scholarly journals Determination of Metals Content in Wine Samples by Inductively Coupled Plasma-Mass Spectrometry

Molecules ◽  
2018 ◽  
Vol 23 (11) ◽  
pp. 2886 ◽  
Author(s):  
Justyna Płotka-Wasylka ◽  
Marcin Frankowski ◽  
Vasil Simeonov ◽  
Żaneta Polkowska ◽  
Jacek Namieśnik
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Metal Content ◽  
Limit Of Detection ◽  
Optical Emission ◽  
Emission Spectrometry ◽  
Potentially Toxic Metals ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry

Knowledge about the metal content of wine is very important, for many reasons. Depending on the element, its quantity varies in wine from ng/L to mg/L. Despite the fact that metals are not directly connected to the taste and aroma of the wine, their content should be determined and controlled, because excess is undesirable, and in some cases prohibited, due to potential toxicity. Several analytical procedures for metal determination are applied. However, due to sensitivity, low limit of detection and speed of analysis, inductively coupled plasma-mass spectrometry (ICP-MS) is one of the most frequently used techniques. The aim of this study was to reveal specific relationships between the wine samples or between the chemical variables in order to classify the wines according to their metal content by application of chemometric analysis. For metals content determination, two techniques, ICP-MS and inductively coupled plasma-optical emission spectrometry (ICP-OES), were applied. Data obtained showed that none of the wine samples surpassed the toxic levels reported for metals in the literature, thus, these wines appeared to be safe as regards the risk associated with the potentially toxic metals intake. However, specific correlations between metals and specific aspects of the wines themselves have been found.

Advantages, drawbacks and applications of mixed Ar–N2 sources in inductively coupled plasma-based techniques: an overview

2014 ◽  
Vol 6 (16) ◽  
pp. 6170-6182 ◽  
Author(s):  
G. L. Scheffler ◽  
D. Pozebon
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Mixed Gas ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry ◽  
Plasma Optical Emission Spectrometry

This review deals with mixed gas Ar–N2 plasmas, highlighting advantages, limitations and applications of them in inductively coupled plasma optical emission spectrometry (ICP OES), inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) techniques, covering publications in the last three decades.

scholarly journals Multi-element analysis of Macedonian wines by inductively coupled plasma–mass spectrometry (ICP–MS) and inductively coupled plasma–optical emission spectrometry (IP–OES) for regional classification

2013 ◽  
Vol 32 (1) ◽  
pp. 265 ◽  
Author(s):  
Violeta Ivanova-Petropulos ◽  
Helmar Wiltsche ◽  
Trajče Stafilov ◽  
Marina Stefova ◽  
Herber Motter ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Inductively Coupled Plasma ◽  
Accurate Determination ◽  
Optical Emission ◽  
Optical Emission Spectrometry ◽  
Emission Spectrometry ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Plasma Mass Spectrometry ◽  
Plasma Optical Emission Spectrometry

Major, minor, and trace elements in wines from the Republic of Macedonia were determined in this study. Both inductively coupled plasma–mass spectrometry (ICP-MS) and inductively coupled plasma– optical emission spectrometry (ICP-OES) were used for accurate determination of the concentration of 42 elements (Ag, Al, Au, B, Ba, Be, Bi, Ca, Cd, Ce, Co, Cu, Dy, Er, Eu, Fe, Ga, Gd, Ge, Ho, La, Lu, Mg, Mn, Mo, Na, Nd, Ni, P, Pb, Pr, S, Sm, Tb, Ti, Tl, Tm, U, V, Yb, Zn, Zr) in 25 Macedonian white, rose, and red wines from different wine regions. By means of factor and cluster analyses, the wines were discriminated according to wine type (white vs. red) and geographical origin. The main discriminant elements were B, Ba, Ca, Fe, Mg, Mn, P, and S. 

scholarly journals P2O5-Free Cerium Containing Glasses: Bioactivity and Cytocompatibility Evaluation

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3267
Author(s):  
Gigliola Lusvardi ◽  
Francesca Sgarbi Stabellini ◽  
Roberta Salvatori
Keyword(s):  
Inductively Coupled Plasma ◽  
Optical Emission ◽  
Emission Spectrometry ◽  
X Ray Diffraction ◽  
Inductively Coupled ◽  
Icp Ms ◽  
Doped Glasses ◽  
Plasma Mass Spectrometry ◽  
Sbf Solution ◽  
Xrd Techniques

(1) Background: valuation of the bioactivity and cytocompatibility of P2O5-free and CeO2 doped glasses. (2) Methods: all glasses are based on the Kokubo (K) composition and prepared by a melting method. Doped glassed, K1.2, K3.6 and K5.3 contain 1.2, 3.6, and 5.3 mol% of CeO2. Bioactivity and cytotoxicity tests were carried out in simulated body fluid (SBF) solution and murine osteocyte (MLO-Y4) cell lines, respectively. Leaching of ions concentration in SBF was determined by inductively coupled plasma mass spectrometry (ICP-MS) and optical emission spectrometry (ICP-OES). The surface of the glasses were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD) techniques. (3) Results: P2O5-free cerium doped glasses are proactive according to European directives. Cerium increases durability and retards, but does not inhibit, (Ca10(PO4)6(OH)2, HA) formation at higher cerium amounts (K3.6 and K5.3); however, cell proliferation increases with the amount of cerium especially evident for K5.3. (4) Conclusions: These results enforce the use of P2O5-free cerium doped bioactive glasses as a new class of biomaterials.

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