scholarly journals Improvement of Heat-Treated Wood Coating Performance Using Atmospheric Plasma Treatment and Design of Experiments Method

Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1520
Author(s):  
Ender Hazir

The aim of this work is to improve the heat-treated wood coating performance using experimental design methodology and air–plasma treatment. Firstly, two different heat treatment processes were applied to the wood samples. In the second stage of the study, air–atmospheric plasma treatment was applied to heat-treated samples. These samples were coated with water-based varnish. Adhesion strength and colour change values of these samples before and after the artificial weathering test were measured. The design of experiments method was used to investigate the significant factors. The heat treatment process (212 °C—1 h and 212 °C—2 h) and atmospheric plasma treatment parameters (pressure, distance, and feed) were selected as independent variables, while adhesion strength and colour change were determined as dependent variables. The factors affecting the surface coating performance before and after the artificial weathering test were evaluated by analysis of variance (ANOVA) and Pareto plot. In addition, the factor levels that maximise the adhesion strength value and minimise the colour change were found using the multiobjective optimisation technique. According to the multiobjective optimisation method, results of treatment feed, working distance, and pressure of 60 mm/s, 7.69 mm, and 1 bar were considered as optimum plasma treatment conditions, respectively, for heat treatment process A. Corresponding values for the heat treatment process B were 60 mm/s, 10 mm, and 2 bar.

Holzforschung ◽  
2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Jure Žigon ◽  
Matjaž Pavlič ◽  
Pierre Kibleur ◽  
Jan Van den Bulcke ◽  
Marko Petrič ◽  
...  

AbstractPlasma treatment is becoming a mature technique for modification of surfaces of various materials, including wood. A better insight in the treatment process and the impact of the plasma on properties of wood bulk are still needed. The study was performed on Norway spruce and common beech wood, as well as their thermally modified variations. The formations of the airborne discharge, as well as mass changes of the treated wood, were monitored. The impact of such treatment on wood-coating interaction was investigated by evaluating the dynamic wettability and penetration into wood. At the wood surface, plasma streamers were observed more intense on denser latewood regions. Wood mass loss was higher with increasing number of passes through the plasma discharge and was lower for thermally modified wood than for unmodified wood. Plasma treatment increased the surface free energy of all wood species and lowered the contact angles of a waterborne coating, these together indicating enhanced wettability after treatment. Finally, the distribution and penetration depth of the coating were studied with X-ray microtomography. It was found that the coating penetrated deeper into beech than into spruce wood. However, the treatment with plasma increased the penetration of the coating only into spruce wood.


2019 ◽  
Vol 2019 ◽  
pp. 1-9 ◽  
Author(s):  
Vlatka Jirouš-Rajković ◽  
Josip Miklečić

Heat treatment is a method of wood modification with increasing market acceptance in Europe. The major patented European commercial heat treatment processes have trade names ThermoWood, Platowood, Retiwood, Le Bois Perdure, and Oil-Heat-Treated Wood (OHT). To what extent modification of wood affects the resistance of wood to weathering is also an important aspect for wood applications, especially where appearance is important. Unfortunately, heat-treated wood has poor resistance to weathering, and surface treatment with coatings is required for both protection and aesthetic reasons. As a substrate for coating, heat-treated wood has altered characteristics such as lower hygroscopicity and liquid water uptake and changed acidity, wettability, surface free energy, and anatomical microstructure. Various wood species, heat treatment method, treatment intensity, and treatment conditions exhibited a different extent of changes in wood properties. These altered properties could affect coating performance on heat-treated wood. The reported changes in acidity and in surface energy due to heat treatments are inconsistent with one another depending on wood species and temperature of the treatments. This paper gives an overview of the research results with regards to properties of heat-treated wood that can affect coating performance and weathering of uncoated and coated heat-treated wood.


2005 ◽  
Vol 495-497 ◽  
pp. 907-912 ◽  
Author(s):  
Suk Hoon Kang ◽  
Hee Suk Jung ◽  
Woong Ho Bang ◽  
Jae Hyung Cho ◽  
Kyu Hwan Oh ◽  
...  

This paper studies the microstructure of drawn gold wires to equivalent strain of 10 and to equivalent strain of 8.5 then heat-treated. The texture of gold wire drawn to strain of 10 is mainly composed of <100> and <111> fibers. Tensile strength of the gold wire increases with <111> fiber fraction, while the grain size does not appear to affect the tensile property. With an exception at heat treatment at 600oC, the texture of gold wire drawn the strain of 8.5 is replaced with <100> fiber component by heat treatment process at 400~700oC. Heat treatment at 600oC produces <110> fiber or <112> fiber, depending upon annealing time.


2017 ◽  
Vol 898 ◽  
pp. 1705-1711 ◽  
Author(s):  
Jun Zhe Li ◽  
Xun Sun ◽  
Hai Tao Liu ◽  
Hai Feng Cheng ◽  
Xiao Shan Zhang

The composition and microstructure of silicon nitride fibers after heat-treatment at elevated temperatures were investigated by XRD, NMR, XPS, SEM and TEM analyses. The results show that as-received fibers consisted of amorphous silicon nitride, and a little Si-C-O structure. During heat-treatment process, α-Si3N4 and β-Si3N4 formed resulting from the crystallization of amorphous silicon nitride, and the formation of β-SiC derived from the decomposition of Si-C-O structure. As heat-treated temperature increased from 1400oC to 1600oC, the above phenomenon become obvious, indicating that the fiber would possess high serving life with serving temperature lower than 1400oC. The tensile strength of fibers stays stable when heat-treated temperature was below 1200oC, while the strength retention of fibers sharply decreased to 50% after heat-treatment at 1400°C.


2014 ◽  
Vol 1061-1062 ◽  
pp. 454-459
Author(s):  
An Min Li ◽  
Ding Ma ◽  
Qi Feng Zheng ◽  
Ruo Huai Chen ◽  
Qiang Li ◽  
...  

The as-cast grate bar structure used in sintering trolley is primarily comprised of austenite and eutectic (eutectic austenite and eutectic carbide).The austenite is dendrite, while the carbides are reticular and chrysanthemum-like. The failed grate bar structure primarily consists of ferrite, carbide, martensite and residual austenite; cavity shrinkage and shrinkage porosity exist in the structure, and the fracture exhibits typical cleavage fracture characteristics. The primary means of failure are abrasion and fracture. The secondary carbides precipitated in the sample (quenching (1050°C+2.5h)+ tempering (390°C+2.5h)) and the other one (quenching (1050°C+2.5h)+ tempering (420°C+2.5h) ) are dispersed and refined. Compared with the as-cast one, their relative abrasion resistance performances respectively are 0.8645 and 0.8752.The values of hardness and impact toughness of the samples heat-treated are greater than those of the as-cast grate bar. The optimum heat treatment process is as follows: quenching (1050°C,2.5h) + tempering (390°C~420°C,2.5h)


Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 157 ◽  
Author(s):  
Jun Zhang ◽  
Ziming Kou ◽  
Yaqin Yang ◽  
Baocheng Li ◽  
Xiaowen Li ◽  
...  

High damping magnesium alloys have poor mechanical properties, so it is necessary to investigate the damping properties of high-strength wrought magnesium alloys to effectively reduce vibration and noise in mechanical engineering. The aim of this work is to improve the mechanical damping performance of a novel high-strength Mg-13Gd-4Y-2Zn-0.5Zr magnesium alloy by optimising the heat treatment process. The mechanical damping coefficient, considering not only damping capacity but also the yield strength, is selected as one of the evaluation indexes. The other evaluation index is the tensile strength. The solid solution and ageing treatment were optimised by Box-Behnken method, an efficient experimental design technique. Heat treatment experiments based on the optimal parameters verified that the best process is a solution at 520 °C for 10 h followed by ageing at 239 °C for 22 h. The damping coefficient reaches 0.296, which is 73.1% higher than that before heat treatment. There was a good agreement between the experimental and Box-Behnken predicted results. The microstructure, morphology and composition of the second phases after heat treatment were analysed by SEM, XRD and EDS. Due to the high content of alloying elements in Mg-13Gd-4Y-2Zn-0.5Zr alloy, there are a large number of second phases after heat treated. They mainly include layer, short rod-shaped, bulk long period stacking order (LPSO) Mg12YZn and granular Mg5Gd phases. It was found that the area fraction of the second phases has an extreme effect on the damping capacity and short rod-shaped LPSO can effectively improve the damping capacity of heat-treated Mg-13Gd-4Y-2Zn-0.5Zr alloy. The volume fraction of the second phases was analysed by ImageJ software. It was concluded that the smaller the area occupied by the second phases, the better the mobility of the dislocation, and the better the damping performance of the alloy. The statistical analysis results obtained using ImageJ software are consistent with the experimental results damping capacity.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3668
Author(s):  
Tian Xia ◽  
Rui Wang ◽  
Zhongnan Bi ◽  
Guoliang Zhu ◽  
Qingbiao Tan ◽  
...  

Additive manufacturing (AM) of nickel-based superalloys is of high interest for application in complex hot end parts. However, it has been widely suggested that the microstructure-properties of the additive manufacturing processed superalloys are not yet fully clear. In this study, the GTD222, an important superalloy for high-temperature hot-end part, were prepared using selective laser melting and then subjected to heat treatment. The microstructure evolution of the GTD222 was investigated and the mechanical properties of heat treated GTD222 were tested. The results have shown that the grain size of the heat treated GTD222 was close to its as-built counterparts. Meanwhile, a large amount of γ’ and nano-scaled carbides were precipitated in the heat treated GTD222. The microstructure characteristics implied that the higher strength of the heat treated GTD222 can be attributed to the γ’ and nano-scaled carbides. This study provides essential microstructure and mechanical properties information for optimizing the heat treatment process of the AM processed GTD222.


CONVERTER ◽  
2021 ◽  
pp. 347-353
Author(s):  
Xiaoming Ren, Et al.

In order to obtain good TaN film transducer and reduce its ignition voltage, the influence of the setting position and cooling method of the heat treatment process on the TaN film transducer were compared and analyzed. By measuring the square resistivity, SEM and XRD, the performance of the film before and after heat treatment were characterized. The ignition voltage of the TaN film transducer was tested, and the results showed that the ignition voltage of the heat-treated TaN film transducer could be reduced a lot. It provided a technical way for the micro-energy of MEMS pyrotechnics.


2014 ◽  
Vol 9 (1-2) ◽  
Author(s):  
Dragan P Vujadinović ◽  
Božana V Odžaković ◽  
Radoslav D Grujić ◽  
Milija Perić

Abstract: A heat-treated beet is defined as a food that is subject to a temperature, high enough to destroy microorganisms and to preserve all the nutrients. The aim of the study presented in this paper was to investigate the effect by cooking on the properties of heat threated beetroot in the temperature range between 75 °C and 115 °C during the 40, 50 and 60 minutes of cooking. In order to determine the optimal conditions for the implementation of various heat treatment procedures consequently, was followed the influence of heat treatment conditions (temperature/time) on the composition, rheological properties, pH, color change (L*, a*, b*) and sensory characteristics during the development of the “pasteurized/sterilized” beet product. This study has shown that the optimum time and temperature for processing of beetroot is 105 °C at 50 minutes. Samples of beetroot, processed under these conditions had the best softness, the most acceptable taste and color (sensory and instrumentally determined).


RSC Advances ◽  
2020 ◽  
Vol 10 (37) ◽  
pp. 22113-22119 ◽  
Author(s):  
Takahiro Suzuki ◽  
Jing Cheng ◽  
Li Qiao ◽  
Yan Xing ◽  
Meng Fei Zhang ◽  
...  

The morphology of the prepared samples. (a) FESEM images of each temperature which shows the structural evolution of as-spun fibers to nanotube during the heat treatment process. (b) TEM images of 600 °C heat-treated sample.


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