scholarly journals Research on a Micro-Processing Technology for Fabricating Complex Structures in Single-Crystal Quartz

Micromachines ◽  
2020 ◽  
Vol 11 (3) ◽  
pp. 337 ◽  
Author(s):  
Chao Han ◽  
Cun Li ◽  
Yulong Zhao ◽  
Bo Li ◽  
Xueyong Wei

Single-crystal quartz material is widely applied in the manufacture of resonators and sensors, but it is difficult to process because of its high hardness. A novel way to fabricate single-crystal quartz structures is proposed in this paper; the method includes quartz-on-silicon (QoS) technology and inductively coupled plasma (ICP) etching, which makes it feasible to fabricate complex structures with crystal quartz. The QoS method encompasses the bonding of silicon and quartz, followed by the thinning and polishing of quartz, which can enable the fabrication of an ultra-thin quartz wafer on silicon. In this way, instead of the conventional wet etching with hydrofluoric acid, the quartz layer can be easily etched using the ICP dry-etching method. Then, the structure of the pure quartz material is obtained by removing the silicon wafer. In addition, the silicon layer can be processed into the appropriate structure. This aspect overcomes the difficulty of processing a complex structure of single-crystal quartz with different crystal orientations. Thin single-crystal quartz wafers of Z-cut with a thickness of less than 40 μm were obtained by using this method, and a complex three-dimensional structure with an 80 μm width was also acquired by the ICP etching of the quartz wafer. The method can be applied to make both crystal-oriented quartz-based sensors and actuators, such as quartz resonant accelerometers.

2021 ◽  
Vol 11 (15) ◽  
pp. 6733
Author(s):  
Mira Naftaly ◽  
Andrew Gregory

Z-cut single-crystal quartz and vitreous silica (silica glass or fused silica) were evaluated for use as reference materials for terahertz and microwave measurements of complex permittivity, with Z-cut quartz confirmed as being suitable. Measurements of refractive indices and absorption coefficients for o-ray and e-ray in quartz and for vitreous silica are reported at frequencies between 0.2 and 6 THz and at 36 and 144 GHz, and compared with data reported in the literature. A previously unreported broad band was seen in the extraordinary absorption of quartz. The Boson peak in silica glass absorption was examined, and for the first time, two negative relationships have been observed: between the refractive index and the Boson peak frequency, and between the Boson peak height and its frequency.


2017 ◽  
Vol 111 (26) ◽  
pp. 263103 ◽  
Author(s):  
Young-Ik Sohn ◽  
Rachel Miller ◽  
Vivek Venkataraman ◽  
Marko Lončar

Author(s):  
Jessica Sheehan

Diamond windows are used extensively in the field of optics due to their high transmittance and durability. However, despite their ability to withstand high pressures, diamond windows are not scratch resistant and need to be replaced when the surface is damaged. Moreover, the high cost of diamond windows necessitates extra care to protect the windows and limits the practical size of the window or lens. Thus, alternatives to the highly expensive diamond windows are needed in the optical sciences. A study of single crystal quartz has been conducted to determine if it will make a suitable replacement material. Since the transmittance of single crystal quartz is well documented and desirable for this application, only strength and surface defect experiments were conducted. Trials were run to determine the modulus of rupture of single crystal quartz samples which were also examined with an interferometer and an atomic force microscope (AFM) to correlate the surface conditions with the modulus of rupture. The results showed that even relatively numerous and large defects on the surface did resulted in single crystal quartz holding to high pressures. In addition, the measured modulus of rupture far exceeded the expected values proving that the single crystal quartz is able to withstand the pressures of vacuum. Single crystal quartz is thus found to be a viable alternative to diamond optical windows.


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