scholarly journals Screen-Printed Electrode Modified by Bismuth /Fe3O4 Nanoparticle/Ionic Liquid Composite Using Internal Standard Normalization for Accurate Determination of Cd(II) in Soil

Sensors ◽  
2017 ◽  
Vol 18 (2) ◽  
pp. 6 ◽  
Author(s):  
Hui Wang ◽  
Guo Zhao ◽  
Yuan Yin ◽  
Zhiqiang Wang ◽  
Gang Liu
2020 ◽  
Vol 187 (4) ◽  
Author(s):  
Sudkate Chaiyo ◽  
Sakda Jampasa ◽  
Natnicha Thongchue ◽  
Eda Mehmeti ◽  
Weena Siangproh ◽  
...  

Author(s):  
Abolfazl Darroudi ◽  
Saeid Nazari ◽  
Seyed Ali Marashi ◽  
Mahdi Karimi-Nazarabad

Abstract An accurate, rapid, simple, and novel technique was developed to determine simvastatin (SMV). In this research, a screen-printed electrode (SPE) was deposited with graphene oxide (GO) and sodium dodecyl sulfate (SDS), respectively. For the first time, the handmade modified SPE measured the SMV by differential pulse voltammetry (DPV) with high sensitivity and selectivity. The results of cyclic voltammetry indicated the oxidation irreversible process of SMV. Various parameters (pH, concentration, scan rate, support electrolyte) were performed to optimize the conditions for the determination of SMV. Under the optimum experiment condition of 0.1 M KNO3 as support electrolyte and pH 7.0, the linear range was achieved for SMV concentration from 1.8 to 36.6 µM with a limit of detection (LOD), and a limit of quantitation (LOQ) of 0.06 and 1.8 µM, respectively. The proposed method was successfully utilized to determine SMV in tablets and urine samples with a satisfactory recovery in the range of 96.2 to 103.3%.


Sign in / Sign up

Export Citation Format

Share Document