scholarly journals Initial β Grain Size Effect on High-Temperature Flow Behavior of Tb8 Titanium Alloys in Single β Phase Field

Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 891
Author(s):  
Qiuyue Yang ◽  
Min Ma ◽  
Yuanbiao Tan ◽  
Song Xiang ◽  
Fei Zhao ◽  
...  
Keyword(s):  
High Temperature ◽  
Titanium Alloys ◽  
Hot Deformation ◽  
Flow Behavior ◽  
Coarse Grained ◽  
Strain Rates ◽  
Processing Parameter ◽  
Fine Grained ◽  
Β Phase ◽  
Different Strains

The high-temperature flow behavior of TB8 titanium alloys with two different grain sizes was investigated in this present work. Results show that a significant characteristic of stress drop is visible at the start stage of the hot deformation process when the strain rates are 100 and 10−1 s−1. With the further increasing of strain, the flow stress initially rises to a maximum value and subsequently attains a plateau for the strain rates of 100 s−1 and a slight decrease for the strain rates of 10−1 s−1. Only dynamic recovery occurs under these deformation conditions. When the strain rates drop to 10−3 s−1, the dynamic recrystallization takes place during hot deformation. The values of deformation activation energy and materials constants at different strains were calculated. The processing maps at different strains were established for the fine- and coarse-grained alloys. The optimal processing parameter for hot processing was attained to be 900 °C/10−3 s−1 for fine-grained alloys and 950 °C/10−3 s−1 for coarse-grained alloys, respectively.

scholarly journals Interfacial Reactions and Fracture Behavior of Ti Alloy-Ag28Cu Brazing Joints: Influence of Titanium Alloy Composition

Metals ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 830 ◽  
Author(s):  
Joachim Gussone ◽  
Galina Kasperovich ◽  
Jan Haubrich ◽  
Guillermo Requena
Keyword(s):  
Titanium Alloys ◽  
Fracture Behavior ◽  
Titanium Substrate ◽  
Tensile Tests ◽  
Coarse Grained ◽  
X Ray ◽  
Fine Grained ◽  
Β Phase ◽  
Brazed Joints ◽  
Crack Paths

Brazing of titanium provides a joining technique suitable for the fabrication of highly-loaded aerospace components, but it still poses numerous challenges, such as the formation of brittle intermetallic interphases. This study of the interphase formation in brazed joints consisting of different titanium alloys (Ti-CP2, Ti-CP4, Ti-6Al-4V, Ti-6Al-2Mo-4Zr-2Sn) and Ag28Cu shows that complex reactions lead to the formation of various intermetallic phases including a Ti2Cu-TiCu boundary zone. The compositions of the titanium alloys influenced the particular microstructures, which have been characterized with various methods including synchrotron X-ray microtomography. Tensile tests evidence high ultimate tensile strengths that are, importantly, not directly limited by the strength of the brazing alloy. The strength of the Ti2Cu-TiCu phase boundary is significantly increased by the alloying elements in Ti-6Al-4V and Ti-6Al-2Mo-4Zr-2Sn and the crack paths change from boundary failure to transcrystalline fracture through TiCu as well as Ag-rich regions. Cu diffusion into the titanium substrate, leading to a coarse grained β-phase that transforms eutectoidally into a lamellar α-Ti + Ti2Cu structure during cooling, occurred in all systems except Ti-6Al-2Mo-4Zr-2Sn where Mo stabilized a fine grained microstructure and enabled the formation of a columnar TiCu structure.

Constitutive Equation for 3104 Alloy at High Temperatures in Consideration of Strain

2016 ◽  
Vol 35 (6) ◽  
pp. 599-605 ◽  
Author(s):  
Fuqiang Zhen ◽  
Jianlin Sun ◽  
Jian Li
Keyword(s):  
Hot Deformation ◽  
Flow Behavior ◽  
Temperature Correction ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Element Analysis ◽  
Hollomon Parameter ◽  
The Finite Element Analysis ◽  
Effects Of Temperature

AbstractThe flow behavior of 3104 aluminum alloy was investigated at temperatures ranging from 250°C to 500°C, and strain rates from 0.01 to 10 s−1 by isothermal compression tests. The true stress–strain curves were obtained from the measured load–stroke data and then modified by friction and temperature correction. The effects of temperature and strain rate on hot deformation behavior were represented by Zener–Hollomon parameter including Arrhenius term. Additionally, the influence of strain was incorporated considering the effect of strain on material constants. The derived constitution equation was applied to the finite element analysis of hot compression. The results show that the simulated force is consistent with the measured one. Consequently, the developed constitution equation is valid and feasible for numerical simulation in hot deformation process of 3104 alloy.

Microstructure Evolution of near α Titanium Alloy during Multi-Step Thermomechanical Deformation Process

2021 ◽  
Vol 1035 ◽  
pp. 305-311
Author(s):  
Qing Shan Liu ◽  
Bo Long Li ◽  
Tong Bo Wang ◽  
Cong Cong Wang ◽  
Peng Qi ◽  
...  
Keyword(s):  
Titanium Alloy ◽  
High Temperature ◽  
Hot Deformation ◽  
Deformation Temperature ◽  
Strain Curve ◽  
Optical Microscope ◽  
Phase Content ◽  
Β Phase ◽  
Α Phase ◽  
Gleeble 3500

A new type of near α high temperature titanium alloy of Ti-Al-Sn-Zr-Mo-Si-Er was studied. The samples with different primary α phase content were prepared by solid solution at 950 °C/1 h—1010 °C/1 h. The multi-step hot compression experiments were carried out by Gleeble-3500 in a sequence of upper region of α + β phase, then followed by lower region of α + β phase. The effects of primary α phase content and deformation temperature on the microstructure of the alloy were studied by means of true stress-strain curve and optical microscope. The results show that the content of primary α phase gradually decreases from 45.4% at 950°C to 0% at 1010°C. As the deformation temperature decreases from 940°C to 900°C, the content of α phase increases gradually from 65% to 94%, which is changed from dynamic recrystallization to deformed structure elongated along RD direction. It is found that the arrangement of α phase along RD direction is the longest at 920°C. With the increase of the deformation temperature in the multi-step high temperature region from 970°C to 990°C, the width of deformed α phase decreases from 3.64 μm at 970°C to 2.71 μm at 990°C. The optimized microstructure is composed of 20% primary α phase arranged along RD direction. This process has a certain potential in the process of hot deformation of the alloy. Key words: high temperature titanium alloy, primary α phase, multi-step hot deformation

High Temperature Oxidation Behavior of Ti3SiC2 in Air

2005 ◽  
Vol 486-487 ◽  
pp. 97-100
Author(s):  
J.H. Ko ◽  
Sung Sic Hwang ◽  
Sang Whan Park ◽  
Dong Bok Lee
Keyword(s):  
High Temperature ◽  
Hot Pressing ◽  
High Temperature Oxidation ◽  
Oxidation Behavior ◽  
Coarse Grained ◽  
Amorphous Sio2 ◽  
Temperature Oxidation ◽  
Fine Grained ◽  
High Temperature Oxidation Behavior ◽  
Tio2 Rutile

Fine-grained and coarse-grained Ti3SiC2 materials were synthesized by hot pressing using TiC0.67 and Si powders as starting materials. The oxidation between 900 and 1100oC in air resulted in the formation of an outer TiO2 (rutile) layer and an inner mixed layer of TiO2 and amorphous SiO2, accompanying the liberation of carbon into the air. Fine-grained Ti3SiC2 displayed better oxidation resistance than coarse-grained one, with activation energies of 376.5~380 kJ/mol for oxidation.

Flow Behavior and Dynamic Recrystallization of BT25y Titanium Alloy During Hot Deformation

2018 ◽  
Vol 37 (2) ◽  
pp. 181-192 ◽  
Author(s):  
Xuemei Yang ◽  
Hongzhen Guo ◽  
Zekun Yao ◽  
Shichong Yuan
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Volume Fraction ◽  
Flow Behavior ◽  
Strain Rates ◽  
Recrystallization Behavior ◽  
Lower Strain ◽  
Deformation Activation Energy ◽  
Strain Data ◽  
Dynamic Recrystallization Behavior

AbstractThe high-temperature plastic deformation and dynamic recrystallization behavior of BT25y alloy were investigated within the deformation temperatures of 1,213–1,293 K and strain rates of 0.001–1.0 s–1 on a Gleeble-1500 thermo-mechanical simulator. Results showed that the dynamic recrystallization (DRX) mechanism played an important role in the hot deformation of BT25y alloy. Based on the regression analysis of the true stress–strain data, the stress exponent and deformation activation energy of BT25y alloy were calculated to be 3.4912 and 288.0435 kJ/mol, respectively. The θ-σ and dθ/dσ–σ curves were plotted to further obtain the critical stress and critical strain for the occurrence of DRX. Based on the analysis results, the DRX kinetic model was established. The model was validated by the comparison between predicted and experimental volume fraction of DRX. As the DRX evolution was sensitive to deformation temperature and strain rate, quantities of dynamically recrystallized grains appeared at higher temperatures and lower strain rates.

Prediction of the Flow Stress of 00Cr17Ni14Mo2 Steel during Hot Deformation

2011 ◽  
Vol 460-461 ◽  
pp. 802-805
Author(s):  
Nan Hai Hao ◽  
Shao Wei Pan
Keyword(s):  
Stainless Steel ◽  
Elevated Temperature ◽  
Flow Stress ◽  
Hot Deformation ◽  
Flow Behavior ◽  
Strain Rates ◽  
Forming Process ◽  
Proposed Model ◽  
316L Austenitic Stainless Steel ◽  
Deformation Tests

The knowledge of the flow behavior of metals during hot deformation is of great importance in determining the optimum forming conditions. In this paper, the flow stress of 00Cr17Ni14Mo2 (ANSI 316L) austenitic stainless steel in elevated temperature is measured with compression deformation tests. The temperatures at which the steel is compressed are 800-1100°C with strain rates of 0.01-1s-1. A mathematical regression model is proposed to describe the flow stress and the validation of the model is conducted also. The proposed model can be used to predict the corresponding flow stress-strain response of 00Cr17Ni14Mo2 stainless steel in elevated temperature for the numerical simulation and design of forming process.

Effect of Hot Deformation Parameters on Flow Behavior and Microstructure of Ti-6Al-4V-0.2O Alloy

2017 ◽  
Vol 898 ◽  
pp. 137-143
Author(s):  
Lin Xiang ◽  
Bin Tang ◽  
Hong Chao Kou ◽  
Jie Shao ◽  
Jin Shan Li
Keyword(s):  
Strain Rate ◽  
Hot Deformation ◽  
Deformation Temperature ◽  
Dynamic Recovery ◽  
Volume Fraction ◽  
Flow Behavior ◽  
Strain Rates ◽  
Compression Tests ◽  
Height Reduction ◽  
Deformation Parameters

Isothermal compression tests were conducted to investigate the effect of hot deformation parameters on flow behavior and microstructure of Ti-6Al-4V-0.2O alloy. The experimental results show that the strain rate and height reduction have little effect on the volume fraction of primary α at a deformation temperature of 860 ̊C. At a deformation temperature of 940 ̊C, the volume fraction of primary α at a high strain rate (10s-1) is about 10% less than that at low strain rates (0.01s-1~1s-1). It may be one of the reasons for the significantly discontinuous yielding phenomenon. Another reason is that the dislocation density decreased suddenly due to the dynamic recovery. With the increasing strain rate and the decreasing deformation temperature, the volume fraction of irregular secondary α increases and lamellar secondary α decreases. And with height reduction increasing, the irregular secondary α increases firstly and then tends to be steady because of dynamic recovery and recrystallization.

scholarly journals Microstructural Variation and a Physical Mechanism Model for a Ti-55511 Alloy during Double-Stage Hot Deformation with Stepped Strain Rates in the β Region

Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6371
Author(s):  
Dao-Guang He ◽  
Gang Su ◽  
Yong-Cheng Lin ◽  
Yu-Qiang Jiang ◽  
Zhou Li ◽  
...  
Keyword(s):  
High Temperature ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Hot Deformation ◽  
Physical Mechanism ◽  
Nucleation Mechanism ◽  
Strain Rates ◽  
Mechanism Model ◽  
Flow Features ◽  
Variation Characteristics

The microstructural variation and high-temperature flow features of a Ti-55511 alloy in the β region are studied by utilizing double-stage compression with a stepped strain rate. The results demonstrate that the stresses in the latter stage of hot compression markedly reduce as the strain at the previous stage or the strain rate at the previous/latter stage drops. Moreover, the annihilation/interaction of substructures is promoted, and the distinct refinement of the dynamic recrystallization (DRX) in the β grain can be found. However, the coarsening of the β grain and the consumption of dislocation substructures are accelerated at high temperatures. Furthermore, the principal DRX nucleation mechanism of the Ti-55511 alloy during double-stage compression with a stepped strain rate in the β region is discontinuous DRX. Additionally, by using the microstructural variation characteristics related to the forming parameters, a physical mechanism equation is modeled to forecast the forming features, the DRX fraction, and the size of the β grain in the investigated alloy. The forecasted results are in accordance with the tested results, indicating that the established model can accurately forecast the microstructure variation and flow features of the studied alloy.

scholarly journals Effect of Initial State and Deformation Conditions on the Hot Deformation Behavior of M50NiL Steel

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5367
Author(s):  
Yan Zhang ◽  
Ming Yang ◽  
Shaolei Long ◽  
Bo Li ◽  
Yilong Liang ◽  
...  
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Experimental Results ◽  
Coarse Grained ◽  
Case Hardening ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Initial State ◽  
Fine Grained

M50NiL steel, which belongs to a new generation of case-hardening steels used in aerospace bearing applications, is used mainly for the manufacturing of aerospace transmission components that operate under high temperatures. In this study, the effects of the hot deformation parameters and the initial microstructure on the hot deformation behavior of M50NiL steel were investigated through Gleeble-3500 isothermal hot compression tests. The experimental results demonstrated that the critical stain of dynamic recrystallization and the deformation activation energy of the coarse-grained samples were higher than those of the fine-grained samples. This is attributed to the difficulty of deformation and the dynamic recrystallization behavior of coarse-grained samples. Moreover, fine-grained samples contain a large number of dispersed phases, which can pin the grain boundaries and inhibit the growth of recrystallized grains. Such phenomena are beneficial for obtaining finer and more uniform microstructures in M50NiL steel. The experimental results can provide a useful reference for preparing M50NiL steel with excellent mechanical properties.

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