scholarly journals Acetylcholinesterase Biosensor Based On Mesoporous Hollow Carbon Spheres/Core-Shell Magnetic Nanoparticles-Modified Electrode for the Detection of Organophosphorus Pesticides

Sensors ◽  
2018 ◽  
Vol 18 (12) ◽  
pp. 4429 ◽  
Author(s):  
Ruiping Luo ◽  
Zijie Feng ◽  
Guannan Shen ◽  
Yi Xiu ◽  
Yukun Zhou ◽  
...  
Keyword(s):  
Detection Limit ◽  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Incubation Time ◽  
Core Shell ◽  
Carbon Electrode ◽  
Carbon Spheres ◽  
Hollow Carbon ◽  
Hollow Carbon Spheres

The present study investigated the synthesis of mesoporous hollow carbon spheres (MHCS) and magnetic mesoporous hollow carbon spheres with core-shell structures (Fe3O4@MHCS). Two acetylcholinesterase sensors (acetylcholinesterase/mesoporous hollow carbon spheres/glassy carbon electrode (AChE/MHCS/GCE) and acetylcholinesterase/core-shell magnetic mesoporous hollow carbon spheres/glassy carbon electrode (AChE/Fe3O4@MHCS/GCE) based on mesoporous carbon materials were prepared. Under the optimum conditions, using Malathion as the model compound, the developed biosensors showed a wide detection range, low detection limit, good reproducibility, and high stability. The AChE/MHCS/GCE electrochemical sensor response exhibited two good linear ranges at the incubation time of 10 min at the Malathion concentration ranges of 0.01 to 100 ppb and 100 to 600 ppb, with a detection limit of 0.0148 ppb (S/N = 3). The AChE/Fe3O4@MHCS/GCE electrochemical sensor that was operated with an incubation time of 12 min at the malathion concentration ranges between 0.01–50 ppb and 50–600 ppb had a detection limit of 0.0182 ppb (S/N = 3). Moreover, the AChE/MHCS/GCE and AChE/Fe3O4@MHCS/GCE biosensors were effective for the detection of real samples, and were demonstrated to be suitable for the field-testing of organophosphorus pesticide (OP) residues.

A Novel Electrochemical Sensor for the Analysis of Salbutamol in Pork Samples by Using NiFe2O4 Nanoparticles Modified Glassy Carbon Electrode

2013 ◽  
Vol 850-851 ◽  
pp. 1279-1282 ◽  
Author(s):  
Su Xing Luo ◽  
Yuan Hui Wu ◽  
Hua Gou ◽  
Yan Liu
Keyword(s):  
Detection Limit ◽  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Electrochemical Method ◽  
Carbon Electrode ◽  
Modified Glassy Carbon Electrode ◽  
Peak Current ◽  
Anodic Peak Current ◽  
Pork Samples

In this work, a simple and sensitive electrochemical method sensor was developed to determine salbutamol based on magnetic NiFe2O4nanoparticles modified glassy carbon electrode. It was found the anodic peak current of salbutamol was linear with the concentration of salbutamol from 2.0 μM to 60 μM with a detection limit of 1.0 μM (S/N=3). The developed method was successfully applied to determine salbutamol content in pork samples with satisfactory results.

scholarly journals Methyldopa electrochemical sensor based on a glassy carbon electrode modified with Cu/TiO2 nanocomposite

2018 ◽  
Vol 83 (7-8) ◽  
pp. 863-874 ◽  
Author(s):  
Somayeh Tajik ◽  
Hadi Beitollahi ◽  
Pourya Biparva
Keyword(s):  
Cyclic Voltammetry ◽  
Detection Limit ◽  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Urine Samples ◽  
Carbon Electrode ◽  
Modified Glassy Carbon Electrode ◽  
Pulse Voltammetry ◽  
Practical Feasibility

A Cu/TiO2 nanocomposite modified glassy carbon electrode (Cu/ /TiO2/GCE) was fabricated to detect methyldopa by cyclic voltammetry (CV) and different pulse voltammetry (DPV) methods. Compared with bare GCE, the Cu/TiO2/GCE exhibited excellent electrochemical activity for the oxidation of methyldopa. Using DPV technique, the calibration curves for methyldopa were found linear in the concentration range of 0.5?800.0 ?M and the detection limit (S/N = 3) was calculated to be 0.23 ?M. Additionally, the prepared electrochemical sensor of Cu/TiO2/GCE demonstrated a practical feasibility in methyldopa tablets and in urine samples analysis.

Sensitive Detection of Levocetirizine as a new Generation Antihistamine by Stripping Square Wave Voltammetry

2020 ◽  
Vol 16 (4) ◽  
pp. 424-437
Author(s):  
Kubra Ozturk ◽  
Nurgul K. Bakirhan ◽  
Sibel A. Ozkan ◽  
Bengi Uslu
Keyword(s):  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Differential Pulse ◽  
Real Sample ◽  
Carbon Electrode ◽  
Modified Glassy Carbon Electrode ◽  
Square Wave ◽  
Real Sample Analysis ◽  
Tablet Dosage

Background:: new and selective electrochemical sensor was developed for the determination of levocetirizine dihydrochloride, which is an antihistaminic drug. Method:: The investigation was performed by using cyclic, differential pulse and square wave voltammetric methods on the β-cyclodextrin modified glassy carbon electrode. It is thereby planned to obtain information about levocetirizine determination and its mechanism. Result:: The efficiency of experimental parameters including pH, scan rate, and accumulation potential and time on the anodic response of levocetirizine dihydrochloride was studied. By employing the developed method and under optimized conditions, the current showed linear dependence with a concentration in the range between 2 × 10-8 M and 6 × 10-6 M in pH 2.0 Britton Robinson (BR) buffer. Conclusion:: The achieved limits of detection and quantification were found as 3.73 × 10-10 M and 1.24 × 10-9 M, respectively. In addition, the possibility of applying the developed sensor for real sample analysis was investigated, so β-cyclodextrin modified glassy carbon electrode was used to determine levocetirizine dihydrochloride in Xyzal® tablet dosage form. Finally, this sensor was successfully applied to the real sample as a selective, simple, reproducible, repeatable electrochemical sensor.

scholarly journals Electrochemical Determination of Capsaicinoids Content in Soy Sauce and Pot-Roast Meat Products Based on Glassy Carbon Electrode Modified with Β-Cyclodextrin/Carboxylated Multi-Wall Carbon Nanotubes

Foods ◽  
2021 ◽  
Vol 10 (8) ◽  
pp. 1743
Author(s):  
Qianhui Gu ◽  
Chaoqun Lu ◽  
Kangwen Chen ◽  
Xingguang Chen ◽  
Pengfei Ma ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Meat Products ◽  
Soy Sauce ◽  
Relative Dispersion ◽  
Carbon Electrode ◽  
Trace Detection ◽  
Multi Wall Carbon Nanotubes

The rapid quantification of capsaicinoids content is very important for the standardization of pungent taste degree and flavor control of soy sauce and pot-roast meat products. To rapidly quantify the capsaicinoids content in soy sauce and pot-roast meat products, an electrochemical sensor based on β-cyclodextrin/carboxylated multi-wall carbon nanotubes was constructed and the adsorptive stripping voltammetry method was used to enrich samples in this study. The results showed that the excellent performance of the established electrochemical sensor was mostly because β-cyclodextrin caused the relative dispersion of carboxylated multi-wall carbon nanotubes on the glassy carbon electrode surface. Capsaicin and dihydrocapsaicin had similar electrochemical behavior, so the proposed method could determine the total content of capsaicinoids. The linearity of capsaicinoids content was from 0.5 to 100 μmol/L and the detection limit was 0.27 μmol/L. The recovery rates of different capsaicinoids content were between 83.20% and 136.26%, indicating the proposed sensor could realize trace detection of capsaicinoids content in sauce and pot-roast meat products. This work provides a research basis for pungent taste degree standardization and flavor control in the food industry.

Highly sensitive detection of hesperidin using AuNPs/rGO modified glassy carbon electrode

The Analyst ◽  
2018 ◽  
Vol 143 (1) ◽  
pp. 297-303 ◽  
Author(s):  
Yang Gao ◽  
Xiufeng Wu ◽  
Hui Wang ◽  
Wenbo Lu ◽  
Mandong Guo
Keyword(s):  
Gold Nanoparticles ◽  
Graphene Oxide ◽  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Carbon Electrode ◽  
Modified Glassy Carbon Electrode ◽  
Reduced Graphene ◽  
Highly Sensitive ◽  
Highly Sensitive Detection

The highly sensitive and selective electrochemical sensor of hesperidin based on gold nanoparticles (AuNPs) and reduced graphene oxide (rGO) modified glassy carbon electrode (GCE) is reported.

Nitrogen-doped hollow carbon spheres with a wrinkled surface: their one-pot carbonization synthesis and supercapacitor properties

2016 ◽  
Vol 52 (78) ◽  
pp. 11693-11696 ◽  
Author(s):  
Lei Liu ◽  
Shi-Da Xu ◽  
Qing Yu ◽  
Feng-Yun Wang ◽  
Hui-Ling Zhu ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Core Shell ◽  
Carbon Spheres ◽  
Melamine Formaldehyde ◽  
One Pot ◽  
Nitrogen Doped ◽  
Wrinkled Surface ◽  
Hollow Carbon ◽  
Hollow Carbon Spheres

Nitrogen-doped hollow carbon spheres with a wrinkled surface were synthesized through direct pyrolysis of core–shell structured graphene oxide–resol@melamine formaldehyde composites.

An electrochemical sensor for honokiol based on a glassy carbon electrode modified with MoS2/graphene nanohybrid film

2014 ◽  
Vol 6 (23) ◽  
pp. 9375-9382 ◽  
Author(s):  
Xiaojuan Zhao ◽  
Xiaohong Xia ◽  
Shengjiao Yu ◽  
Chunming Wang
Keyword(s):  
Electrochemical Sensor ◽  
Glassy Carbon Electrode ◽  
Glassy Carbon ◽  
Carbon Electrode ◽  
Sensitive Determination

An electrochemical sensor for the sensitive determination of honokiol was successfully constructed based on MoS2/graphene nanohybrid.

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