scholarly journals Demonstration of Optical Microscopy and Image Processing to Classify Respirable Coal Mine Dust Particles

Minerals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 838
Author(s):  
Nestor Santa ◽  
Cigdem Keles ◽  
J. R. Saylor ◽  
Emily Sarver

Respirable coal mine dust represents a serious health hazard for miners. Monitoring methods are needed that enable fractionation of dust into its primary components, and that do so in real time. Near the production face, a simple capability to monitor the coal versus mineral dust fractions would be highly valuable for tracking changes in dust sources—and supporting timely responses in terms of dust controls or other interventions to reduce exposures. In this work, the premise of dust monitoring with polarized light microscopy was explored. Using images of coal and representative mineral particles (kaolinite, crystalline silica, and limestone rock dust), a model was built to exploit birefringence of the mineral particles and effectively separate them from the coal. The model showed >95% accuracy on a test dataset with known particles. For composite samples containing both coal and minerals, the model also showed a very good agreement with results from the scanning electron microscopy classification, which was used as a reference method. Results could further the concept of a “cell phone microscope” type monitor for semi-continuous measurements in coal mines.

Minerals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 276
Author(s):  
Lei Pan ◽  
Sean Golden ◽  
Shoeleh Assemi ◽  
Marc Freddy Sime ◽  
Xuming Wang ◽  
...  

Respirable coal mine dust (RCMD) particles, particularly the nano-sized fraction (<1 μm) of the RCMD if present, can cause severe lung diseases in coal miners. Characterization of both the particle size and chemical composition of such RCMD particles remains a work in progress, in particular, with respect to the nano-sized fraction of RCMD. In this work, various methods were surveyed and used to obtain both the size and chemical composition of RCMD particles, including scanning electron microscopy (SEM), scanning transmission electron microscopy (S-TEM), dynamic light scattering (DLS), and asymmetric flow field-flow fractionation (AsFIFFF). It was found that the micron-sized fraction (>1 μm) of RCMD particles collected at the miner location, from an underground coal mine, contained more coal particles, while those collected at the bolter location contained more rock dust particles. Two image processing procedures were developed to determine the size of individual RCMD particles. The particle size distribution (PSD) results showed that a significant amount (~80% by number) of nano-sized particles were present in the RCMD sample collected in an underground coal mine. The presence of nano-sized RCMD particles was confirmed by bulk sample analysis, using both DLS and AsFIFFF. The mode particle size at the peak frequency of the size distribution was found to be 300–400 nm, which was consistent with the result obtained from SEM analysis. The chemical composition data of the nano-sized RCMD showed that not only diesel particles, but also both coal and rock dust particles were present in the nano-sized fraction of the RCMD. The presence of the nano-sized fraction of RCMD particles may be site and location dependent, and a detailed analysis of the entire size range of RCMD particles in different underground coal mines is needed.


Author(s):  
W. Dorriné ◽  
P. Van Espen ◽  
F. Adams ◽  
B. Préat

Extremely dusty working conditions are a serious health risk for coal miners. Quartz and other minerals are known to cause lung diseases when inhaled over long periods of time. In this work, a study was made of the mineral content in coal mine dust. Individual particles were characterised using computer controlled electron microprobe analysis and then classified into different mineral categories using a multivariate classification procedure.Coal mine dust particles were collected from the Zolder coal mine, Belgium, using a BAT II cyclone sampling unit. Small quantities of the dust were suspended in n-hexane using an ultrasonic water bath. Approximately 100 μl of the suspension were spotted on a plexiglass stub and dried. The excess carbon was removed by ashing the samples for two hours in a low temperature asher (LTA). The samples were coated with a carbon layer of ±40 nm for microprobe analysis. An identical sample preparation procedure was used to prepare 6 mineral standards : biotite, illite, kaolinite, quartz, muscovite and ripidolite.


Minerals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 426
Author(s):  
Behrooz Abbasi ◽  
Xiaoliang Wang ◽  
Judith C. Chow ◽  
John G. Watson ◽  
Bijan Peik ◽  
...  

Respirable coal mine dust (RCMD) exposure is associated with black lung and silicosis diseases in underground miners. Although only RCMD mass and silica concentrations are regulated, it is possible that particle size, surface area, and other chemical constituents also contribute to its adverse health effects. This review summarizes measurement technologies for RCMD mass concentrations, morphology, size distributions, and chemical compositions, with examples from published efforts where these methods have been applied. Some state-of-the-art technologies presented in this paper have not been certified as intrinsically safe, and caution should be exerted for their use in explosive environments. RCMD mass concentrations are most often obtained by filter sampling followed by gravimetric analysis, but recent requirements for real-time monitoring by continuous personal dust monitors (CPDM) enable quicker exposure risk assessments. Emerging low-cost photometers provide an opportunity for a wider deployment of real-time exposure assessment. Particle size distributions can be determined by microscopy, cascade impactors, aerodynamic spectrometers, optical particle counters, and electrical mobility analyzers, each with unique advantages and limitations. Different filter media are required to collect integrated samples over working shifts for comprehensive chemical analysis. Teflon membrane filters are used for mass by gravimetry, elements by energy dispersive X-ray fluorescence, rare-earth elements by inductively coupled plasma-mass spectrometry and mineralogy by X-ray diffraction. Quartz fiber filters are analyzed for organic, elemental, and brown carbon by thermal/optical methods and non-polar organics by thermal desorption-gas chromatography-mass spectrometry. Polycarbonate-membrane filters are analyzed for morphology and elements by scanning electron microscopy (SEM) with energy dispersive X-ray, and quartz content by Fourier-transform infrared spectroscopy and Raman spectroscopy.


Environments ◽  
2021 ◽  
Vol 8 (11) ◽  
pp. 114
Author(s):  
Jiří Bílek ◽  
Ondřej Bílek ◽  
Petr Maršolek ◽  
Pavel Buček

Sensor technology is attractive to the public due to its availability and ease of use. However, its usage raises numerous questions. The general trustworthiness of sensor data is widely discussed, especially with regard to accuracy, precision, and long-term signal stability. The VSB-Technical University of Ostrava has operated an air quality sensor network for more than two years, and its large sets of valid results can help in understanding the limitations of sensory measurement. Monitoring is focused on the concentrations of dust particles, NO2, and ozone to verify the impact of newly planted greenery on the reduction in air pollution. The sensor network currently covers an open field on the outskirts of Ostrava, between Liberty Ironworks and the nearby ISKO1650 monitoring station, where some of the worst air pollution levels in the Czech Republic are regularly measured. In the future, trees should be allowed to grow over the sensors, enabling assessment of the green barrier effect on air pollution. As expected, the service life of the sensors varies from 1 to 3 years; therefore, checks are necessary both prior to the measurement and regularly during operation, verifying output stability and overall performance. Results of the PMx sensory measurements correlated well with the reference method. Concentration values measured by NO2 sensors correlated poorly with the reference method, although timeline plots of concentration changes were in accordance. We suggest that a comparison of timelines should be used for air quality evaluations, rather than particular values. The results showed that the sensor measurements are not yet suitable to replace the reference methods, and dense sensor networks proved useful and robust tools for indicative air quality measurements (AQM).


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