scholarly journals Densification, Microstructure and Properties of 90W-7Ni-3Fe Fabricated by Selective Laser Melting

Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 884 ◽  
Author(s):  
Junfeng Li ◽  
Zhengying Wei ◽  
Bokang Zhou ◽  
Yunxiao Wu ◽  
Sheng-Gui Chen ◽  
...  

The preparation of refractory tungsten and tungsten alloys has always been challenging due to their inherent properties. Selective laser melting (SLM) offers a choice for preparing tungsten and tungsten alloys. In this work, 90W-7Ni-3Fe samples were prepared by selective laser melting and investigated. Different process parameter combinations were designed according to the Taguchi method, and volumetric energy density (VED) was defined. Subsequently, the effects of process parameters on densification, phase composition, microstructure, tensile properties, and microhardness were investigated. Nearly a full densification sample (≥99%) was obtained under optimized process parameters, and the value of VED was no less than 300 J/mm3. Laser power had a dominant influence on densification behavior compared with other parameters. The main phases of 90W-7Ni-3Fe are W and γ-(Ni-Fe), dissolved with partial W. In addition, 90W-7Ni-3Fe showed a high tensile strength (UTS = 1121 MPa) with poor elongation (<1%). A high average microhardness (>400 HV0.3) was obtained, but the microhardness presented a fluctuation along building direction due to the inhomogeneous microstructure.

2020 ◽  
Vol 861 ◽  
pp. 77-82
Author(s):  
Gan Li ◽  
Cheng Guo ◽  
Wen Feng Guo ◽  
Hong Xing Lu ◽  
Lin Ju Wen ◽  
...  

This study investigated the effect of laser power (P), scan speed (v) and hatch space (h) on densification behavior, surface quality and hardness of 18Ni300 maraging steel fabricated by selective laser melting (SLM). The results indicated that the relative density of the SLMed samples has a shape increase from 73% to 97% with the laser energy density increasing from 0.5 to 2.2 J/mm2. The relative density ≥ 99% was achieved at the energy density in the range of 2.2~5.9 J/mm2. The optimum process parameters were found to be laser power of 150~200 W, scan speed of 600mm/s and hatch space of 0.105mm. In addition, it was found that the hardness increased initially with the increasing relative density up to relative density of 90% and then little relationship, but finally increase again significantly. This work provides reference for determining process parameters for SLMed maraging steel and the development of 3D printing of die steels.


Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 877
Author(s):  
Cong Ma ◽  
Xianshun Wei ◽  
Biao Yan ◽  
Pengfei Yan

A single-layer three-dimensional model was created to simulate multi-channel scanning of AlSi25 powder in selective laser melting (SLM) by the finite element method. Thermal behaviors of laser power and scanning speed in the procedure of SLM AlSi25 powder were studied. With the increase of laser power, the maximum temperature, size and cooling rate of the molten pool increase, while the scanning speed decreases. For an expected SLM process, a perfect molten pool can be generated using process parameters of laser power of 180 W and a scanning speed of 200 mm/s. The pool is greater than the width of the scanning interval, the depth of the molten pool is close to scan powder layer thickness, the temperature of the molten pool is higher than the melting point temperature of the powder and the parameters of the width and depth are the highest. To confirm the accuracy of the simulation results of forecasting excellent process parameters, the SLM experiment of forming AlSi25 powder was carried out. The surface morphology of the printed sample is intact without holes and defects, and a satisfactory metallurgical bond between adjacent scanning channels and adjacent scanning layers was achieved. Therefore, the development of numerical simulation in this paper provides an effective method to obtain the best process parameters, which can be used as a choice to further improve SLM process parameters. In the future, metallographic technology can also be implemented to obtain the width-to-depth ratio of the SLM sample molten pool, enhancing the connection between experiment and theory.


2015 ◽  
Vol 21 (4) ◽  
pp. 423-432 ◽  
Author(s):  
Luke N. Carter ◽  
Khamis Essa ◽  
Moataz M Attallah

Purpose – The purpose of this paper is to optimise the selective laser melting (SLM) process parameters for CMSX486 to produce a “void free” (fully consolidated) material, whilst reducing the cracking density to a minimum providing the best possible fabricated material for further post-processing. SLM of high temperature nickel base superalloys has had limited success due to the susceptibly of the material to solidification and reheat cracking. Design/methodology/approach – Samples of CMSX486 were fabricated by SLM. Statistical design of experiments (DOE) using the response surface method was used to generate an experimental design and investigate the influence of the key process parameters (laser power, scan speed, scan spacing and island size). A stereological technique was used to quantify the internal defects within the material, providing two measured responses: cracking density and void per cent. Findings – The analysis of variance (ANOVA) was used to determine the most significant process parameters and showed that laser power, scan speed and the interaction between the two are significant parameters when considering the cracking density. Laser power, scan speed, scan spacing and the interaction between power and speed, and speed and spacing were the significant factors when considering void per cent. The optimum setting of the process parameters that lead to minimum cracking density and void per cent was obtained. It was shown that the nominal energy density can be used to identify a threshold for the elimination of large voids; however, it does not correlate well to the formation of cracks within the material. To validate the statistical approach, samples were produced using the predicted optimum parameters in an attempt to validate the response surface model. The model showed good prediction of the void per cent; however, the cracking results showed a greater deviation from the predicted value. Originality/value – This is the first ever study on SLM of CMSX486. The paper shows that provided that the process parameters are optimised, SLM has the potential to provide a low-cost route for the small batch production of high temperature aerospace components.


Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7486
Author(s):  
Stanislav V. Chernyshikhin ◽  
Denis G. Firsov ◽  
Igor V. Shishkovsky

Unique functional properties such as the low stiffness, superelasticity, and biocompatibility of nickel–titanium shape-memory alloys provide many applications for such materials. Selective laser melting of NiTi enables low-cost customization of devices and the manufacturing of highly complex geometries without subsequent machining. However, the technology requires optimization of process parameters in order to guarantee high mass density and to avoid deterioration of functional properties. In this work, the melt pool geometry, surface morphology, formation mode, and thermal behavior were studied. Multiple combinations of laser power and scanning speed were used for single-track preparation from pre-alloyed NiTi powder on a nitinol substrate. The experimental results show the influence of laser power and scanning speed on the depth, width, and depth-to-width aspect ratio. Additionally, a transient 3D FE model was employed to predict thermal behavior in the melt pool for different regimes. In this paper, the coefficients for a volumetric double-ellipsoid heat source were calibrated with bound optimization by a quadratic approximation algorithm, the design of experiments technique, and experimentally obtained data. The results of the simulation reveal the necessary conditions of transition from conduction to keyhole mode welding. Finally, by combining experimental and FE modeling results, the optimal SLM process parameters were evaluated as P = 77 W, V = 400 mm/s, h = 70 μm, and t = 50 μm, without printing of 3D samples.


Coatings ◽  
2019 ◽  
Vol 9 (6) ◽  
pp. 377 ◽  
Author(s):  
Yueling Lyu ◽  
Jingwei Wang ◽  
Yulin Wan ◽  
Yangzhi Chen

Selective laser melting (SLM) is an important advanced additive manufacturing technology. The existing SLM products cannot fully meet the requirements of high-precision and strength of the mechanical component because of their defects. The TiAlN/TiN multilayer coating can improve the surface property of SLM products. The present work aims to explore the influences of different process parameters of SLM on the property of TiAlN/TiN multilayer coating plating on the 361L specimen and the mechanism of these influences. Taking laser power, scanning speed, and scanning space as factors, an orthogonal experiment was designed. The TiAlN/TiN multilayer coating specimens can be obtained by plating on the 361L specimen, fabricated by the process parameters of SLM on the orthogonal experiment. The surface topographies and properties of TiAlN/TiN multilayer coating were tested, the influences of SLM process parameters on TiAlN/TiN multilayer coating were analyzed, and the optimal process parameter was obtained. The electron microscope images revealed that the surface morphology of TiAlN/TiN multilayer coating plating on the SLM specimen was relatively flat, and there were some macro-particles in different sizes and pin holes dispersed on it. The thickness of the TiAlN/TiN multilayer coating was 2.77–3.29 μm. The microhardness value of coating SLM specimen was more than four times that of the uncoated SLM specimen and the wear rates of the uncoated specimen were 2–4 times that of the corresponding coating specimen. The comprehensive analysis shows that the laser power had the greatest influence on the comprehensive property of the coating. The primary cause of the influence of SLM process parameters on the properties of the TiAlN/TiN multilayer coating was preliminarily discussed. When the laser power was 170 W, the scanning speed was 1,100 mm/s, and the scanning space was 0.08mm, the TiAlN/TiN multilayer coating plating on the SLM specimen had the best comprehensive property.


2016 ◽  
Vol 879 ◽  
pp. 330-334 ◽  
Author(s):  
Zhan W. Chen ◽  
Kourosh Darvish ◽  
Timotous Pasang

A strong research effort has continued to determine how selective laser melting (SLM) process parameters relate to the amount of defects present in SLM products. However, how these parameters affect the track profiles which should geometrically affect the amount of lack of fusion (LOF) during SLM has not been studied. This study is needed as severe LOF should be a severe quality and property issue. In this work, how laser power (P) and thus energy, as other build rate related parameters are kept unchanged, affects the size of SLM tracks and the formation of LOF during SLM of CoCrMo alloy has been studied. Through examining the track profiles, track sizes have been geometrically demonstrated to insufficiently overlay and overlap for LOF free when the recommended condition (P = 180W) was used. A further contributing factor for LOF is the irregularity of track shape. Increasing P increased the sizes and improved the stability of the melt and the shape regularity of the tracks, reducing the amount of LOF. It will be shown that there is a rapid decay in the amount of LOF as P increases from 180 W, predominantly as the result of geometrical effect of the track profile on track coverage.


Author(s):  
Aljaž Iveković ◽  
Neda Omidvari ◽  
Bey Vrancken ◽  
Karel Lietaert ◽  
Lore Thijs ◽  
...  

Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 5028
Author(s):  
Fujia Sun ◽  
Ping Liu ◽  
Xiaohong Chen ◽  
Honglei Zhou ◽  
Pengfei Guan ◽  
...  

The approximate process range for preparing the Cu–Cr–Zr alloy by selective laser melting (SLM) was determined by ANSYS simulation, and the influence of the SLM process parameters on the comprehensive properties of the SLM-formed alloy was studied by the design of experiments. The Cu–Cr–Zr alloy with optimum strength and hardness was prepared with high efficiency by optimizing the process parameters for SLM (i.e., laser power, scanning speed, and hatching distance). It is experimentally shown that tensile strength and hardness of the SLM alloy are increased by increasing laser power and decreasing scanning speed, whereas they are initially increased and then decreased by increasing the hatching distance. Moreover, strength, roughness and hardness of the SLM alloy are optimized when laser power is 460 W, scanning speed is 700 mm/s and hatching distance is 0.06 mm. The optimized properties of the SLM alloy are a tensile strength of 153.5 MPa, hardness of 119 HV, roughness of 31.384 μm and relative density of 91.62%.


Coatings ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1323
Author(s):  
Yanlong Jing ◽  
Peng Wang ◽  
Xiaoling Yan

To improve the quality of thick powder bed and realize the matching of thick powder bed and thin powder bed in the later stage, the influence of process parameters for the single-track, multi-layer fabrication, relative density, surface quality, defect, remelting, and boundary optimization performance of different layer thicknesses of Ti-6Al-4V fabricated by selective laser melting were investigated. It is more conducive to the stable forming of single-track when the point distance is half the diameter of the laser beam, and the exposure time is appropriately extended. The thin powder bed needs the corresponding point distance and exposure time under the laser power of 280–380 W to obtain high-density specimens. The thick powder bed needs to be able to ensure the formation of high-quality specimens under the smaller point distance and longer exposure time under higher laser power of 380 W. Both thick powder bed and thin powder bed will cause un-melted defects between molten pools, spheroidization defects caused by splashing, and microporous defects. The remelting process can significantly improve the surface quality of the formed specimen, but the surface quality of the thick powder bed is worse than that of the thin powder bed. The boundary quality of thick powder bed is worse than that of thin powder bed, and the boundary shape has a greater influence on the quality of the SLM forming boundary. Different strategies should be adopted to form the boundary of different shapes. Increasing the boundary count and increasing the laser power are more conducive to the improvement of boundary quality.


Sign in / Sign up

Export Citation Format

Share Document