scholarly journals Optimization of Operating Parameters on Dry Grinding of Calcite in a Stirred Media Mill Using the Box-Behnken Design

Minerals ◽  
2020 ◽  
Vol 10 (3) ◽  
pp. 251
Author(s):  
Diler Katircioglu-Bayel
Keyword(s):  
Mass Fraction ◽  
Filling Ratio ◽  
Operating Parameters ◽  
Stirrer Speed ◽  
Solid Mass ◽  
Optimum Conditions ◽  
Box Behnken Design ◽  
Dry Grinding ◽  
Grinding Time ◽  
Stirred Media Mill

The optimization of the operating parameters of a stirred media mill in the dry grinding of calcite was investigated. A three-level Box-Behnken design was used for the purpose of examining the impact of four independent factors, the stirrer speed (SS), grinding time (GT), media filling ratio (MFR), and solid mass fraction (SMF), on the product particle size (d50). For the purpose of establishing an empirical correlation between operating parameters and responses, a series of experiments were carried out. Variance analysis showed a reasonably good value for d50 (R2 = 0.965). According to the software solutions, the optimum conditions for minimizing the d50 size were found to be 573 rpm stirrer speed, 11.18 min grinding time, 63% media filling ratio, and 11.52% solid mass fraction, with 3.78 µm for the d50 size. To verify the improvement of grinding, verification tests were performed using the above-mentioned optimum conditions and the average d50 size and standard deviation were found to be 3.83 µm and 0.025, respectively. The average d50 value obtained was smaller than those obtained in the 27 tests. Furthermore, when the optimum result obtained from the experiments was compared with the result obtained using the software, a 22% energy saving was achieved. The impacts of grinding on the structural characteristics of calcite particles were characterized by XRD analysis. XRD measurements indicated that no change was observed in the peak areas of ground calcite specimens compared to the untreated calcite specimen.

The effect of operating parameters on the performance of a biosand filter: a statistical experiment design approach

2015 ◽  
Vol 16 (3) ◽  
pp. 775-782 ◽  
Author(s):  
Krutika Rajesh Tundia ◽  
M. Mansoor Ahammed ◽  
Duithy George
Keyword(s):  
Pore Volume ◽  
Microbiological Quality ◽  
Pause Time ◽  
Operating Parameters ◽  
Optimum Conditions ◽  
Box Behnken Design ◽  
Biosand Filter ◽  
Bacterial Removal ◽  
The Ideal

The influence of three important parameters, namely, pause time, charge volume and influent turbidity on the performance of a biosand filter (BSF) was assessed by employing response surface methodology with a Box-Behnken design. Fifteen runs were conducted in triplicate using a full-scale BSF with a pore volume of 19.6 L, and the performance of the filter was assessed by monitoring total coliforms, Escherichia coli and turbidity of the effluent. Results showed that there was a significant improvement in the microbiological quality of filtered water when the pause time was increased from 12 to 36 h, while it deteriorated as charge volume was increased from 10 to 30 L. The effluent microbiological quality was unaffected by changes in the influent turbidity in the range of 10–50 NTU. Further, effluent turbidity was not significantly affected by the changes in any of the operating parameters, and it remained below 1.5 NTU in all the runs. At optimum conditions of pause time 23 h, charge volume 19.4 L and influent turbidity 32 NTU, bacterial removal exceeded 99.4%. The results show that charging of the filter with about one pore volume of water once a day would be the ideal operating strategy for a BSF.

Decolorization of Reactive Black 5 using Peroxymonosulfate in Fentonlike Process

2013 ◽  
Vol 16 (2) ◽  
Author(s):  
Gülin Ersöz ◽  
Süheyda Atalay
Keyword(s):  
Advanced Oxidation Processes ◽  
Catalytic Effect ◽  
Industrial Effluents ◽  
Operating Parameters ◽  
Reactive Black 5 ◽  
Process Performance ◽  
Optimum Conditions ◽  
Oxidation Processes ◽  
Wide Availability ◽  
Initial Ph

AbstractOne of the advanced oxidation processes, the Oxone process, was studied to determine its effects on the decolorization of Reactive Black 5 (RB5) in an aqueous solution. Ferrous ion was chosen as the transition metal due to its potential catalytic effect and wide availability in dye containing industrial effluents. The effects of the operating parameters such as Fe(II) and Oxone concentration, initial pH, and temperature on the process performance were investigated. The optimum conditions were determined as: 0.5 mM of Oxone concentration, 0.5 mM of Fe

Lipase Acrylic Resin Catalyzed Interesterification of Sewage Sludge in Micro Packed Bed Reactor: Box-Behnken Design

2020 ◽  
Vol 870 ◽  
pp. 81-96
Author(s):  
Ali A. Jazie ◽  
Riyam Imad Jaddan ◽  
Mohamed F. Al-Dawody ◽  
Suhad A. Abed
Keyword(s):  
Enzyme Activity ◽  
Sewage Sludge ◽  
Ethyl Acetate ◽  
Acrylic Resin ◽  
Packed Bed ◽  
Biodiesel Production ◽  
Packed Bed Reactor ◽  
Heating Process ◽  
Optimum Conditions ◽  
Box Behnken Design

Ethyl acetate as acyl accepter have been used for sewage sludge biodiesel production in micro packed bed reactor. Lipase acrylic resin enzyme activity was investigated in the interesterification reaction of converting the sewage sludge into a biodiesel product. The main parameters affecting the process was adjusted via the design of Box-Behnken and approach of response surface then the optimum conditions were as follow (reaction time=15 h, ethyl acetate/oil ratio=24:1, temperature=40 °C and enzyme quantity=18 wt%) providing 95.78 % biodiesel yield. The lipase acrylic resin was examined under the optimum conditions for the reusability. the flow effect and the heating process of the micro packed bed reactor was investigated. The product biodiesel physicochemical properties were evaluated according to the ASTM D-6751-2 and found acceptable comparable to the mineral diesel properties.

scholarly journals Optimization of Insoluble and Soluble Fibres Extraction fromAgave americanaL. Using Response Surface Methodology

2014 ◽  
Vol 2014 ◽  
pp. 1-13 ◽  
Author(s):  
Amine Bouaziz ◽  
Manel Masmoudi ◽  
Amel Kamoun ◽  
Souhail Besbes
Keyword(s):  
Ionic Strength ◽  
Design Methodology ◽  
Extraction Yield ◽  
Agitation Speed ◽  
Optimum Conditions ◽  
Box Behnken Design ◽  
Factors Affecting ◽  
Soluble Fibre ◽  
Experimental Design Methodology ◽  
Significant Factors

Experimental design methodology was used to determine significant factors affecting the extraction yield of soluble and insoluble fibres fromAgave americanaL. and in second time to find optimum conditions leading to the highest yield. Results clearly indicated that the temperature, the powder to water (P/W) ratio, and the agitation speed were the most important factors influencing fibres extraction yield which increased with temperature, P/W ratio, and agitation speed. Ionic strength affected significantly soluble fibre extraction yield and was the most important factor among nonsignificant ones influencing insoluble fibres extraction yield. Then, a Box-Behnken design was carried out to maximise fibres extraction. Selected optimal conditions were temperature: 90°C; P/W ratio: 0.1625; agitation speed: 400 rpm; and ionic strength: 1.5 g/L. These conditions yielded 93.02% and 80.46% of insoluble and soluble fibres, respectively. Concentrates showed high fibres purity and good functional properties.

Effect of Operating Parameters on the Breakage Process of Calcite in a Stirred Media Mill

2018 ◽  
Vol 36 (2) ◽  
pp. 399-408 ◽  
Author(s):  
Diler Katircioglu-Bayel ◽  
Safak Gokhan Ozkan ◽  
Oner Yusuf Toraman
Keyword(s):  
Operating Parameters ◽  
Stirred Media Mill

scholarly journals Investigation on geothermal binary-flashing cycle employing zeotropic mixtures as working fluids

2019 ◽  
Vol 7 (1) ◽  
Author(s):  
Lingbao Wang ◽  
Xianbiao Bu ◽  
Huashan Li
Keyword(s):  
Global Warming ◽  
Heat Exchanger ◽  
Performance Improvement ◽  
Mass Fraction ◽  
Superior Performance ◽  
Operating Parameters ◽  
Exergy Destruction ◽  
Environmental Friendliness ◽  
Evaluation Indexes ◽  
Net Power Output

AbstractThe binary-flashing cycle (BFC) is supposed to be a promising technology for geothermal recovery due to the full use of geofluid. For further performance improvement, the potential of using mixtures of a hydrocarbon and a retardant in the BFC system is investigated. R245fa is selected as a retardant and blended with R600 to form zeotropic mixtures. With the thermal efficiency (ηth), exergy efficiency (ηex), net power output per ton geofluid (PRW), and exergy destruction rate (Ed) as evaluation indexes, the flowsheet modeling and optimization are conducted to explore the optimal compositions and operating parameters. It is revealed the optimal mass fraction of R600/R245fa is 0.44/0.56, at which the flammability of R600 is suppressed, the global warming potential (GWP) of R245fa is reduced. The maximum ηex and PRW are higher than those of component fluids. The maximum Ed occurs in the heat exchanger, which should be optimized. The recommended generation pressures are 1200–1430, 1240–1480, 1220–1460, and 1170–1420 kPa, respectively, for R600 mass fraction of 0.2, 0.4, 0.6, and 0.8. In addition, the flashing temperature is also optimized. Although the mixtures do not always yield superior performance, it is still beneficial to apply the mixtures to the BFC system through systematic consideration of safety and environmental friendliness.

scholarly journals Optimization of Fenton Technology for Recalcitrant Compounds and Bacteria Inactivation

Catalysts ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1483
Author(s):  
Pablo Salgado ◽  
José Luis Frontela ◽  
Gladys Vidal
Keyword(s):  
Regression Coefficient ◽  
Interactive Effects ◽  
Molar Ratio ◽  
Main Process ◽  
Optimum Conditions ◽  
Box Behnken Design ◽  
E Coli ◽  
Bacteria Inactivation ◽  
The Individual ◽  
Good Agreement

In this work, the Fenton technology was applied to decolorize methylene blue (MB) and to inactivate Escherichia coli K12, used as recalcitrant compound and bacteria models respectively, in order to provide an approach into single and combinative effects of the main process variables influencing the Fenton technology. First, Box–Behnken design (BBD) was applied to evaluate and optimize the individual and interactive effects of three process parameters, namely Fe2+ concentration (6.0 × 10−4, 8.0 × 10−4 and 1.0 × 10−3 mol/L), molar ratio between H2O2 and Fe2+ (1:1, 2:1 and 3:1) and pH (3.0, 4.0 and 5.0) for Fenton technology. The responses studied in these models were the degree of MB decolorization (D%MB), rate constant of MB decolorization (kappMB) and E. coli K12 inactivation in uLog units (IuLogEC). According to the results of analysis of variances all of the proposed models were adequate with a high regression coefficient (R2 from 0.9911 to 0.9994). BBD results suggest that [H2O2]/[Fe2+] values had a significant effect only on D%MB response, [Fe2+] had a significant effect on all the responses, whereas pH had a significant effect on D%MB and IuLogEC. The optimum conditions obtained from response surface methodology for D%MB ([H2O2]/[Fe2+] = 2.9, [Fe2+] = 1.0 × 10−3 mol/L and pH = 3.2), kappMB ([H2O2]/[Fe2+] = 1.7, [Fe2+] = 1.0 × 10−3 mol/L and PH = 3.7) and IuLogEC ([H2O2]/[Fe2+] = 2.9, [Fe2+] = 7.6 × 10−4 mol/L and pH= 3.2) were in good agreement with the values predicted by the model.

Evolution of pyrophyllite particle sizes during dry grinding

Clay Minerals ◽  
2000 ◽  
Vol 35 (2) ◽  
pp. 423-432 ◽  
Author(s):  
P. Uhlík ◽  
V. Šucha ◽  
D. D. Eberl ◽  
L'. Puškelová ◽  
M. Čaplovičová
Keyword(s):  
Size Distribution ◽  
Thickness Distribution ◽  
Particle Sizes ◽  
Transmission Electron ◽  
Lognormal Size Distribution ◽  
Dry Grinding ◽  
Time And Energy ◽  
Grinding Time ◽  
Crystallite Thickness ◽  
Number Of Particles

AbstractThe Bertaut-Warren-Averbach (BWA) technique and high-resolution transmission electron microscopy (HRTEM) were used to characterize the products of dry-ground pyrophyllite. Mean crystallite thickness and crystallite thickness distributions were measured for each sample using the BWA technique. Mean crystallite thickness decreases during the treatment with respect to grinding time and energy applied per unit mass. The BWA data were checked by HRTEM measurements and good fits were obtained for samples having small mean particle thicknesses. Samples with thicker particles could not be measured properly by HRTEM because the number of particles counted from images is statistically insufficient. The shape of the crystallite and the particle-size distribution were used to determine the mechanism of pyrophyllite particle degradation. Particles initially having a lognormal size distribution are first delaminated randomly, then some are delaminated preferentially, thereby producing polymodal thickness distributions. Finally all particles undergo delamination yielding a lognormal thickness distribution.

A New Technological Study on Synthesis of Bis(2-chloroethoxy)Methane

2014 ◽  
Vol 1033-1034 ◽  
pp. 7-11
Author(s):  
Yan Bai ◽  
Xuan Tang ◽  
Kui Zhou ◽  
Cun She Zhang
Keyword(s):  
Mass Fraction ◽  
Acid Catalysis ◽  
Molar Ratio ◽  
Optimum Conditions ◽  
Reaction Conditions ◽  
Ethylene Chlorohydrin ◽  
Optimum Reaction ◽  
Chromatographic Detection ◽  
Catalyst Dosage ◽  
Technological Study

bis(2-chloroethoxy)methane was synthesized by the reaction of ethylene chlorohydrin and Oligopolyformaldehyde under sulfuric acid catalysis. optimum reaction conditions obtained were as follows: the molar ratio of Oligopolyformaldehyde and ethylene chlorohydrin of 1.2:2, catalyst dosage was 5‰mass fraction of ethylene chlorohydrin, toluene were chose as water-carrying agent, All reactant were refluxed on temperature of 110°C until no water generated. Under the optimum conditions the yield of bis(2-chloroethoxy)methane was 97.7%. The structure of bis(2-chloroethoxy)methane were conformed by ATR IR. The purity of bis(2-chloroethoxy)methane were 99% by gas chromatographic detection.

scholarly journals Optimization of process variables for phyllanthin extraction from Phyllanthus amarus leaves by supercritical fluid using a Box-Behnken experimental design followed by HPLC identification

2013 ◽  
Vol 63 (2) ◽  
pp. 193-207 ◽  
Author(s):  
Ajit A. Patil ◽  
Sachin S. Bhusari ◽  
Devanand B. Shinde ◽  
Pravin S. Wakte
Keyword(s):  
Carbon Dioxide ◽  
Hplc Analysis ◽  
Extraction Time ◽  
Phyllanthus Amarus ◽  
Process Variables ◽  
Optimum Conditions ◽  
Box Behnken Design ◽  
Assisted Extraction ◽  
Predicted Values ◽  
Good Agreement

The response surface methodology using the Box-Behnken design was established to describe supercritical carbon dioxide assisted extraction of phyllanthin from Phyllanthus amarus Schum and Thonn leaves prior to HPLC analysis. The effects of extraction pressure, temperature, modifier concentration and extraction time on the yield of phyllanthin were investigated. By solving the regression equation, the optimum conditions were as follows: extraction pressure 23.2 MPa, temperature 40 °C, methanol as modifier at a concentration of 10 % and time 90 min. Under these conditions, the phyllanthin yield was 12.83 ± 0.28 mg g-1, which was in good agreement with the predicted values. Modifier concentration and extraction time showed a significant effect on the phyllanthin yield.

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