scholarly journals Dynamically Recrystallized Microstructures, Textures, and Tensile Properties of a Hot Worked High-Mn Steel

Metals ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 30 ◽  
Author(s):  
Pavel Dolzhenko ◽  
Marina Tikhonova ◽  
Rustam Kaibyshev ◽  
Andrey Belyakov

The deformation microstructures and mechanical properties were studied in a high-Mn steel subjected to hot compression. The deformation microstructures resulted from the development of dynamic recrystallization (DRX). Two DRX mechanisms, namely discontinuous and continuous, operated during warm-to-hot working. Under the conditions of hot working when the flow stresses were below 100 MPa, a power law function was obtained between the DRX grain size and the true flow stress with a grain size exponent of −0.8 owing to the discontinuous DRX. On the other hand, the gradual change in the operating DRX mechanism from a discontinuous to continuous one upon a transition from hot to warm working, when the true flow stress increases above 100 MPa, resulted in the grain size exponent of about −0.5 in the power law between the flow stress and the DRX grain size. The DRX microstructures developed by warm-to-hot working provide a beneficial combination of mechanical properties including high ultimate tensile strength in the range of 700–900 MPa and sufficient ductility with a uniform elongation well above 50%. The strengthening of the samples with DRX microstructures was attributed to the combined effect of the grain size and dislocation strengthening resulting in a rather high grain boundary strengthening factor of 570 MPa μm0.5 in the Hall-Petch-type relationship.

Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 4004
Author(s):  
Pavel Dolzhenko ◽  
Marina Tikhonova ◽  
Rustam Kaibyshev ◽  
Andrey Belyakov

The features of discontinuous dynamic recrystallization (DRX) in a highly-alloyed austenitic stainless steel were studied at temperatures of 800 °C to 1100 °C. Hot deformation accompanied by DRX was characterized by an activation energy of 415 kJ/mol. The frequency of the sequential DRX cycles depended on the deformation conditions; and the largest fraction of DRX grains with small grain orientation spread below 1° was observed at a temperature of around 1000 °C and a strain rate of about 10−3 s−1. The following power law relationships were obtained for DRX grain size (DDRX) and dislocation density (ρ) vs. temperature-compensated strain rate (Z) or peak flow stress (σP): DDRX ~ Z−0.25, ρ ~ Z0.1, σP ~ DDRX−0.9, σP ~ ρ1.4. The latter, i.e., σP ~ ρ1.4, was valid in the flow stress range below 300 MPa and changed to σP ~ ρ0.5 on increasing the stress. The obtained dependencies suggest a unique power law function between the dislocation density and the DRX grain size with an exponent of −0.5.


2012 ◽  
Vol 706-709 ◽  
pp. 2704-2709 ◽  
Author(s):  
Andrey Belyakov ◽  
Nadezhda Dudova ◽  
Marina Tikhonova ◽  
Taku Sakai ◽  
Kaneaki Tsuzaki ◽  
...  

Dynamic recrystallization (DRX) is one of the most important mechanisms for microstructure evolution during deformation of various metals and alloys. So-called discontinuous DRX usually develops in structural materials with low to medium stacking fault energy during hot working. The local migration, i.e. bulging, of grain boundaries leads to the formation of recrystallization nuclei, which then grow out consuming work-hardened surroundings. The cyclic character of nucleation and growth of new grains during deformation results in a dynamically constant average grain size. The dynamic grain size is sensitively dependent on temperature and strain rate and can be expressed by a power law function of flow stress with a grain size exponent of about-0.7 under conditions of hot working. Recent studies on DRX phenomenon suggest that a decrease in deformation temperature changes the structural mechanism for new grain formation. As a result, the grain size exponent in the relationship between the dynamic grain size and flow stress approaches about-0.25 under warm working conditions.


2012 ◽  
Vol 468-471 ◽  
pp. 2124-2127 ◽  
Author(s):  
Shao Feng Zeng ◽  
Kai Huai Yang ◽  
Wen Zhe Chen

Equal channel angular pressing (ECAP) was applied to a commercial AZ61 magnesium alloy for up to 8 passes at temperatures as low as 473K. Microstructures and mechanical properties of as-received and ECAP deformed samples were investigated. The microstructure was initially not uniform with a “bimodal” grain size distribution but became increasingly homogeneous with further ECAP passes and the average grain size was considerably reduced from over 26 μm to below 5 μm. The ultimate tensile strength (UTS) decreases clearly after one pass, but increases significantly up to two passes, and then continuously slowly decreases up to six passes, and again increases slightly up to eight passes. In contrast, the uniform elongation increased significantly up to 3 passes, followed by considerable decrease up to 8 passes. These observations may be attributed to combined effects of grain refinement and texture development.


2020 ◽  
Vol 2 (11) ◽  
Author(s):  
Juhani Laitila ◽  
Lassi Keränen ◽  
Jari Larkiola

AbstractIn this study, we present the effect of enhanced cooling on the mechanical properties of a high-strength low-alloy steel (having a yield strength of 700 MPa) following a single-pass weld process. The properties evaluated in this study include uniform elongation, impact toughness, yield, tensile and fatigue strengths alongside the cooling time of the weld. With the steel used in this study, the enhanced cooling resulted in a weld joint characterized with excellent cross-weld uniform elongation, yield and fatigue strength. The intensified cooling reduced the time it takes for the weld to reach 100 °C by around 190 s. Not only the fusion line of the weld was less pronounced, but also the grain size of the CGHAZ was greatly refined as a result of the enhanced cooling. The results indicate that combining external cooling to the welding processes can be beneficial for the studied high-strength steel.


1984 ◽  
Vol 5 ◽  
pp. 1-8 ◽  
Author(s):  
Nobuhiko Azuma ◽  
Akira Higashi

Uniaxial compression tests were carried out with specimens cut from several deep ice cores obtained at Dye 3, Greenland, in 1980 and 1981. The power law relationship of = Αση was obtained between the uniaxial strain-rate and the uniaxial stress σ. In a range of strain-rates between 10−8 and 10−7 s−1, the value of the power n for samples with strong single maximum fabric was approximately 4, significantly larger than the value of 3 which has been generally accepted from experiments using artificial polycrystalline ice. A work-hardening effect was found in the ice-core samples taken from a depth of 1900 m, which had a smaller grain size than the others. Recrystallization occurred when the temperature of the specimen was raised during the test and this ultimately caused the formation of the so-called diamond pattern ice fabric.


2014 ◽  
Vol 794-796 ◽  
pp. 870-875 ◽  
Author(s):  
Min Zha ◽  
Yan Jun Li ◽  
Ragnvald H. Mathiesen ◽  
Christine Baumgart ◽  
Hans J. Roven

Ultrafine-grained (UFG) binary Al-xMg (x=1, 5 and 7 wt %) alloys were processed by equal channel angular pressing (ECAP) at room temperature via route Bccombined with inter-pass annealing. The effects of Mg content, grain size and strain rate on mechanical properties and dynamic strain aging (DSA) behaviour of the Al-Mg alloys upon tensile testing at room temperature were studied. An increase in Mg content from 5 to 7 wt % leads to a pronounced increase in strength and uniform elongation in both the as-homogenized and as-ECAP Al-Mg alloys. Thereby, the Al-7Mg alloy, either prior to or after ECAP processing, possess significantly higher strength and comparable or even higher uniform elongation than the more dilute Al-Mg alloys. However, the as-ECAP Al-Mg alloys exhibit significantly higher strength but little work hardening and hence rather limited uniform elongation. In general, decreasing grain size leads to significant increase in strength while dramatic decrease in ductility. Moreover, DSA serration amplitudes increase with reducing grain size in the micrometer range. However, the UFG Al-Mg alloys exhibit much less DSA effect than the micrometer scaled grain size counterparts, i.e. probably due to the high dislocation densities and special grain boundary features in the UFG materials. Also, the Al-Mg alloys, especially those with a UFG structure, exhibit higher strength and ductility at lower strain rate than at higher strain rate, due mainly to enhanced DSA effect and hence work hardening at a lower strain rate.


2008 ◽  
Vol 140 ◽  
pp. 185-190 ◽  
Author(s):  
T.B. Tengen ◽  
Tomasz Wejrzanowski ◽  
R. Iwankiewicz ◽  
Krzysztof Jan Kurzydlowski

Predicting the properties of a material from knowledge of the internal microstructures is attracting significant interest in the fields of materials design and engineering. The most commonly used expression, known as Hall-Petch Relationship (HPR), reports on the relationship between the flow stress and the average grain size. However, there is much evidence that other statistical information that the grain size distribution in materials may have significant impact on the mechanical properties. These could even be more pronounced in the case of grains of the nanometer size, where the HPR is no longer valid and the Reverse-HPR is more applicable. This paper proposes a statistical model for the relationship between flow stress and grain size distribution. The model considered different deformation mechanisms and was used to predict mechanical properties of aluminium and copper. The results obtained with the model shows that the dispersion of grain size distribution plays an important role in the design of desirable mechanical properties. In particular, it was found that that the dependence of a material’s mechanical properties on grain size dispersion also follows the HPR to Inverse-HPR type of behaviour. The results also show that copper is more sensitive to changes in grain size distribution than aluminium.


2008 ◽  
Vol 584-586 ◽  
pp. 547-552 ◽  
Author(s):  
Daisuke Terada ◽  
Toshiaki Masui ◽  
Naoya Kamikawa ◽  
Nobuhiro Tsuji

Effect of solid solution elements on microstructure evolution and mechanical properties was investigated using a high purity Al (purity 99.99%) and Al-0.5 at.% X ( X = Si, Ag, Mg ) alloys deformed by accumulative roll bonding (ARB) process up to 7 cycles (equivalent strain of 5.6) at ambient temperature. The ARB-processed high purity Al showed the equiaxed microstructure having mean grain size of 750 nm. On the other hand, the microstructure of the ARB-processed Al-0.5at.%X alloys showed lamellar boundary structures elongated along RD. The mean lamellar boundary spacing significantly differed depending on the alloying elements, which suggested that solute atoms had a significant effect on microstructure evolution. The difference in the grain size was regarded to be caused by the difference in recovery processes in the alloys. The tensile strength of the alloys increased with increasing the number of ARB cycles. In the Al-Si and Al-Ag alloys, the post-uniform elongation increased with increasing the number of the ARB cycles. On the other hand, the elongation of the Al-Mg hardly changed during the ARB process.


2013 ◽  
Vol 59 (213) ◽  
pp. 35-46 ◽  
Author(s):  
Daisy Huang ◽  
Jonah H. Lee

AbstractAn attempt is made to obtain and quantify the mechanical properties of two common types of seasonal snow on the ground. Different samples of natural snow whose metamorphism had stabilized (such as would remain on a road throughout winter in a cold, snowy area) were gathered and tested using mesoscale indentation tests (metrics on the order of mm to cm). Results from the stress vs displacement curves from indentation indicated that (1) first peak strength decreased, according to a power law, with increasing indenter size and was not affected by snow average grain size, (2) plateau strength decreased with increasing indenter size, and snow compaction strength might be calculated from these data, and (3) mean energy absorption density during indentation was independent of indenter size in some size ranges, and decreased with increasing indenter size in other size ranges.


2014 ◽  
Vol 20 (4) ◽  
pp. 285-295
Author(s):  
Ana Alil ◽  
Miljana Popović ◽  
Tamara Radetić ◽  
Endre Romhanji

In this study, fully annealed AA5083 type alloy sheets with 1 mm in thickness were processed by accumulative roll bonding (ARB) at room temperature, up to 6 ARB cycles. It was found that microstructure was refined and mechanical properties were significantly improved with ARB processing. The maximum achieved values of hardness and tensile strength were two and three times greater than that of the initial material, respectively. This was attributed to the intensive strain hardening and grain size refinement which occurred during ARB deformation. However, the uniform elongation values were decreased by increasing the number of ARB cycles, and early fracture was registered. SEM fractography of fractured surfaces after tensile tests revealed a typical ductile fracture of ARB processed specimens, which was changed with ARB deformation. It was observed that ductile area on the fractured surfaces and the amount of necking, which occured before fracture, were decreased with increasing the number of ARB cycles. 


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