scholarly journals Influence of Different Conditioning Treatments on The Bond Integrity of Root Dentin to rGO Infiltrated Dentin Adhesive. SEM, EDX, FTIR and MicroRaman Study

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1555
Author(s):  
Firas Alqarawi ◽  
Mazen Alkahtany ◽  
Khalid Almadi ◽  
Afnan Gassem ◽  
Faris Alshahrani ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Bond Strength ◽  
Strength Test ◽  
Control Group ◽  
Micro Raman Spectroscopy ◽  
Fiber Posts ◽  
Root Canal Disinfection ◽  
Reduced Graphene ◽  
Root Dentin ◽  
Push Out

The present study aimed to synthesize and equate the mechanical properties and dentin interaction of two adhesives; experimental adhesive (EA) and 5 wt.% reduced graphene oxide rGO) containing adhesive. Scanning electron microscopy (SEM)-Energy-dispersive X-ray spectroscopy (EDX), Micro-Raman spectroscopy, push-out bond strength test, and Fourier Transform Infrared (FTIR) spectroscopy were employed to study nano-bond strength, degree of conversion (DC), and adhesive-dentin interaction. The EA was prepared, and rGO particles were added to produce two adhesive groups, EA-rGO-0% (control) and rGO-5%. The canals of sixty roots were shaped and prepared, and fiber posts were cemented. The specimens were further alienated into groups based on the root canal disinfection technique, including 2.5% sodium hypochlorite (NaOCl), Photodynamic therapy (PDT), and ER-CR-YSGG laser (ECYL). The rGO nanoparticles were flake-shaped, and EDX confirmed the presence of carbon (C). Micro-Raman spectroscopy revealed distinct peaks for graphene. Push-out bond strength test demonstrated highest values for the EA-rGO-0% group after NaOCl and PDT conditioning whereas, rGO-5% showed higher values after ECYL conditioning. EA-rGO-0% presented greater DC than rGO-5% adhesive. The rGO-5% adhesive demonstrated comparable push-out bond strength and rheological properties to the controls. The rGO-5% demonstrated acceptable DC (although lower than control group), appropriate dentin interaction, and resin tag establishment.

scholarly journals Effect of Chlorhexidine and Ethanol Application on Longterm Push-out Bond Strength of Fiber Posts to Dentin

2015 ◽  
Vol 16 (7) ◽  
pp. 547-553 ◽  
Author(s):  
Roberta Tarkany Basting ◽  
Cecília Pedroso Turssi ◽  
Flavia Lucisano Botelho do Amaral ◽  
Fabiana Mantovani Gomes França ◽  
Rafaela Crystyan Vaneli ◽  
...  
Keyword(s):  
Bond Strength ◽  
Repeated Measures ◽  
Adhesive System ◽  
Resin Cement ◽  
Control Group ◽  
Test Analysis ◽  
Significance Level ◽  
Fiber Posts ◽  
Etch And Rinse ◽  
Push Out

ABSTRACT Aim The aim of this study was to evaluate the effect of chlorhexidine and ethanol application on the push-out bond strength and bond durability of fiber posts cemented with an etch-and-rinse adhesive system/resin cement to intraradicular dentin. Materials and methods Fifty-four bovine roots were shaped for the cementation of a fiberglass post and received the application of 37% phosphoric acid. They were then randomly divided into three groups, according to the type of dentin treatment (n = 18) performed: no treatment (control group), 100% ethanol, or 2% chlorhexidine. Next, the adhesive system (Adper Scotch Bond Multipurpose Plus, 3M ESPE) was applied to the dentin, according to the manufacturer's instructions. Glass fiber posts were cemented with dual resin cement (Rely X ARC, 3M ESPE). After 48 hours, the specimens were serially sectioned for push-out test analysis, providing two slices from each root third (cervical, medium and apical), one of which was tested immediately and the other stored in distilled water for 180 days. The data were analyzed with three-way analysis of variance (ANOVA) for repeated measures and Tukey's test at a 5% significance level. Results Intraradicular treatment with chlorhexidine yielded the highest bond strength means, followed by ethanol treatment. The control group presented the lowest bond strength means. Water storage exerted no effect on bond strength values. Conclusion Both chlorhexidine and ethanol improved push-out bond strength to intraradicular dentin, with the former providing the best results, regardless of the storage time. Clinical significance The application of 2% chlorhexidine or 100% ethanol may be an important step that can be taken to enhance bond strength of fiber posts to intraradicular dentin, when dual resin cements are used. How to cite this article França FMG, Vaneli RC, de Melo Conti C, Basting RT, do Amaral FLB, Turssi CP. Effect of Chlorhexidine and Ethanol Application on Long-term Pushout Bond Strength of Fiber Posts to Dentin. J Contemp Dent Pract 2015;16(7):547-553.

scholarly journals Effect of cement type and thickness on push-out bond strength of fiber posts

2018 ◽  
Vol 12 (4) ◽  
pp. 277-282
Author(s):  
Farzaneh Farid ◽  
Khadijeh Rostami ◽  
Sareh Habibzadeh ◽  
MohammadJavad Kharazifard
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Test Results ◽  
Resin Cements ◽  
Fiber Posts ◽  
Significant Difference ◽  
Root Dentin ◽  
Group 2 ◽  
Self Etch ◽  
Push Out

Background. This study investigated the effect of the thickness of two resin cements on push-out bond strength of fiber posts to root dentin. Methods. Sixty decoronated single-rooted teeth were endodontically treated. The specimens were then randomly allocated to two groups (n=30); group 1: drill size 90 w, matching the size of fiber posts used; group 2: drill size 110, larger than the posts. The specimens in each group were divided into 2 subgroups (n=15); subgroup SE, in which the posts were cemented with self-etch Panavia F2.0 and subgroup SA, in which self-adhesive Panavia cement was used. After 72 hours, 2 slices with 1 mm of thickness were prepared from the mid-root of each specimen. Push-out bond strength test was performed in a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with two-way ANOVA and t-test. Results. The mean bond strengths of the posts cemented in matched-size spaces for SE and SA groups were 4.02±1.6 and 4.12±2.3 MPa, respectively. For posts cemented in oversized spaces, the values were 4.9±2.3 and 2.8±1.3 MPa, respectively. In matched-size spaces, there was no significant difference between the two groups. Conclusion. The results of this study suggested that increasing the cement thickness would reduce the bond strength of fiber posts to root dentin when self-adhesive cements are used; however, self-etch adhesives were not affected.

scholarly journals Effects of Heat Treating Silane and Different Etching Techniques on Glass Fiber Post Push-out Bond Strength

2014 ◽  
Vol 39 (5) ◽  
pp. E217-E224 ◽  
Author(s):  
P Samimi ◽  
V Mortazavi ◽  
F Salamat
Keyword(s):  
Heat Treatment ◽  
Hydrogen Peroxide ◽  
Bond Strength ◽  
Glass Fiber ◽  
Control Group ◽  
Fiber Post ◽  
Fiber Posts ◽  
Heat Treated ◽  
Significant Difference ◽  
Push Out

SUMMARY The aims of this study were to compare two pretreatment methods of a fiber post and to evaluate the effect of heat treatment to applied silane on the push-out bond strength for different levels of root. In this in vitro study, 40 glass fiber posts were divided into five groups (n=8) according to the kind of surface treatment applied. They were then inserted into extracted and endodontically treated human canines using a self-etch resin cement (Panavia F2.0, Kuraray, Japan). Group HF+S = hydrofluoric acid (HF) etching and silane (S) application; group HF+S+WP = HF etching and heat-treated silane application and warmed posts (WP); group H2O2+S = hydrogen peroxide etching and silane application; group H2O2+S+WP = hydrogen peroxide and heat-treated-silane application and warmed post; and group C, the control group, received no pretreatment. After completion of thermal cycling (1000 cycles, 5-55°C), all specimens were cut horizontally to obtain three sections. Each section was subjected to a push-out test, and the test results were analyzed using two-way analysis of variance, post-hoc Tukey honestly significant difference test, and a paired sample t-test (α=0.05). It was found that bond strength was not statistically influenced by the kind of etching material used (p=0.224), but was significantly affected by heat treatment of applied silane (p<0.001). The interaction between these two factors was not statistically significant (p=0.142). Group HF+S+WP showed the highest bond strength (12.56±1.73 MPa) (p<0.05). Scanning electron microscopy revealed the effect of the different treatments on the surface characteristics of posts. In the four pretreated groups, the bond strength decreased significantly from the coronal to the apical root canal sections (p≤0.05). The results of this study show that the use of heat-treated silane significantly enhances the push-out bond strength of the fiber posts to root. HF acid etching with heat-treated silane application led to the highest bond strength.

scholarly journals Influence of sodium hypochlorite/etidronic acid combination and SmearOFF on push-out bond strength of fiber posts to root dentin

2020 ◽  
Vol 39 (4) ◽  
pp. 554-562
Author(s):  
Cevat Emre ERİK ◽  
Bulem ÜREYEN KAYA ◽  
Murat MADEN ◽  
Ekim Onur ORHAN
Keyword(s):  
Bond Strength ◽  
Sodium Hypochlorite ◽  
Etidronic Acid ◽  
Fiber Posts ◽  
Root Dentin ◽  
Push Out

Effect of Mechanical Cycling on the Push-out Bond Strength of Fiber Posts Adhesively Bonded to Human Root Dentin

2007 ◽  
Vol 32 (6) ◽  
pp. 579-588 ◽  
Author(s):  
L. F. Valandro ◽  
P. Baldissara ◽  
G. A. Galhano ◽  
R. M. Melo ◽  
A. Mallmann ◽  
...  
Keyword(s):  
Bond Strength ◽  
Clinical Relevance ◽  
Extended Period ◽  
Adhesively Bonded ◽  
Mechanical Cycling ◽  
Fiber Posts ◽  
Root Dentin ◽  
Push Out ◽  
Retention Strength

Clinical Relevance When adhesively cemented, tested fiber posts are fatigue resistant and appear to have no affect on bond strength to root dentin. Thus, the retention strength of these fiber posts could be maintained for an extended period; however, further studies should be conducted.

scholarly journals Dentin Bond Integrity of Filled and Unfilled Resin Adhesive Enhanced with Silica Nanoparticles—An SEM, EDX, Micro-Raman, FTIR and Micro-Tensile Bond Strength Study

Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1093
Author(s):  
Aasem M. Alhenaki ◽  
Esra A. Attar ◽  
Abdullah Alshahrani ◽  
Imran Farooq ◽  
Fahim Vohra ◽  
...  
Keyword(s):  
Raman Spectroscopy ◽  
Bond Strength ◽  
Silica Nanoparticles ◽  
Negative Control Group ◽  
Negative Control ◽  
Tensile Bond Strength ◽  
Control Group ◽  
Mean Values ◽  
Micro Raman Spectroscopy ◽  
Dentin Adhesive

The objective of this study was to synthesize and assess unfilled and filled (silica nanoparticles) dentin adhesive polymer. Methods encompassing scanning electron microscopy (SEM)—namely, energy dispersive X-ray spectroscopy (EDX), micro-tensile bond strength (µTBS) test, Fourier transform infrared (FTIR), and micro-Raman spectroscopy—were utilized to investigate Si particles’ shape and incorporation, dentin bond toughness, degree of conversion (DC), and adhesive–dentin interaction. The Si particles were incorporated in the experimental adhesive (EA) at 0, 5, 10, and 15 wt. % to yield Si-EA-0% (negative control group), Si-EA-5%, Si-EA-10%, and Si-EA-15% groups, respectively. Teeth were set to form bonded samples using adhesives in four groups for µTBS testing, with and without aging. Si particles were spherical shaped and resin tags having standard penetrations were detected on SEM micrographs. The EDX analysis confirmed the occurrence of Si in the adhesive groups (maximum in the Si-EA-15% group). Micro-Raman spectroscopy revealed the presence of characteristic peaks at 638, 802, and 1300 cm−1 for the Si particles. The µTBS test revealed the highest mean values for Si-EA-15% followed by Si-EA-10%. The greatest DC was appreciated for the control group trailed by the Si-EA-5% group. The addition of Si particles of 15 and 10 wt. % in dentin adhesive showed improved bond strength. The addition of 15 wt. % resulted in a bond strength that was superior to all other groups. The Si-EA-15% group demonstrated acceptable DC, suitable dentin interaction, and resin tag formation.

scholarly journals Effect of different root dentin pretreatment protocols on the bond strength of fiber posts cemented with core buildup material

2019 ◽  
Vol 22 (1) ◽  
pp. Process
Author(s):  
Rowaida Naeem ◽  
Maged Zohdy ◽  
Tarik Salah
Keyword(s):  
Bond Strength ◽  
Failure Modes ◽  
Testing Machine ◽  
Calculated Data ◽  
Core Material ◽  
Fiber Posts ◽  
Stereo Microscope ◽  
Root Dentin ◽  
Self Etch ◽  
Push Out

Objective: The purpose of the study was to evaluate the push out bond strength of fiber posts -after cementaion with core build up material and dentin pretreatment using different adhesive protocols- in different root regions. Material and Methods: 28 endodonticaly treated human premolars were divided into 4 groups. The post spaces were treated with 1 of 4 different dentin bonding protocols: total etch light cured adhesive, solobond m; total etch dual cured adhesive, Excite f DSC; self-etching light cured adhesive, single bond universal; or self-etching dual cured adhesive, futura bond dc. Fiber posts, were luted with dual cured core material. The roots were cut into 2-mm-thick sections, in cervical, middle, and apical regions. Push-out tests were performed with a universal testing machine, and bond strength values (MPa) were calculated. Data were analyzed with 1- and 2-way analysis of variance and Tukey multiple comparison tests (a=.05). Failure modes were examined under stereo microscope. Results: The highest mean bond strength values were obtained for self-etch dual cured adhesive, (9.69 MPa). The Total etch light cured adhesive (2.81 MPa) showed the lowest bond strength. Self-etch light-polymerized and total etch dual-polymerized adhesives provided similar bond strengths (5.37, 5.72 respectively). The regional bond strength values were reduced significantly in apical post space (P<0.01). The most predominant failure type was mixed failure followed by adhesive failure. Conclusion: Dentin pretreatment using self-etch dual cured adhesives prior to fiber posts cementation offers a high bond strength. While using total-etch light cured adhesives is not recommended due to the low bonding quality. KeywordsDentin; Bond strength; Fiber posts; Core buildup material; Adhesive protocols; Pretreatment.

Effect of the frequency of mechanical pulses for fatigue aging testing on push-out bond strength between glass fiber posts and root dentin

2016 ◽  
Vol 30 (11) ◽  
pp. 1243-1252 ◽  
Author(s):  
Marília Pivetta Rippe ◽  
Vinícius Felipe Wandscher ◽  
César Dalmolin Bergoli ◽  
Paolo Baldissara ◽  
Mutlu Özcan ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Fiber ◽  
Fiber Posts ◽  
Glass Fiber Posts ◽  
Root Dentin ◽  
Push Out
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