scholarly journals Comparative Study on the Impact Wedge-Peel Performance of Epoxy-Based Structural Adhesives Modified with Different Toughening Agents

Polymers ◽  
2020 ◽  
Vol 12 (7) ◽  
pp. 1549
Author(s):  
Gyeong-Seok Chae ◽  
Hee-Woong Park ◽  
Jung-Hyun Lee ◽  
Seunghan Shin

Epoxy adhesives are widely used in various industries because of their high heat and chemical resistance, high cohesion, and minimal shrinkage. Recently, epoxy adhesives have been applied in the automotive industry as structural adhesives for lightweight vehicles. However, the brittleness of the epoxy is an obstacle for this application, since the automotive industry requires epoxy-based structural adhesives to have a high level of high-speed impact resistance. Hence, we used phenol-terminated polyurethane (PTPU) as a toughening agent for epoxy adhesives and compared the results with those that were obtained with carboxyl-terminated butadiene acrylonitrile copolymer (CTBN). The high-energy impact resistance of the epoxy adhesives was measured by the impact wedge-peel (IWP) test, and the shear strength was measured by the single lap joint test. As a result, the 20 wt % PTPU-modified epoxy adhesive showed remarkably higher total absorbed energy (25.8 J) during the IWP test and shear strength (32.3 MPa) as compared with the control epoxy adhesive (4.1 J and 20.6 MPa, respectively). In particular, the total absorbed energy of the PTPU-modified epoxy adhesive was much larger than that of the CTBN-modified epoxy adhesive (5.8 J). When more than 10 wt % PTPU was added, the modified epoxy adhesives showed stable crack growth and effectively transferred external stress to the substrate. These results were explained by changes in the glass transition temperature, crosslinking density, and morphology due to the toughening agents.

1994 ◽  
Vol 04 (C8) ◽  
pp. C8-771-C8-776 ◽  
Author(s):  
J. L. Lataillade ◽  
D. Grapotte ◽  
F. Cayssials

2018 ◽  
Vol 244 ◽  
pp. 01019
Author(s):  
Jakub Szabelski

The aim of this study was to determine the impact of the incorrect mix ratio on the strength of joints bonded with a commercial epoxy adhesive compo-sition. The performance of cold-cured as well as accelerated cured butt joints was monitored at elevated temperature conditions. The obtained data was subjected to statistical analysis to show the correlation between joint strength at high temperature and incorrect mix ratio. The degradation of adhesive material properties with increase of hardener ratio in adhesive material was observed, as well as the change in failure type from mixed type to clearly cohesive (for inadequate volume of harde-ner) or adhesive (for excessive amount of hardener). Surprisingly insufficiency of hardener doesn’t affect the strength of joint in such manner. General recommend-dation were drawn for the preparation of two-component epoxy adhesives for joints to be used in elevated temperature, particularly when uncertainty regarding the correct resin/hardener mix ratio and future research was planned.


Author(s):  
Ali A. Heravi ◽  
Oliver Mosig ◽  
Ahmed Tawfik ◽  
Manfred Curbach ◽  
Viktor Mechtcherine

The ductile behavior of strain hardening cement-based composites (SHCC) under direct tensile load makes them promising solutions for applications where high energy dissipation is needed, such as earthquake, impact by a projectile, or blast. However, the superior tensile ductility of SHCC due to multiple cracking does not necessarily entail compressive and shear ductility. As an effort to characterize the behavior of SHCC under impact compressive and shear loading, relevant to the mentioned high-speed loading scenarios, the paper at hand studies the performance of a SHCC and its constituent cement-based matrices using the split-Hopkinson bar method. For compression experiments, cylindrical specimens with a length-to-diameter ratio (l/d) of 1.6 were used. The selected length of the sample led to similar failure modes under the quasi-static and impact loading conditions, which was necessary for a reliable comparison of the obtained compressive strengths. The impact experiments were performed in a split-Hopkinson pressure bar (SHPB) at a strain rate that reached 110 s-1 at the moment of failure. For shear experiments, a special adapter was developed for a split-Hopkinson tension bar (SHTB). The adapter enabled performing impact shear experiments on planar specimens using the tensile wave generated in the SHTB. Results showed a dynamic increase factor (DIF) of 2.3 and 2.0 for compressive and shear strength of SHCC, respectively. As compared to the non-reinforced constituent matrix, the absolute value of the compressive strength was lower for the SHCC. Contrarily, under shear loading, the SHCC yielded the higher shear strength than the non-reinforced matrix.


Author(s):  
Prayers Roy ◽  
Shaker A. Meguid

Abstract In this paper, we examine the energy absorption and containment capabilities of a newly proposed dual-ring design accounting for interactions between a released blade and fully bladed fan disk using 3D finite element analysis. The components of this dual-ring design are strategically selected to ensure high energy absorption and high impact resistance, thus leading to reduced damage of the disk and increased safety. Three containment ring designs are examined: (i) conventional single-ring design composed of one of titanium, aluminum or Kevlar, (ii) a newly proposed aluminium-Kevlar dual-ring arrangement, and (iii) dual-ring arrangement with an interfacial gap between them to arrest and contain the released blade and ensure free passage of the trailing blades. The results of our numerical simulations indicate that although the single-ring design resists penetration and contains the released blade within the confines of the disk, it does not remove the released blade from the path of the trailing blades leading to severe damage to the fan disk. On the contrary, our new dual-ring design, which contains an interfacial gap, has potential to successfully arrest the released blade within the confines of the ring and out of the path of the trailing blades. This design significantly can reduce the impact damage to the fan disk and reduces kinetic energy of the released blade to near zero in less than half a rotation of the fan disk.


2002 ◽  
Vol 124 (4) ◽  
pp. 374-378 ◽  
Author(s):  
C. M. Lawrence Wu ◽  
Robert K. Y. Li ◽  
N. H. Yeung

Isotropic conductive adhesives (ICA) have been considered as replacement materials for lead-tin solder alloys. In this paper, the post-impact shear strength of ICA surface mount (SM) joints was obtained experimentally and compared with that of SM lead-tin joints. The dynamic impact energy was provided in the form of three-point bending on the PCB using equipment called the split Hopkinson bar. Strain rates of over 4000/s were used for the impact bending test. The action of impact bending was used to simulate the effect on the PCB and the interconnection as a result of high energy impact on an electronic equipment. Shear test was then performed to examine the change in strength of the ICA joints as a result of impact damage. It was found that the SM ICA joints failed due to impact at a strain rate just over 4000/s. Microstructural examination carried out using a scanning electron microscope revealed that the interface between the ICA and copper pad on the PCB was the weakest region of the joint.


2020 ◽  
Vol 11 (4) ◽  
pp. 423-447 ◽  
Author(s):  
Hiroki Tamai ◽  
Sota Jinkawa ◽  
Yoshimi Sonoda

Medium-density polyethylene pipe has been widely introduced to low-pressure gas pipes because of its high flexibility and corrosion resistance. However, many third-party damages due to the impact of heavy equipment have been reported during the construction every year, thus, to prevent the third-party damage, materials such as high-density polyethylene and polyamide have been considered as the new gas pipe candidates. However, their impact resistance capacity under the third-party attack has not been clarified. In this study, static and impact loading experiments were conducted to compare load resistance capacities. As a result, it was revealed that the high-density polyethylene pipe and the polyamide pipe had higher static load capacity and impact resistance than the medium-density polyethylene pipe. By comparing the absorbed energy of the static test and the impact test and calculating the pseudo absorbed energy of the impact test, the evaluation formula judging the safer side of whether the penetration occurred was proposed. Furthermore, as one of the methods to protect the gas pipe, the protective effect of winding a sheet made of reinforced fiber and non-woven fabric was clarified.


2020 ◽  
Vol 23 (16) ◽  
pp. 3446-3455
Author(s):  
Yuyan Sun ◽  
Sheng Wang ◽  
Ziguo Wang

The brick-and-mortar microstructure of nacre is usually considered as a source of inspiration for the development of strong and tough artificial materials. In this article, a nacre-inspired layered-and-staggered structural building ceramic protective covering was fabricated, and the effect of four types of adhesive materials on the ballistic performance of the protective covering was investigated through the ballistic test. The experimental results showed that under the impact of the 7.62-mm ordinary rifle bullet at a speed of 790–820 m/s, the average crater diameter in the concrete targets with protective covering was reduced by 40%–72%, and the penetration depth in the concrete was reduced by 70%–100%, compared with those of unprotected concrete targets. For the concrete targets with protective covering, that adopting the silicone sealant interlayers exhibited a smaller crater area but a maximum penetration depth, while that adopting the epoxy adhesive interlayers showed a larger crater area but a minimum penetration depth. Since the targets with the low-cost polyurethane sealant interlayers presented the smallest crater area and the shallower penetration depth, it can be concluded that the concrete with the protective covering using polyurethane sealant interlayers showed the better projectile impact resistance.


2012 ◽  
Vol 626 ◽  
pp. 255-259
Author(s):  
Siti Nur Liyana Mamauod ◽  
Mohd Hanafiah Abidin ◽  
Ahmad Zafir Romli

In the present study, experiment was carried out to investigate the impact properties of flexible and rigid polymer reinforced with E-glass fiber, under low velocity impact. The experimental work includes preparing the cured glassflexible modified epoxy and placed it onto the uncured glass-epoxy composite samples. The experimental results prove that the hybridization improves the impact strength of laminates. The flexibility segments that were introduced into the epoxy system increased the penetration impact resistance value. Hence more impact energy is required to perforate the samples compared to epoxy composite system which is brittle phase.


Author(s):  
J A Harris ◽  
R D Adams

Using an instrumented impact test, the strength and energy absorption of bonded single lap joints have been measured for single lap joints with four epoxy adhesives and three aluminium alloy adherends. Compared with the static values, joint strength is not significantly affected by the high loading rates. Energy absorption is large when joint strength is sufficient for plastic deformation to occur in the adherends prior to failure, which is only the case for certain adherend/adhesive combinations. Spot welded joints are shown to be inferior in performance in the tests. The effect of loading rate on bonded joint strength has been analysed using a non-linear finite element method, from which predictions of joint strength in keeping with the experimental results have been obtained. Crush tests carried out on open-ended cylinders have been used to simulate the impact behaviour of an energy absorbing structure. Similar performance was observed for cylinders with either bonded or spot welded longitudinal seams, although the large deformations in the crumple zones led to some debonding and weld fracture.


2012 ◽  
Vol 502 ◽  
pp. 169-173
Author(s):  
Yan Qing Li ◽  
Jia Ying Sun ◽  
Wei Tian ◽  
Cheng Yan Zhu

In this paper, the low-velocity impact properties of the 3D woven composites were tested. Through the study on the relationship of absorbed energy and material structure, the impact resistance of the composites has been discussed. The research results show that the low-velocity impact resistance of quasi-orthogonal composites is the best, the low-velocity impact resistance of orthogonal composites is the worst and angle tangled of interlayer joint composites stand somewhere between the two. Adding quasi-orthogonal unit into the structure, the low-velocity impact property of the composites can be enhanced efficiently. On the other hand, if the unit distribution of the enforced fabric is changed, the break time and break point will be changed. But the effect on the total absorbed energy is not obvious.


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