scholarly journals Time-Dependent Mechanical Properties in Polyetherimide 3D-Printed Parts Are Dictated by Isotropic Performance Being Accurately Predicted by the Generalized Time Hardening Model

Polymers ◽  
2020 ◽  
Vol 12 (3) ◽  
pp. 678 ◽  
Author(s):  
A. G. Salazar-Martín ◽  
A. A. García-Granada ◽  
G. Reyes ◽  
G. Gomez-Gras ◽  
J. M. Puigoriol-Forcada
Keyword(s):  
Mechanical Properties ◽  
Stress Relaxation ◽  
Relaxation Behavior ◽  
Time Dependent ◽  
Secondary Creep ◽  
Stress Relaxation Behavior ◽  
Build Orientation ◽  
Fused Deposition ◽  
3D Printed ◽  
Generalized Time

The Fused-Deposition Modelling (FDM) technique has transformed the manufacturing discipline by simplifying operational processes and costs associated with conventional technologies, with polymeric materials being indispensable for the development of this technology. A lack of quantification of viscoelastic/plastic behavior has been noted when addressing FDM parts with Polyetherimide (PEI), which is currently being investigated as a potential material to produce functional end-products for the aerospace and health industry. Primary and secondary creep along with stress relaxation tests have been conducted on FDM PEI specimens by applying stresses from 10 to 40 MPa for 100 to 1000 min. Specimens were 3D printed by varying the part build orientation, namely XY, YZ, and XZ. Creep results were fitted to the Generalized Time Hardening equation (GTH), and then this model was used to predict stress relaxation behavior. FDM PEI parts presented an isotropic creep and stress relaxation performance. The GTH model was proven to have a significant capacity to fit viscoelastic/plastic performances for each single build orientation (r > 0.907, p < 0.001), as well as a tight prediction of the stress relaxation behavior (r > 0.998, p < 0.001). Averaged-orientation coefficients for GTH were also closely correlated with experimental creep data (r > 0.958, p < 0.001) and relaxation results data (r > 0.999, p < 0.001). FDM PEI parts showed an isotropic time-dependent behavior, which contrasts with previous publications arguing the significant effect of part build orientation on the mechanical properties of FDM parts. These findings are strengthened by the high correlation obtained between the experimental data and the averaged-coefficient GTH model, which has been proven to be a reliable tool to predict time-dependent performance in FDM parts.

Study of Printing Orientation on Mechanical Properties in Additive Manufacturing Process

2019 ◽  
Author(s):  
Peyman Honarmandi ◽  
Hongbin Xu
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Young’S Modulus ◽  
Manufacturing Process ◽  
Young's Modulus ◽  
Innovative Technology ◽  
Build Orientation ◽  
Fused Deposition ◽  
3D Printed

Abstract Additive manufacturing (AM) is an innovative technology that creates parts by adding small portions of materials layer by layer, which frees designers to create parts that were not possible to manufacture with subtractive manufacturing processes previously. This led to wide-spread popularity of 3D-printing technology. In this technology. fused deposition modeling (FDM) is the most affordable one in the market now. Therefore, it is vital to understand how the print orientation, which can be customized very easily, affects the mechanical properties of the prints to maximize the strength of the product. This paper aims to present the methodology and results of the experimental characterization of the acrylonitrile butadiene styrene (ABS) 3D-printed part. Tensile characterization of ABS was performed to analyze anisotropic nature of 3D-printed parts caused by its unique manufacturing process. Specimens were printed with six different configurations: four raster ([45/−45], [30/−60], [15/−75] and [0/90]) and three build orientations (0 or flat, 45, and 90 degrees with respect to the build plate, all printed in [45/−45] raster orientation). Dogbone tensile specimens were printed and pulled using the tensile test machine. The young’s modulus, yield strength, ultimate strength, strain at failure, breaking strength were found for each configuration. As the build orientation angle increased and the raster orientation goes from [45/−45] to [0/90], mechanical properties decreased steadily except the Young’s modulus. For build orientation, Young’s modulus decreased first then increased as angle increased, and for the raster orientation, there was no statistically significant difference as raster changed from [45/−45] to [0/90]. Overall, [45/−45] flat configuration is the strongest and the most stable configuration.

scholarly journals Interrelation between Fiber–Matrix Interphasial Phenomena and Flexural Stress Relaxation Behavior of a Glass Fiber–Polymer Composite

Polymers ◽  
2021 ◽  
Vol 13 (6) ◽  
pp. 978
Author(s):  
George C. Papanicolaou ◽  
Diana V. Portan ◽  
Lykourgos C. Kontaxis
Keyword(s):  
Stress Relaxation ◽  
Glass Fiber ◽  
Radial Distance ◽  
Relaxation Behavior ◽  
Fiber Reinforced Polymer ◽  
Time Dependent ◽  
Stress Relaxation Behavior ◽  
Reinforced Polymer ◽  
Fiber Matrix ◽  
Fiber Interaction

The response of fiber-reinforced polymer composites to an externally applied mechanical excitation is closely related to the microscopic stress transfer mechanisms taking place in the fiber–matrix interphasial region. In particular, in the case of viscoelastic responses, these mechanisms are time dependent. Defining the interphase thickness as the maximum radial distance from the fiber surface where a specific matrix property is affected by the fiber presence, it is important to study its variation with time. In the present investigation, the stress relaxation behavior of a glass fiber-reinforced polymer (GFRP) under flexural conditions was studied. Next, applying the hybrid viscoelastic interphase model (HVIM), developed by the first author, the interphase modulus and interphase thickness were both evaluated, and their variation with time during the stress relaxation test was plotted. It was found that the interphase modulus decreases with the radial distance, being always higher than the bulk matrix modulus. In addition, the interphase thickness increases with time, showing that during stress relaxation, fiber–matrix debonding takes place. Finally, the effect of fiber interaction on the interphase modulus was found. It is observed that fiber interaction depends on both the fiber–matrix degree of adhesion as well as the fiber volume fraction and the time-dependent interphase modulus.

Physical property of 3D-printed sinusoidal pattern using shape memory TPU filament

2020 ◽  
Vol 90 (21-22) ◽  
pp. 2399-2410 ◽  
Author(s):  
Shahbaj Kabir ◽  
Hyelim Kim ◽  
Sunhee Lee
Keyword(s):  
Mechanical Properties ◽  
Tensile Test ◽  
Shape Memory ◽  
Fused Deposition Modeling ◽  
Loss Modulus ◽  
Thermoplastic Polyurethane ◽  
Heating Process ◽  
Fused Deposition ◽  
3D Printed ◽  
Sinusoidal Pattern

This study has investigated the physical properties of 3D-printable shape memory thermoplastic polyurethane (SMTPU) filament and its 3D-printed sinusoidal pattern obtained by fused deposition modeling (FDM) technology. To investigate 3D filaments, thermoplastic polyurethane (TPU) and SMTPU filament were examined by conducting infrared spectroscopy, x-ray diffraction (XRD), dynamic mechanical thermal analysis (DMTA), differential scanning calorimetry (DSC) and a tensile test. Then, to examine the 3D-printed sinusoidal samples, a sinusoidal pattern was developed and 3D-printed. Those samples went through a three-step heating process: (a) untreated state; (b) 5 min heating at 70°C, cooling for 30 min at room temperature; and (c) a repeat of step 2. The results obtained by the three different heating processes of the 3D-printed sinusoidal samples were examined by XRD, DMTA, DSC and the tensile test to obtain the effect of heating or annealing on the structural and mechanical properties. The results show significant changes in structure, crystallinity and thermal and mechanical properties of SMTPU 3D-printed samples due to the heating steps. XRD showed the increase in crystallinity with heating. In DMTA, storage modulus, loss modulus and the tan σ peak position also changed for various heating steps. The DSC result showed that the Tg for different steps of the SMTPU 3D-printed sample remained almost the same at around 51°C. The tensile property of the TPU 3D-printed sinusoidal sample decreased in terms of both load and elongation with increased heating processes, while for the SMTPU 3D-printed sinusoidal sample, the load decreased but elongation increased about 2.5 times.

Effects of accelerator type on stress relaxation behavior and network structure of aged natural rubber/chloroprene rubber vulcanizates

2016 ◽  
Vol 49 (5) ◽  
pp. 381-396 ◽  
Author(s):  
Farzad A Nobari Azar ◽  
Murat Şen
Keyword(s):  
Stress Relaxation ◽  
Natural Rubber ◽  
Network Structure ◽  
Structural Changes ◽  
Relaxation Behavior ◽  
Stress Relaxation Behavior ◽  
Rubber Blends ◽  
Chloroprene Rubber ◽  
Weather Changes ◽  
Behavior Network

Natural rubber/chloroprene rubber (NR/CR) blends are among the commonly used rubber blends in industry and continuously are exposed to severe weather changes. To investigate the effects of accelerator type on the network structure and stress relaxation of unaged and aged NR/CE vulcanizates, tetramethyl thiuram disulfide, 2-mercaptobenzothiazole, and diphenyl guanidine accelerators have been chosen to represent fast, moderate, and slow accelerator groups, respectively. Three batches have been prepared with exactly the same components and mixing conditions differing only in accelerator type. Temperatures scanning stress relaxation and pulse nuclear magnetic resonance techniques have been used to reveal the structural changes of differently accelerated rubber blends before and after weathering. Nonoxidative thermal decomposition analyses have been carried out using a thermogravimetric analyzer. Results indicate that there is a strong interdependence between accelerator type and stress relaxation behavior, network structure, cross-linking density, and aging behavior of the blends. Accelerator type also affects decomposition energy of the blends.

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