scholarly journals Adhesion Performance and Recovery of Acrylic PSA with Acrylic Elastomer (AE) Blends via Thermal Crosslinking for Application in Flexible Displays

Polymers ◽  
2019 ◽  
Vol 11 (12) ◽  
pp. 1959 ◽  
Author(s):  
Jung-Hun Lee ◽  
Gyu-Seong Shim ◽  
Hyun-Joong Kim ◽  
Youngdo Kim
Keyword(s):  
Crosslinking Agent ◽  
Peel Strength ◽  
Mechanical Analysis ◽  
Pressure Sensitive Adhesive ◽  
Flexible Display ◽  
Flexible Displays ◽  
Adhesion Properties ◽  
Pressure Sensitive ◽  
Thermal Crosslinking ◽  
Adhesion Performance

Acrylic pressure-sensitive adhesive (PSA) is used to fix each layer of a flexible display. Acrylic PSA needs to satisfy specific elongation and recovery requirements so that reliability of the flexible display can be achieved. For this reason, we aimed to design an acrylic PSA/acrylic elastomer (AE) blend and to study how some viscoelastic and adhesion properties are influenced by the AE content into the mixed, blended system. Samples were characterized by UV–Vis spectrophotometry for transmittance, texture analysis for adhesion performances, and dynamic mechanical analysis (DMA) for recovery and viscoelasticity. When acrylic PSA/AE was simply blended, the adhesion performance changed due to the influence of the long molecular chains of AE. Based on this result, the AE content was fixed at 10 wt %, and acrylic PSA prepolymer was crosslinked at different concentrations of crosslinking agent. Peel strength and probe tack decreased as the concentration of crosslinking agent increased, as reported in previous studies. On the other hand, as the content of the crosslinking agent increased, recovery characteristics were improved. Additionally, as the content of the crosslinking agent increased, the storage modulus also increased, although the glass-transition temperature was not affected. According to these findings, we successfully proved the possibility of using AE to adjust adhesion performance and recovery of acrylic PSA for designing flexible displays.

scholarly journals Adhesion Properties of Acrylonitrile-Butadiene Rubber/Standard Malaysian Rubber Blend Based Pressure-Sensitive Adhesive

2014 ◽  
Vol 2014 ◽  
pp. 1-6 ◽  
Author(s):  
B. T. Poh ◽  
J. Lamaming ◽  
G. S. Tay
Keyword(s):  
Shear Strength ◽  
Peel Strength ◽  
Coated Sample ◽  
Butadiene Rubber ◽  
Pressure Sensitive Adhesive ◽  
Adhesion Properties ◽  
Pressure Sensitive ◽  
Poly Ethylene ◽  
Pet Film ◽  
Peel Tests

Viscosity and adhesion properties of NBR/SMR L blend based pressure-sensitive adhesive were investigated using coumarone-indene resin, toluene, and poly(ethylene terephthalate) (PET) as tackifier, solvent, and coating substrate, respectively. Coumarone-indene resin content was fixed at 40 parts per hundred parts of rubber (phr) in the adhesive formulation. The ratio of NBR/SMR L blend used was 0, 20, 40, 60, 80, and 100% of NBR content. Four different thicknesses, that is, 30, 60, 90, and 120 µm, were used to coat the PET film. The viscosity of adhesive was determined by a Brookfield viscometer, whereas loop tack, peel strength, and shear strength were measured using a Lloyd Adhesion Tester operating at 30 cm/min. Result indicates that the viscosity, loop tack, and shear strength of blend adhesives increase with % NBR. However, for peel strength, it indicates a maximum at 40% NBR blend ratio for the three modes of peel tests. In all cases, 120 µm coated sample consistently exhibits the highest adhesion values compared to the other coating thicknesses, an observation which is associated with the higher volume of adhesive in the former system.

scholarly journals Active Bio-Based Pressure-Sensitive Adhesive Based Natural Rubber for Food Antimicrobial Applications: Effect of Processing Parameters on Its Adhesion Properties

Polymers ◽  
2021 ◽  
Vol 13 (2) ◽  
pp. 199
Author(s):  
Theerarat Sengsuk ◽  
Ponusa Songtipya ◽  
Ekwipoo Kalkornsurapranee ◽  
Jobish Johns ◽  
Ladawan Songtipya
Keyword(s):  
Natural Rubber ◽  
Shelf Life ◽  
Aluminum Foil ◽  
Processing Parameters ◽  
Main Process ◽  
Pressure Sensitive Adhesive ◽  
Cinnamon Oil ◽  
Adhesion Properties ◽  
Pressure Sensitive ◽  
Process Factors

A novel active bio-based pressure-sensitive adhesive incorporating cinnamon oil (Bio-PSA/CO) obtained from the mixture of natural rubber (NR), xyloglucan (XG), and cinnamon oil (CO) for food antimicrobial applications were successfully developed by using a two-roll mill mixer. The effect of the main process factors (i.e., nip gap and mastication time) and XG content on the adhesion properties of the obtained PSA were investigated with different coated substrates including kraft paper, nylon film, polypropylene (PP) film, and aluminum foil (Al). The results suggested that the developed NR-PSA/CO could be applied well to all types of substrate materials. Peel strength and shear strength of the NR-PSA/CO with all substrate types were in the ranges of ~0.03 × 102–5.64 × 102 N/m and ~0.24 × 104–9.50 × 104 N/m2, respectively. The proper processed condition of the NR-PSA/CO was represented with a nip gap of 2 mm and a mastication time of 15 min. An increase in XG content up to 40–60 phr can improve the adhesion properties of the adhesive. The resulting material could be used as an active sticky patch to extend the shelf-life of food in a closed packaging system. The shelf-life of the food samples (banana cupcake) could be extended from 4 to 9 days with NR-PSA/CO patch.

Formulation and Evaluation of Quetiapine Loaded Pressure Sensitive Adhesive Patch for Transdermal Drug Delivery

2021 ◽  
pp. 2535-2539
Author(s):  
Milan B. Agrawal ◽  
Mayur M. Patel
Keyword(s):  
Ex Vivo ◽  
Research Work ◽  
Physicochemical Characterization ◽  
Oral Formulation ◽  
Peel Strength ◽  
Pressure Sensitive Adhesive ◽  
Promising Alternative ◽  
Permeability Enhancement ◽  
Pressure Sensitive ◽  
Adhesive Patch

The present research work was intended to develop and characterize the transdermal adhesive patch of quetiapine using different types of acrylate, polyisobutylene and silicon adhesives. Various permeation enhancers such as 1, 8 – cineole, D-limonene, Azone, IPM and Oleic acid were also evaluated to achieve desired permeation rate and hence to attain the improved bioavailability of quetiapine as compared to oral formulation. Formulations prepared were evaluated for physicochemical characterization, permeability enhancement potential by ex vivo, and stability studies. The results of the optimized formulation showed peel strength of 423 ± 4.13 cN/cm, flux of 54.92 ± 0.79 (µg/h/cm2) and % drug content of 98.16 ± 0.43% which was stable up to six months in accelerated condition. The results of the study revealed that the developed transdermal patch of quetiapine can be a promising alternative which provides effective management of schizophrenia in terms of improved patient compliance and reduced dosage frequency.

PEEL ADHESION PROPERTIES OF AIR-DRIED PHARMACEUTICAL PRESSURE SENSITIVE ADHESIVE

1999 ◽  
Vol 17 (10) ◽  
pp. 2093-2106
Author(s):  
N.M. Panagiotou ◽  
G. Bamopoulos ◽  
A.K. Stubos ◽  
P. Patsilinacos ◽  
Z.B. Maroulis
Keyword(s):  
Pressure Sensitive Adhesive ◽  
Adhesion Properties ◽  
Pressure Sensitive ◽  
Peel Adhesion

scholarly journals Tacky-Free Polyurethanes Pressure-Sensitive Adhesives by Molecular-Weight and HDI Trimer Design

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2164
Author(s):  
Ji-Hong Bae ◽  
Jong-Chan Won ◽  
Won-Bin Lim ◽  
Byeong-Joo Kim ◽  
Ju-Hong Lee ◽  
...  
Keyword(s):  
Molecular Weight ◽  
Crosslinking Agent ◽  
Crosslinking Density ◽  
Peel Strength ◽  
Poly Ethylene Glycol ◽  
Synthetic Process ◽  
Pressure Sensitive Adhesives ◽  
Pressure Sensitive ◽  
Optimal Balance ◽  
Poly Ethylene

Polyurethane pressure-sensitive adhesives (PU-PSAs) with satisfactory tack, cohesion, and removability were newly developed through the synthetic process by reacting methylene diisocyanate, poly(ethylene glycol) (PEG), and a 1,4-butanediol chain extender based on the different HDI/HDI trimer ratios. The sticking properties of PU-PSAs depended on both the HDI/HDI trimer ratio and crosslinking-agent composition in the formulation. The molecular weight (MW) dependence of adhesion in PU-PSA was observed in the range of 1000 < Mn < 3000, suggesting that the increase in MW limits the pressure-sensitive adhesion of these samples. The differences in the crosslinking-density significantly affected the cohesion, adhesion, and tack in PU-PSA. The formulation of 50 wt.% 600PEG and 50 wt.% crosslinking-agent and an HDI/HDI trimer ratio of 1.0 led to the optimal balance between the adhesion and cohesion properties owing to the sufficient tack, high 180-peel strength, and good cohesion.

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