scholarly journals Influence of the Epoxy Resin Process Parameters on the Mechanical Properties of Produced Bidirectional [±45°] Carbon/Epoxy Woven Composites

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1273
Author(s):  
Claudia A. Ramírez-Herrera ◽  
Isidro Cruz-Cruz ◽  
Isaac H. Jiménez-Cedeño ◽  
Oscar Martínez-Romero ◽  
Alex Elías-Zúñiga

This work focuses on investigating the curing process of an epoxy-based resin—Aerotuf 275-34TM, designed for aerospace applications. To study the curing degree of Aerotuf 275-34TM under processing conditions, woven carbon fiber fabric (WCFF)/Aerotuf 275-34TM composite laminates were produced by compression molding using different processing temperatures (110, 135, 160, and 200 °C) during 15 and 30 min. Then, the mechanical behavior of the composite laminates was evaluated by tensile tests and correlated to the resin curing degree through Fourier-transform infrared spectroscopy (FTIR) analysis. The results show the occurrence of two independent reactions based on the consumption of epoxide groups and maleimide (MI) double bonds. In terms of epoxide groups, a conversion degree of 0.91 was obtained for the composite cured at 160 °C during 15 min, while the measured tensile properties of [±45°] WCFF/Aerotuf 275-34TM laminates confirmed that these epoxy resin curing processing conditions lead to an enhancement of the composite mechanical properties.

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5856
Author(s):  
Pragya Mishra ◽  
Pia Åkerfeldt ◽  
Farnoosh Forouzan ◽  
Fredrik Svahn ◽  
Yuan Zhong ◽  
...  

Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.


2019 ◽  
Vol 54 (13) ◽  
pp. 1705-1715
Author(s):  
MHR Jen ◽  
GT Kuo ◽  
YH Wu ◽  
YJ Chen

The mechanical properties and fatigue responses of Ti/APC-2 neat and nanocomposites with inclined single-edged cracks due to tensile and cyclic tests at elevated temperature were investigated. Two types of composite laminates [Ti/(0/90)s/Ti] were fabricated with and without (W/WO) nanoparticles SiO2 of optimal 1 wt.%. The geometry and dimensions of specimens were L × W × t = 240 × 25 × 1.55 mm3. The cracks were of constant length 3 mm and width 0.3 mm. The inclined angles were 0°, 45°, and 60°. Both the tensile and cyclic tests were conducted at elevated temperatures 25℃ (RT), 100℃, 125℃, and 150℃. From the tensile tests we obtained the load vs. displacement curves for both types of laminates with varied inclinations at elevated temperatures. Next, we received the applied load vs. cycles curves for the same laminates with inclined cracks at the corresponding temperature due to cyclic tests. According to the experimental data of both tensile and cyclic tests the mechanical properties, such as strength, stiffness, and life, decreased as the temperature rises. The greater the inclined angles were, the greater the strength and stiffness were. Similarly, the fatigue life was in the same trend. However, the effect of inclined angle on mechanical properties was more strong than those of temperature. The mechanical properties of nanocomposite laminates were higher than those of neat composite laminates, but not significant. The main reason was that the enhancement of spreading nano-powder silica on the laminate interfaces did not effectively eliminate the stress intensity at the crack tip locally.


Polymers ◽  
2020 ◽  
Vol 12 (8) ◽  
pp. 1688
Author(s):  
Marius Marinel Stănescu ◽  
Dumitru Bolcu

When obtaining environment-friendly hybrid resins made of a blend of Dammar natural resin, in a prevailing volume ratio, with epoxy resin, it is challenging to find alternatives for synthetic resins. Composite materials reinforced with waste paper and matrix made of epoxy resin or hybrid resin with a volume ratio of 60%, 70% and 80% Dammar were studied. All samples obtained have been submitted to tensile tests and Scanning Electron Microscopy (SEM) analysis. The tensile response, tensile strength, modulus of elasticity, elongation at break and the analysis of the fracture surface were determined. The damping properties of vibrations of bars in hybrid resins and in the composite materials under study were also examined. The mechanical properties of the four types of resins and of the composite materials were compared. The chemical composition for a hybrid resin specimen were obtained using the Fourier Transformed Infrared Spectroscopy (FTIR) and Energy, Dispersive X-ray Spectrometry (EDS) analyzes.


2011 ◽  
Vol 331 ◽  
pp. 65-68
Author(s):  
Ge Wang ◽  
Fu Ming Chen ◽  
Hai Tao Cheng ◽  
Zi Xuan Yu ◽  
Ze Hui Jiang ◽  
...  

The objective of this work was to use a novel 3-D test analysis system for evaluating the mechanical properties of the natural fiber fabric composites under biaxial loads. Composites with three resin matrices (water-based epoxy resin, isocyanate resin, phenolic resin) were investigated, and strain filed were characterized by using the digital speckle correlation. The water-based epoxy resin plate and isocyanate resin plate demonstrated a characteristic of orthotropy and elastoplasticity, while the phenolic resin board revealed linear elastic and brittle-fracture simultaneously at X,Y-axial. Dissimilarities of biaxial load value were related to the orthotropy of composite structure, and load changes in fracture direction had a negative effect on the other directions at breaking moment. The degrees of dropping presented a positive correlation with the load values at rift direction. Under the linear elastic stage, the value of load and average strain at Y-direction were larger than that under X-direction within the same testing area. The strain-filed at X/Y-direction provided by isocyanate and phenolic resin plates illustrated a more smooth change than that of the water-based epoxy resin plate.


2020 ◽  
Vol 321 ◽  
pp. 04029
Author(s):  
Ioana POPA ◽  
Maxime BERTHAUD ◽  
Clément CISZAK ◽  
Jean-Michel BROSSARD ◽  
Daniel MONCEAU ◽  
...  

Titanium alloys are widely used in aerospace applications due to their good ratio of weight versus mechanical properties. When exposed to air at 560°C, Ti6242S titanium alloy presents very good oxidation resistance: a very thin oxide layer forms at its surface and oxygen dissolution inside the metallic material is rather limited. However, in real functioning conditions of the plane, near seas or oceans, the atmosphere contains NaCl, that can crystallise at the surface of hot parts. An active corrosion mechanism is established in these conditions, with catastrophic effect on the material behaviour at high temperature: very thick and brittle oxide scales and very important damaging of the metal outer part. Another issue is the formation of Na2SO4 specie by reaction of NaCl with kerosene combustion gases (SO2/SO3), leading to mixed NaCl/Na2SO4 deposits. The effect of exposure conditions on the mechanical properties of titanium alloy Ti6242S was evaluated through tensile tests performed on the raw alloy and after oxidation in air at 560°C of the specimens: without any deposit, with NaCl solid deposit, with NaCl/Na2SO4 solid deposit. The evolution of mechanical properties was interpreted in connexion with the microstructural modifications that occur during the high temperature ageing.


2021 ◽  
Vol 2 (1) ◽  
pp. 17
Author(s):  
Sunil Kumar ◽  
Arun Gupta

<p>Among the various kinds of reinforcing element, Multi Wall Carbon Nano-tubes (MWCNT) and Nanoclay have found much more attention as a filler element to upgrade the mechanical properties of polymer composite material. In this paper, production of hybrid nanocomposites and the effect of MWCNT and nanoclay on mechanical properties of hybrid nanocomposites have been evaluated. In hybrid nanocomposites, MWCNT and nanoclay are embedded in epoxy resin. The processing of hybrid nanocomposite is always been a difficult task for researcher to prepare defects free samples. Here, the processing of Epoxy/Nanoclay-MWCNT hybrid composites has been done by using homogenizer and ultrasonic techniques for complete dispersion of nanoparticles into epoxy resin. The MWCNT and nanoclay were embedded into epoxy resin in different weight fractions and mixtures were used for tensile test and hardness specimen production. The tensile modulus and tensile strength values have been calculated via tensile tests. The test result shows that tensile modulus of samples increases as the filler content increase up to certain extent but then start decreasing. Also the elongation reduces as the filler content rises in the epoxy which shows the brittleness present in the samples. Rockwell hardness on B-scale was conducted on Nanocomposite samples and found that increasing the filler content excessively does not improve hardness as much.</p>


2020 ◽  
Vol 834 ◽  
pp. 57-66
Author(s):  
Mihaela Raluca Condruz ◽  
Alexandru Paraschiv ◽  
Andreea Deutschlander ◽  
Ionel Mîndru

Mechanical properties of several composite materials were assessed in order to establish their suitability for unmanned aerial vehicle components manufacturing. The materials under evaluation consisted in E-glass fiber (satin/twill weave) impregnated with polyester, respective epoxy resin. The study was focused on two mechanical tests: low-velocity impact and tensile tests. Based on the results obtained, it was observed that configurations reinforced with twill weave presented higher tensile strength compared with satin reinforced configurations. Moreover, they presented a lower damage degree in case of impact tests. It was concluded that fabric quality has a considerable influence on the impregnation process and on the composite material mechanical properties. In the present case, the twill weave impregnated with epoxy resin can be used to manufacture small range UAV components.


2013 ◽  
Vol 592-593 ◽  
pp. 425-428
Author(s):  
Ming Hwa R. Jen ◽  
Che Kai Chang ◽  
Bo Cyuan Lin

The aims of this study are to fabricate Ti/APC-2 hybrid composite laminates with and without (W/WO) nanoparticles and investigate the mechanical properties of laminates with single-edged cracks due to both tensile and cyclic tests. The mechanical properties such as ultimate tensile strength and longitudinal stiffness of original composite laminates W/WO nanoparticles were first obtained from the static tensile tests. However, the load-displacement diagrams were plotted for the crack laminates. The constant stress amplitude tension-tension cyclic tests were conducted to receive the S-N curves and fatigue data. The ultimate strengths for both Ti/APC-2 composite laminates W/WO nanoparticles were very close at varied crack length. Ti/APC-2 cross-ply nanocomposite laminates had better fatigue resistance than that of laminates without nanoparticles. The longer the crack length is, the more their properties are reduced. Also, the values of fracture toughness of both hybrid cracked laminates W/WO nanoparticles were obtained by rule of mixtures and found acceptable. Finally, in predicting crack growth rate and residual life, instead of commonly used Paris Law for metals, the modified method was adopted for hybrid cracked laminates. The prediction is not satisfactorily acceptable, even if most results are in good agreement with empirical data.


2012 ◽  
Vol 535-537 ◽  
pp. 2499-2502
Author(s):  
X. Wang ◽  
S. R. Zheng ◽  
R. M. Wang

Epoxy resin structural adhesives modified by flexible curing agent. Dependening on the mechanical properties of epoxy resins on the flexible curing agent content was studied. The impact fracture toughness was discussed in terms of fracture surface fractography.


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