Synthesis and Total 1H- and 13C-NMR Assignment of Cephem Derivatives for Use in ADEPT Approaches

Lorena Blau; Renato Menegon; Elizabeth Ferreira; Antonio Ferreira; Elisangela Boffo; Leila Tavares; Vladimir Heleno; Man-Chin Chung

doi:10.3390/molecules13040841

Synthesis and Total 1H- and 13C-NMR Assignment of Cephem Derivatives for Use in ADEPT Approaches

Molecules ◽

10.3390/molecules13040841 ◽

2008 ◽

Vol 13 (4) ◽

pp. 841-854 ◽

Cited By ~ 3

Author(s):

Lorena Blau ◽

Renato Menegon ◽

Elizabeth Ferreira ◽

Antonio Ferreira ◽

Elisangela Boffo ◽

...

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

1H And 13C Nmr

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1H and 13C NMR assignment of benzothiophenquinones from the sulfur-oxidizing archaebacterium Sulfolobus solfataricus

European Journal of Biochemistry ◽

10.1111/j.1432-1033.1986.tb09936.x ◽

1986 ◽

Vol 160 (1) ◽

pp. 37-40 ◽

Cited By ~ 15

Author(s):

Virginia LANZOTTI ◽

Antonio TRINCONE ◽

Agata GAMBACORTA ◽

Mario ROSA ◽

Eberhard BREITMAIER

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

Sulfolobus Solfataricus ◽

1H And 13C Nmr ◽

Sulfur Oxidizing

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ChemInform Abstract: The 1H and 13C NMR Assignment of 4-Oxo-1,4-dihydro-3′-methylsulfinyl-3,4′-diquinolinyl Sulfides and Their 6- and 8-Nitro and 1-Methyl Derivatives.

ChemInform ◽

10.1002/chin.199830027 ◽

2010 ◽

Vol 29 (30) ◽

pp. no-no

Author(s):

M. J. MASLANKIEWICZ

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

1H And 13C Nmr ◽

Methyl Derivatives

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ChemInform Abstract: Complete 1H- and 13C-NMR Assignment of Polycyclic Aromatic Fluoranthenes by Long-Range Optimized Homo- and Heteronuclear Correlation Spectroscopy.

ChemInform ◽

10.1002/chin.198821051 ◽

1988 ◽

Vol 19 (21) ◽

Author(s):

B. P. CHO ◽

R. G. HARVEY

Keyword(s):

Long Range ◽

13C Nmr ◽

Nmr Assignment ◽

Correlation Spectroscopy ◽

1H And 13C Nmr ◽

Heteronuclear Correlation ◽

Polycyclic Aromatic ◽

Heteronuclear Correlation Spectroscopy

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Complete 1H and 13C NMR assignment of digeneaside, a low-molecular-mass carbohydrate produced by red seaweeds

Carbohydrate Research ◽

10.1016/j.carres.2006.01.002 ◽

2006 ◽

Vol 341 (5) ◽

pp. 677-682 ◽

Cited By ~ 31

Author(s):

Sérgio D. Ascêncio ◽

Alexandre Orsato ◽

Robson A. França ◽

M. Eugênia R. Duarte ◽

Miguel D. Noseda

Keyword(s):

Molecular Mass ◽

13C Nmr ◽

Nmr Assignment ◽

1H And 13C Nmr ◽

Red Seaweeds

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A new Precursor for the Radiosynthesis of 6-O-(2-[18F]Fluoroethyl)-6-O-desmethyl-diprenorphine ([18F]FE-DPN) by Nucleophilic Radiofluorination

Letters in Organic Chemistry ◽

10.2174/1570178617999200719153812 ◽

2020 ◽

Vol 17 ◽

Author(s):

János Marton ◽

Paul Cumming ◽

Beate Bauer ◽

Gjermund Henriksen

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

Reference Standard ◽

One Pot ◽

1H And 13C Nmr ◽

Alternative Synthesis ◽

Synthesis Routes

: We present the preparation of the new precursor 6-O-(2-tosyloxyethoxy)-6-O-desmethyl-3-O-trityl-diprenorphine (TE-TDDPN) for a one-pot, two step nucleophilic radiosynthesis of 6-O-(2-[ 18F]fluoroethyl-6-O-desmethyl-diprenorphine ([18F]FE-DPN). The route to the precursor consists of a five-step synthesis starting from diprenorphine. We also provide alternative synthesis routes for the cold reference standard and the complete 1H- and 13C-NMR assignment of the prepared derivatives.

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ChemInform Abstract: Complete 1H and 13C NMR Assignment of Balearone by 2D NMR Spectroscopy.

ChemInform ◽

10.1002/chin.199152284 ◽

2010 ◽

Vol 22 (52) ◽

pp. no-no

Author(s):

V. AMICO ◽

M. PIATTELLI ◽

P. NERI ◽

M. RECUPERO

Keyword(s):

Nmr Spectroscopy ◽

13C Nmr ◽

Nmr Assignment ◽

2D Nmr ◽

2D Nmr Spectroscopy ◽

1H And 13C Nmr

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Confirmation and complete 1H and 13C NMR assignment of the structure of peptidoglycan from Sarcina ventriculi, a highly adaptable Gram-positive bacterium

Carbohydrate Research ◽

10.1016/s0008-6215(97)00133-x ◽

1997 ◽

Vol 303 (1) ◽

pp. 103-112 ◽

Cited By ~ 2

Author(s):

Jeongrim Lee ◽

Rawle I. Hollingsworth

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

Positive Bacterium ◽

Gram Positive ◽

1H And 13C Nmr ◽

Sarcina Ventriculi

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Complete 1H and 13C NMR assignment of mono-sulfated galactosylceramides with four types of ceramides from human kidney

Carbohydrate Research ◽

10.1016/s0008-6215(99)00291-8 ◽

2000 ◽

Vol 324 (3) ◽

pp. 218-222 ◽

Cited By ~ 8

Author(s):

Naoko Iida-Tanaka ◽

Ineo Ishizuka

Keyword(s):

13C Nmr ◽

Nmr Assignment ◽

Human Kidney ◽

1H And 13C Nmr

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1H and 13C NMR Assignment of Regioirregular Sequence in Poly((S)-(−)-propylene oxide) Prepared with Organotin-Alkyl Phosphate Condensate by 2D NMR Technique

Polymer Journal ◽

10.1295/polymj.25.697 ◽

1993 ◽

Vol 25 (7) ◽

pp. 697-705 ◽

Cited By ~ 3

Author(s):

Katsuhito Miura ◽

Tatsuki Kitayama ◽

Koichi Hatada ◽

Tetsuya Nakata

Keyword(s):

Propylene Oxide ◽

13C Nmr ◽

Nmr Assignment ◽

2D Nmr ◽

1H And 13C Nmr ◽

Alkyl Phosphate

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1,3-Oxazepane-4,7-Diones Compounds: 1H and 13C NMR High-Resolution Spectroscopy (1D and 2D)

International Journal of Spectroscopy ◽

10.1155/2011/945216 ◽

2011 ◽

Vol 2011 ◽

pp. 1-7 ◽

Cited By ~ 2

Author(s):

AbdulKarim-Talaq Mohammad ◽

Hasnah Osman ◽

Guan-Yeow Yeap

Keyword(s):

High Resolution ◽

13C Nmr ◽

Phenyl Ring ◽

Nmr Assignment ◽

Alkyl Chain ◽

High Resolution Spectroscopy ◽

Two Dimensional ◽

1H And 13C Nmr ◽

Nmr Techniques ◽

C Nmr

The complete 1H and 13C NMR assignment of new 1,3-oxazepane-4,7-dione compounds has been obtained using one- and two-dimensional NMR techniques including COSY, HMQC, and HMBC experiments. The data deduced from this study show that the alkyl chain and the phenyl ring are in different planes compared to the oxazepine ring.

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