scholarly journals The Influence of Laser Nitriding on Creep Behavior of Ti-4Al-4V Alloy with Widmanstätten Microstructure

Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 236 ◽  
Author(s):  
Luciana Narciso da Silva Briguente ◽  
Javier Oñoro ◽  
Flávio Perpétuo Briguente ◽  
Fabrícia Assis Resende ◽  
Joares Lidovino dos Reis ◽  
...  
Keyword(s):  
Laser Power ◽  
Specific Resistance ◽  
Surface Hardness ◽  
Base Material ◽  
Constant Load ◽  
Mechanical Resistance ◽  
Creep Tests ◽  
Laser Nitriding ◽  
Stationary Creep ◽  
Good Creep Resistance

Ti-6Al-4V alloy has been considered in applications of aeronautical and aerospace industries, due to its properties such as high specific resistance, good creep resistance and metallurgical stability. However, its use in applications for high temperatures is restricted due to its great affinity with the oxygen, which results in the formation of oxide layers and limits its mechanical resistance at these conditions. Thus, specific treatments have been employed in the material to work as surface barriers to avoid the oxygen diffusion in the alloy under high temperature conditions. One surface treatment that can be used is laser nitriding. In the present work, the surface of Ti-6Al-4V alloy with Widmanstätten microstructure was nitrided by applying Nd:YAG laser focal with 0.6 mm diameter, at laser power of 700, 750 and 800 W, process speed of 100 mm/s and 20 L/min of N2 flow. Creep tests were performed at constant load at 600 °C and 125 MPa, to verify the influence of treatment on the Ti-6Al-4V alloy. Results have indicated a lower stationary creep rate for the titanium alloy with Widmanstätten laser-nitrided structure when compared to the non-nitriding material. Besides that, the surface hardness increased from 368 HV of base material to 1000 HV after laser nitriding.

A Comparison of Gas Nitriding and Laser Nitriding on Industrial Pure Iron and Ti-Induced Iron

2018 ◽  
Vol 934 ◽  
pp. 79-88 ◽  
Author(s):  
An Min Liu ◽  
Yu Fan ◽  
Pei Zhi Li ◽  
Kun Chen ◽  
Ke Pu ◽  
...  
Keyword(s):  
Pure Iron ◽  
Laser Power ◽  
Metal Layer ◽  
Nitrogen Compound ◽  
Surface Hardness ◽  
Nitride Layer ◽  
Nitrogen Compounds ◽  
Laser Nitriding ◽  
Gas Nitriding ◽  
The Difference

Overview of Gas nitriding on the surface of industrial pure iron and laser gas nitriding, research under different nitriding process, the phase, organization and mechanical properties of the nitride layer that is the difference. Plasma sprayed titanium on industrial pure iron surface, the laser nitriding experiments were carried out on the titanium surface. The formation of iron and nitrogen compounds is induced by the combination of titanium nitride. The difference between gas nitriding and laser nitriding is analyzed. The results show that: (1) after gas nitriding, the nitrides formed on the surface of pure iron are mainly ε-Fe2-3N and γ′-Fe4N, the surface hardness is 158 HV, and the increase is 32%. (2) in the 500 W laser power, laser nitriding formed on the surface of Titanium metal layer of pure iron, but not the formation of iron and nitrogen compound, the surface hardness of 168 HV, increased by 46%. (3) under the condition of 500 W laser power, the industrial pure iron was nitrided by laser, without the formation of iron and nitrogen compounds, but the surface hardness of the sample was increased by 20%.

Field observations on the load–strain–time behaviour of geogrid reinforcement

1994 ◽  
Vol 31 (4) ◽  
pp. 564-569 ◽  
Author(s):  
R.J. Fannin
Keyword(s):  
Tensile Strength ◽  
Field Data ◽  
Constant Load ◽  
Reinforced Soil ◽  
Mean Annual Temperature ◽  
Creep Tests ◽  
Geogrid Reinforcement ◽  
Rapid Loading ◽  
Strip Test ◽  
Relationship Of

Field data are reported that describe the load–strain–time relationship of geogrid reinforcement in a reinforced soil structure. The data are for a period exceeding 5 years and reveal a continued strain in the reinforcement, which occurs at nearly constant load. The response to loading is attributed to creep of the polymeric material. A comparison of the field data with laboratory isochronous load–strain curves, from rapid loading creep tests performed at a temperature similar to the mean annual temperature in the backfill soil, shows the curves describe very well the magnitude of creep strains observed in the field. Implications of the load–strain–time performance data are assessed with reference to the use in design of a tensile strength established from the rapid-loading creep test and wide-width strip test. The need to clarify, in design of polymeric reinforced soil structures, between a safe and allowable tensile strength is emphasized. Key words : reinforced soil, geogrid, creep, tensile strength, strain.

scholarly journals A Comparison between CoNiCrAlY Bond Coat and Zirconia Plasma Sprayed Coatings on Creep Tests

2008 ◽  
Vol 591-593 ◽  
pp. 30-35
Author(s):  
Danieli A.P. Reis ◽  
Carlos de Moura Neto ◽  
Antônio Augusto Couto ◽  
Cosme Roberto Moreira Silva ◽  
Francisco Piorino Neto ◽  
...  
Keyword(s):  
Bond Coat ◽  
Ceramic Coating ◽  
Constant Load ◽  
Creep Tests ◽  
Engineering Ceramic ◽  
Wide Range ◽  
Plasma Sprayed Coatings ◽  
Plasma Sprayed ◽  
Engine Components ◽  
Sprayed Coatings

Thermomechanical and electrical properties of zirconia-based ceramics have led to a wide range of advanced and engineering ceramic applications like solid electrolyte in oxygen sensors, fuel cells and furnace elements and its low thermal conductivity has allowed its use for thermal barrier coatings for aerospace engine components. A comparison between CoNiCrAlY bond coat and zirconia plasma sprayed coatings on creep tests of the Ti-6Al-4V alloy was studied. The material used was commercial Ti-6Al-4V alloy. Yttria (8 wt.%) stabilized zirconia (YSZ) with a CoNiCrAlY bond coat was atmospherically plasma sprayed on Ti-6Al-4V substrates by Sulzer Metco Type 9 MB. Constant load creep tests were conducted on a standard creep machine in air on coated samples, at stress levels of 520 MPa at 500°C to evaluate the oxidation protection on creep of the Ti-6Al-4V alloy. Results indicate that the creep resistance of the ceramic coating was greater than metallic coating.

Effect of Friction Stir Processing Parameters on the Properties of AA7075-T73/Al2O3 Surface Metal Matrix Composite

2020 ◽  
Vol 1002 ◽  
pp. 140-150
Author(s):  
Ali H. Al-Helli ◽  
Ahmed R. Alhamaoy ◽  
Ayad Murad Takhakh
Keyword(s):  
Friction Stir Processing ◽  
Particle Distribution ◽  
Surface Hardness ◽  
Base Material ◽  
Processing Parameters ◽  
Optical Microscope ◽  
Friction Stir ◽  
Surface Composite ◽  
Surface Metal ◽  
Number Of Passes

Friction Stir Processing (FSP) technology was wielded to output the Al7075/ Al2O3 surface composite. The effects parameters of processing method on particle distribution have been studied. The microstructure and mechanical characteristics of the samples were examined using the optical microscope, SEM and hardness examination. Acquired consequences, showed that Al2O3 particles were in a good interior distribution inside the basement. This technique produced excellent bonding between the surface composite and the base material. On other hand the surface hardness was increased about 25% as compared with the substrate. In addition, grain matrix refinement and enhanced particle distribution were obtained after each FSP pass. Also the dispersion of Al2O3 particles in the stirred area became more homogeneous and the average hardness improved by increasing the number of passes.

An investigation of the creep processes in tin and aluminum using a depth-sensing indentation technique

1992 ◽  
Vol 7 (3) ◽  
pp. 627-638 ◽  
Author(s):  
V. Raman ◽  
R. Berriche
Keyword(s):  
Stress Exponent ◽  
Constant Load ◽  
Indentation Creep ◽  
Depth Sensing ◽  
Creep Tests ◽  
Si Substrates ◽  
Uniaxial Creep ◽  
Rate Versus ◽  
Deformation Properties ◽  
Film Substrate

Constant load creep experiments were conducted using a depth-sensing indentation instrument with indentation depths in the submicron range. Experiments were conducted on polycrystalline Sn and sputtered Al films on Si substrates. The results show that the plastic depth versus time curves and the strain rate versus stress plots from these experiments are analogous to those obtained from conventional creep experiments using bulk specimens. The value of the stress exponent for Sn is close to the reported values from uniaxial creep tests. Tests on Al films showed that the stress exponent is dependent on the indentation depth and is governed by the proximity to the film/substrate interface. Load change experiments were also performed and the data from these tests were analyzed. It is concluded that indentation creep experiments may be useful in elucidating the deformation properties of materials and in identifying deformation mechanisms.

scholarly journals Influence of Zirconia Plasma-Sprayed Coating on Creep of the Ti-6Al-4V Alloy

2006 ◽  
Vol 530-531 ◽  
pp. 690-695 ◽  
Author(s):  
Danieli A.P. Reis ◽  
Cosme Roberto Moreira Silva ◽  
Maria do Carmo de Andrade Nono ◽  
M.J.R. Barboza ◽  
Francisco Piorino Neto ◽  
...  
Keyword(s):  
Creep Resistance ◽  
Surface Oxidation ◽  
Constant Load ◽  
Nitrogen Atmosphere ◽  
High Temperature Strength ◽  
Secondary Creep ◽  
Creep Tests ◽  
Oxidation Protection ◽  
Sprayed Coating ◽  
Plasma Sprayed

The titanium affinity by oxygen is one of main factors that limit the application of their alloys as structural materials at high temperatures. Notables advances have been obeserved in the development of titanium alloys with the objective of improving the specific high temperature strength and creep-resistance properties. However, the surface oxidation limits the use of these alloys in temperatures up to 600°C. The objective of this work was estimate the influence of the plasma-sprayed coatings for oxidation protection on creep of the Ti-6Al-4V alloy, focusing on the determination of the experimental parameters related to the primary and secondary creep states. Constant load creep tests were conducted with Ti-6Al-4V alloy in air for coated and uncoated samples and in nitrogen atmosphere for uncoated samples at 500°C to evaluate the oxidation protection on creep of the Ti-6Al-4V alloy. Yttria (8 wt.%) stabilized zirconia (YSZ) with a CoNiCrAlY bond coat was atmospherically plasma sprayed on Ti-6Al-4V specimens. Results indicated the creep resistance of the coated alloy was greater than uncoated in air, but nitrogen atmosphere was more efficient in oxidation protection. Previously reported results about the activation energies and the stress exponents values indicate that the primary and stationary creep, for both test conditions, was probably controlled by dislocation climb. Occurred a decreasing of steady state creep in function of the reduction of oxidation process, showing that Ti-6Al-4V alloy lifetime was strongly affected by the atmosphere due the oxidation suffered by the material.

scholarly journals Nanoindentation Studies of Plasticity and Dislocation Creep in Halite

Geosciences ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 79 ◽  
Author(s):  
Christopher Thom ◽  
David Goldsby
Keyword(s):  
Strain Rate ◽  
Stress Exponent ◽  
Creep Behavior ◽  
Constant Load ◽  
Dislocation Creep ◽  
Indentation Creep ◽  
Creep Tests ◽  
Creep Flow ◽  
A Value ◽  
Flow Laws

Previous deformation experiments on halite have collectively explored different creep mechanisms, including dislocation creep and pressure solution. Here, we use an alternative to conventional uniaxial or triaxial deformation experiments—nanoindentation tests—to measure the hardness and creep behavior of single crystals of halite at room temperature. The hardness tests reveal two key phenomena: (1) strain rate-dependent hardness characterized by a value of the stress exponent of ~25, and (2) an indentation size effect, whereby hardness decreases with increasing size of the indents. Indentation creep tests were performed for hold times ranging from 3600 to 106 s, with a constant load of 100 mN. For hold times longer than 3 × 104 s, a transition from plasticity to power-law creep is observed as the stress decreases during the hold, with the latter characterized by a value of the stress exponent of 4.87 ± 0.91. An existing theoretical analysis allows us to directly compare our indentation creep data with dislocation creep flow laws for halite derived from triaxial experiments on polycrystalline samples. Using this analysis, we show an excellent agreement between our data and the flow laws, with the strain rate at a given stress varying by less than 5% for a commonly used flow law. Our results underscore the utility of using nanoindentation as an alternative to more conventional methods to measure the creep behavior of geological materials.

High-Temperature Creep Tests of Two Creep-Resistant Materials at Constant Stress and Constant Load

2019 ◽  
Vol 827 ◽  
pp. 246-251
Author(s):  
Vàclav Sklenička ◽  
Květa Kuchařová ◽  
Marie Kvapilová ◽  
Luboš Kloc ◽  
Jiří Dvořák ◽  
...  
Keyword(s):  
Creep Behaviour ◽  
Constant Load ◽  
Complex Stress ◽  
Constant Stress ◽  
Fracture Mechanisms ◽  
Stress Tests ◽  
Creep Tests ◽  
Deformation And Fracture ◽  
Dependent Component ◽  
The Difference

Creep is defined as a time dependent component of plastic deformation. Creep tests can be performed either at constant load or at constant applied stress. Engineering creep tests carried out at constant load are aimed at determination of the creep strength or creep fracture strength, i.e. the data needed for design. The constant stress tests are important as a data source for fundamental investigations of creep deformation and fracture mechanisms and for finite element modelling of more complex stress situations. For some materials, the difference between the two type of testing can be very small, while for other materials is large, depending on the creep plasticity of the material under testing. The paper aims to compare the creep results of two different creep-resistant materials: the advanced 9%Cr martensitic steel (ASME Grade P91) and a Zr1%Nb alloy obtained by both testing methods and to clarify the decisive factors causing observed differences in their creep behaviour.

Creep Characterization of Ni-Based Superalloy IN-792 Using the 4- and 6-θ Projection Method

2013 ◽  
Vol 136 (1) ◽  
Author(s):  
S. A. Sajjadi ◽  
M. Berahmand ◽  
A. Rezaee-Bazzaz
Keyword(s):  
Projection Method ◽  
High Strain ◽  
Operating Temperature ◽  
Constant Load ◽  
Least Square ◽  
Creep Tests ◽  
Wide Range ◽  
Creep Curves ◽  
Projection Techniques

This paper studies the accuracy of a technique which is capable of predicting and modeling a wide range of creep life in Ni-based superalloys. The θ-projection method was applied to characterize the creep behavior of the Ni-based superalloy IN-792 at 800 °C. Constant load creep tests have been carried out over a wide range of loads at the constant operating temperature. Creep curves were fitted using either 4-θ or 6-θ equation by the use of a nonlinear least-square technique. The results showed that both 4- and 6-θ projection parameters revealed a good linearity as a function of stress. Comparison of experimental creep curves with those predicted using both of the utilized θ-projection techniques showed that the techniques fit the experimental data at high strain values very well while the 6-θ approach describes much better the creep curves at low strain region.

A Review on Surface Engineering of Ti6Al4V Titanium Alloy Using Gas and Laser Nitriding Techniques

2015 ◽  
Vol 766-767 ◽  
pp. 618-625 ◽  
Author(s):  
J.R Deepak
Keyword(s):  
Titanium Alloy ◽  
Surface Properties ◽  
Surface Engineering ◽  
Surface Hardness ◽  
Aircraft Engine ◽  
Ti6al4v Alloy ◽  
Surface Stability ◽  
Laser Nitriding ◽  
Gas Nitriding ◽  
Grade 5

Nitriding is the most common surface engineering technique that is being used in Titanium alloys for improving their surface properties, viz hardness, wear resistance, etc. Ti6Al4V (Grade 5) Titanium Alloy is a super alloy that exhibits excellent mechanical strength; it is highly resistance to creep at very high temperatures which maintains good surface stability. It is resistant to corrosion and oxidation. The main objective of this review paper is to study the recent research works carried on Nitriding of Ti6Al4V alloy by using, viz gas Nitriding and laser Nitriding. This process is used in the surface hardening of machine parts such as aircraft engine parts, crank pins, valve seats, gears, bush, aero engine cylinders, aero crank shafts. Gas Nitriding is a diffusional technique in which the nitrogen atoms are diffused into the surface of the metal to obtain hard surface. By Laser Nitriding is a diffusional technique by which the surface properties of the titanium alloy is enhanced. Laser nitriding process comprises of various stages, viz, transport of heat, melting effect, diffusion and convection effect. By Nitriding technique the surface hardness of super alloys like Titanium Alloy Ti6Al4V Grade 5 can be increased by increasing the hardness on the surface there by its scope of application is widened. In this paper a literature survey is carried out and the recent research works on surface engineering of Ti6Al4V alloy using gas and laser Nitriding technique is summarized.

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