original shape after five cycles. The aerogel may be an appropriate material for the adsorption of heavy metal ions.


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