scholarly journals Influence of Different Annealing Atmospheres on the Mechanical Properties of Freestanding MCrAlY Bond Coats Investigated by Micro-Tensile Creep Tests

Metals ◽  
2019 ◽  
Vol 9 (6) ◽  
pp. 692 ◽  
Author(s):  
Sven Giese ◽  
Steffen Neumeier ◽  
Jan Bergholz ◽  
Dmitry Naumenko ◽  
Willem J. Quadakkers ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Creep Strength ◽  
Bond Coat ◽  
Oxide Dispersion Strengthened ◽  
Tensile Creep ◽  
Creep Tests ◽  
Bond Coats ◽  
Nial Phase ◽  
Lower Strain ◽  
Plasma Sprayed

The mechanical properties of low-pressure plasma sprayed (LPPS) MCrAlY (M = Ni, Co) bond coats, Amdry 386, Amdry 9954 and oxide dispersion strengthened (ODS) Amdry 9954 (named Amdry 9954 + ODS) were investigated after annealing in three atmospheres: Ar–O2, Ar–H2O, and Ar–H2–H2O. Freestanding bond coats were investigated to avoid any influence from the substrate. Miniaturized cylindrical tensile specimens were produced by a special grinding process and then tested in a thermomechanical analyzer (TMA) within a temperature range of 900–950 °C. Grain size and phase fraction of all bond coats were investigated by EBSD before testing and no difference in microstructure was revealed due to annealing in various atmospheres. The influence of annealing in different atmospheres on the creep strength was not very pronounced for the Co-based bond coats Amdry 9954 and Amdry 9954 + ODS in the tested conditions. The ODS bond coats revealed significantly higher creep strength but a lower strain to failure than the ODS-free Amdry 9954. The Ni-based bond coat Amdry 386 showed higher creep strength than Amdry 9954 due to the higher fraction of the β-NiAl phase. Additionally, its creep properties at 900 °C were much more affected by annealing in different atmospheres. The bond coat Amdry 386 annealed in an Ar–H2O atmosphere showed a significantly lower creep rate than the bond coat annealed in Ar–O2 and Ar–H2–H2O atmospheres.

scholarly journals A Comparison between CoNiCrAlY Bond Coat and Zirconia Plasma Sprayed Coatings on Creep Tests

2008 ◽  
Vol 591-593 ◽  
pp. 30-35
Author(s):  
Danieli A.P. Reis ◽  
Carlos de Moura Neto ◽  
Antônio Augusto Couto ◽  
Cosme Roberto Moreira Silva ◽  
Francisco Piorino Neto ◽  
...  
Keyword(s):  
Bond Coat ◽  
Ceramic Coating ◽  
Constant Load ◽  
Creep Tests ◽  
Engineering Ceramic ◽  
Wide Range ◽  
Plasma Sprayed Coatings ◽  
Plasma Sprayed ◽  
Engine Components ◽  
Sprayed Coatings

Thermomechanical and electrical properties of zirconia-based ceramics have led to a wide range of advanced and engineering ceramic applications like solid electrolyte in oxygen sensors, fuel cells and furnace elements and its low thermal conductivity has allowed its use for thermal barrier coatings for aerospace engine components. A comparison between CoNiCrAlY bond coat and zirconia plasma sprayed coatings on creep tests of the Ti-6Al-4V alloy was studied. The material used was commercial Ti-6Al-4V alloy. Yttria (8 wt.%) stabilized zirconia (YSZ) with a CoNiCrAlY bond coat was atmospherically plasma sprayed on Ti-6Al-4V substrates by Sulzer Metco Type 9 MB. Constant load creep tests were conducted on a standard creep machine in air on coated samples, at stress levels of 520 MPa at 500°C to evaluate the oxidation protection on creep of the Ti-6Al-4V alloy. Results indicate that the creep resistance of the ceramic coating was greater than metallic coating.

Effect of multi-pass friction stir processing on thermal distribution and mechanical properties of AZ91

2020 ◽  
Vol 21 (4) ◽  
pp. 411
Author(s):  
Hoda Agha Amini Fashami ◽  
Nasrollah Bani Mostafa Arab ◽  
Mohammad Hoseinpour Gollo ◽  
Bahram Nami
Keyword(s):  
Mechanical Properties ◽  
Creep Strength ◽  
Friction Stir Processing ◽  
Material Behavior ◽  
Az91 Alloy ◽  
Residual Stress Field ◽  
Three Dimensional Model ◽  
Creep Tests ◽  
Friction Stir ◽  
Thermal Distribution

In this paper, the effect of multi-pass friction stir processing on mechanical properties of AZ91 alloy has been studied. For this purpose, the microhardness, tensile, and creep tests were conducted at several temperatures. Optical microscopy and scanning electron micrograph were used to study the microstructure of the processed samples. The experimental results indicated that at room temperature, the microhardness, tensile, and creep strength of the processed samples as compared to the unprocessed ones increased by 23%, 29%, and 38%, respectively. Also, after friction stir processing, the tensile and creep strength of the samples at 210 °C increased by 31% and 47%. In addition, a three-dimensional model was developed to simulate two-pass friction stir processing using ABAQUS/Explicit software. This model involved the Johnson-Cook models for defining material behavior during the process and identifying the fracture criterion. To control the mesh distortion during consecutive passes, the Arbitrary Lagrangian-Eulerian technique was used. Using the developed model, the peak temperature, thermal distribution, and residual stress field during multi-pass friction stir processing on AZ91 have been studied. The empirical results indicated the beneficial influence of the multi-pass friction stir processing on the microstructure and high-temperature mechanical properties of AZ91 alloy.

scholarly journals The Mechanical Properties of Single Crystals of Pure Ice

1969 ◽  
Vol 8 (54) ◽  
pp. 463-473 ◽  
Author(s):  
S. J. Jones ◽  
J. W. Glen
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Single Crystals ◽  
Fracture Stress ◽  
Constant Strain Rate ◽  
Tensile Creep ◽  
Stress Dependence ◽  
Creep Tests ◽  
Dislocation Multiplication ◽  
Compressive Tests

AbstractResults obtained from tensile and compressive tests on pure ice single crystals at various temperatures down to −90°C are reported. At −50°C tensile creep tests give a continually increasing creep rate until fracture, as observed at higher temperatures. The stress dependence of the strain-rate is discussed. Fracture stress increases with decreasing temperature. Results from constant strain-rate compressive tests are compared with theoretical curves computed from Johnston’s (1962) theory of dislocation multiplication. A dislocation velocity of the order of 0.5×10−8 m s−1 is deduced for ice at −50°C.

Microstructure and Tensile Creep Behavior of Mg-Nd-RE-Ca Casting Alloys

2007 ◽  
Vol 345-346 ◽  
pp. 557-560 ◽  
Author(s):  
Joong Hwan Jun ◽  
Bong Koo Park ◽  
Jeong Min Kim ◽  
Ki Tae Kim ◽  
Woon Jae Jung
Keyword(s):  
Mechanical Properties ◽  
Elevated Temperatures ◽  
Tensile Creep ◽  
Secondary Creep ◽  
Creep Tests ◽  
X Ray ◽  
Casting Alloys ◽  
High Temperature Mechanical Properties ◽  
Ca Addition ◽  
Average Size

Influences of Ca addition on microstructures and mechanical properties at room and elevated temperatures have been investigated for Mg-1.5%Nd-1.0%RE-0.5%Zn-(0~1.0)%Ca casting alloys, on basis of experimental results from X-ray diffractometry (XRD), scanning electron microscopy (SEM) with energy dispersive X-ray spectroscopy (EDS), tensile and creep tests. Microstructures of the alloys are characterized by dendritic α-(Mg) grains surrounded by Mg12Nd-Zn-(Ca) eutectic network phase. The average size of α grains decreases gradually with an increase in Ca content. At room temperature, yield strength (YS) is enhanced with increasing Ca content with a decrease in ultimate tensile strength (UTS) and elongation to fracture, whereas the Ca addition leads to greater YS and UTS at 175oC. The tensile creep strain and secondary creep rate, measured at 150 and 200oC under 100MPa for 100hrs, become lower with the increase in Ca content. The obtained tensile properties at elevated temperature demonstrate that the addition of Ca plays a role in improving high temperature mechanical properties including creep resistance for the Mg-Nd-RE-Zn-(Ca) alloys. In view of microstructural evolution, this would be attributed to the refined primary α grains and higher thermal stability of the Mg12Nd-Zn-Ca eutectic strengthening phase.

Effects of Alloying Elements on Mechanical Properties of Mg-Al Alloys

2005 ◽  
Vol 488-489 ◽  
pp. 845-848 ◽  
Author(s):  
Yeon Jun Chung ◽  
Jung Lae Park ◽  
Nack J. Kim ◽  
Kwang Seon Shin
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Elevated Temperatures ◽  
Casting Machine ◽  
Al Alloys ◽  
Alloying Elements ◽  
Tensile Creep ◽  
Thermally Stable ◽  
Creep Tests ◽  
High Temperature Mechanical Properties

The effects of alloying elements on the microstructure and high temperature mechanical properties of Mg-Al alloys were investigated in this study. In order to improve the high temperature mechanical properties, Sr or Mm was added to the Mg-9Al alloy. The effect of Sn on the Mg-9Al alloy was also examined since Sn was expected to improve the high temperature mechanical properties by forming the thermally stable Mg2Sn phase. The specimens used in this study were produced on a 320 ton cold chamber high-pressure die casting machine. The microstructures of the specimens were examined by optical and scanning electron microscopy and tensile and creep tests were performed at elevated temperatures. Tensile tests were carried out at room temperature, 150oC and 200oC using an initial strain rate of 2×10-4/sec. In addition, tensile creep tests were conducted at the stress levels of 50 MPa and 70 MPa. From the microstructure analyses of the specimens after heat treatment at 400oC for 12 hours, it was found that most of the Mg17Al12 precipitate dissolved into the matrix, while the thermally stable phases continued to exist. The high temperature mechanical properties of the Mg-9Al alloys were found to improve significantly with the additions of Sr, Mm and Sn, due to the formation of the thermally stable precipitates.

Thermal and Loading Effects on Mechanical Properties of a Hot Isostatically Pressed Si3N4

1994 ◽  
Author(s):  
Jagannathan Sankar ◽  
Jayant Neogi ◽  
Suneeta S. Neogi ◽  
Marvln T. Dixie ◽  
Ranji Vaidyanathan
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Silicon Nitride ◽  
Elevated Temperatures ◽  
Heat Engine ◽  
Tensile Tests ◽  
Tensile Creep ◽  
Uniaxial Tensile ◽  
Creep Tests ◽  
Loading Effects

The effect of thermal soaking on the mechanical properties of a candidate material for advanced heat engine applications namely, hot isostatically pressed (HIPed) silicon nitride (GTEPY6) are reported here. Pure uniaxial tensile tests conducted at room and at elevated temperatures indicated that the tensile strength of this material dropped significantly after 1000°C. The residual tensile strength of PY6 material after thermal soaking at 1200° and 1300°C was also investigated. Test results showed that thermal soaking at 1200° and 1300°C increased the residual tensile strength. The thermal soaking time had a greater effect on the residual tensile strength at 1300°C. Tensile creep tests performed at 1200° and 1300°C showed that the steady state creep rate was influenced by both the temperature and the applied stress. The higher stress exponent in HIPed as compared to a sintered silicon nitride shows higher creep resistance in the case of HIPed materials.

scholarly journals The Mechanical Properties of Single Crystals of Pure Ice

1969 ◽  
Vol 8 (54) ◽  
pp. 463-473 ◽  
Author(s):  
S. J. Jones ◽  
J. W. Glen
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Single Crystals ◽  
Fracture Stress ◽  
Constant Strain Rate ◽  
Tensile Creep ◽  
Stress Dependence ◽  
Creep Tests ◽  
Dislocation Multiplication ◽  
Compressive Tests

Abstract Results obtained from tensile and compressive tests on pure ice single crystals at various temperatures down to −90°C are reported. At −50°C tensile creep tests give a continually increasing creep rate until fracture, as observed at higher temperatures. The stress dependence of the strain-rate is discussed. Fracture stress increases with decreasing temperature. Results from constant strain-rate compressive tests are compared with theoretical curves computed from Johnston’s (1962) theory of dislocation multiplication. A dislocation velocity of the order of 0.5×10−8 m s−1 is deduced for ice at −50°C.

scholarly journals Evaluation of Commercial Coatings on MarM-002, IN-939 and CM-247 Substrates

1996 ◽  
Author(s):  
J. G. Goedjen ◽  
G. P. Wagner
Keyword(s):  
Electron Beam ◽  
Vapor Deposition ◽  
Bond Coat ◽  
Physical Vapor Deposition ◽  
Thermally Grown Oxide ◽  
Department Of Energy ◽  
Superior Performance ◽  
Air Plasma ◽  
Bond Coats ◽  
Plasma Sprayed

As part of the U.S. Department of Energy Advanced Turbine Systems Program, the performance of Chromalloy RT122, RT122 over RT69 and the Howmet 150L bond coats were evaluated for use in the next generation of Westinghouse combustion turbines. Air plasma sprayed and electron beam physical vapor deposition 8% yttria stabilized zirconia thermal barrier coatings were applied to the bond coats. The coating systems were evaluated in air at 2102°F (1150°C), cooling to room temperature once per day. The life-limiting failure mode in both air plasma sprayed (APS) and electron beam - physical vapor deposition (EB-PVD) coating systems is the oxidation of the bond coat. The coating life is related to the growth rate and morphology of the thermally grown oxide. The superior performance of RT122 on MarM-002, the duplex bond coat system of RT122 over RT69 on MarM-002 and Howmet 150L on MarM-002 can be related to the development of a uniform, slow growing oxide scale. The development of a non-uniform oxidation front contributes to the reduced life of RT122 on IN-939 and CM-247.

scholarly journals Comparative Study on the Thermal Performance of Cr-CrxOy and YSZ-CoNiCrAlY Coatings Exposed at 900 °C

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6040
Author(s):  
Markus Kiryc ◽  
Norbert Kazamer ◽  
Deniz Kurumlu ◽  
Gabriela Marginean
Keyword(s):  
Mechanical Properties ◽  
Heat Treating ◽  
Atmospheric Plasma ◽  
Oxidation Protection ◽  
Bond Coats ◽  
Hot Gas ◽  
Temperature Regimes ◽  
Heat Treated ◽  
Plasma Sprayed ◽  
Crack Susceptibility

Yttria stabilized zirconia (YSZ) thermal barrier coatings (TBCs) deposited on CoNiCrAlY oxidation protective bond coats are commonly required in temperature regimes up to 1200 °C (e.g., hot gas turbine regions) due to their superior thermal behavior and mechanical properties. For temperatures up to around 900 °C, oxidation protection can be alternatively provided by metallic-ceramic Cr-CrxOy coatings. For the present research, Cr-CrxOy atmospheric plasma sprayed (APS) and YSZ-CoNiCrAlY APS-high velocity oxy-fuel TBC coatings were deposited on a NiCr20Co18Ti substrate. The samples were isothermally heat treated at 900 °C for 10 h in an environmental atmosphere and subsequently isothermally oxidized at the same temperature for 1200 h. Investigations of the physical, chemical, and mechanical properties were performed on the as-sprayed, heat-treated, and oxidized samples. The oxidation behavior, microhardness, cohesion, and adhesion of the samples were correlated with the microstructural investigations and compared to the conventional TBC system. It could be shown that heat treating decreased the Cr-CrxOy coatings crack susceptibility and led to the formation of a protective thermally grown Cr oxide layer. The experimental work on the YSZ-CoNiCrAlY system revealed that the phase composition of the bond coat has a direct influence on the oxidation protection of the coating system.

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