scholarly journals Characterization of Porous Phosphate Coatings Enriched with Calcium, Magnesium, Zinc and Copper Created on CP Titanium Grade 2 by Plasma Electrolytic Oxidation

Metals ◽  
2018 ◽  
Vol 8 (6) ◽  
pp. 411 ◽  
Author(s):  
Krzysztof Rokosz ◽  
Tadeusz Hryniewicz ◽  
Wojciech Kacalak ◽  
Katarzyna Tandecka ◽  
Steinar Raaen ◽  
...  
Keyword(s):  
Plasma Electrolytic Oxidation ◽  
Phosphate Coatings ◽  
Electrolytic Oxidation ◽  
Calcium Magnesium ◽  
Titanium Grade ◽  
Plasma Electrolytic ◽  
Porous Phosphate

scholarly journals Characterization of Porous Phosphate Coatings Enriched with Magnesium or Zinc on CP Titanium Grade 2 under DC Plasma Electrolytic Oxidation

Metals ◽  
2018 ◽  
Vol 8 (2) ◽  
pp. 112 ◽  
Author(s):  
Krzysztof Rokosz ◽  
Tadeusz Hryniewicz ◽  
Sofia Gaiaschi ◽  
Patrick Chapon ◽  
Steinar Raaen ◽  
...  
Keyword(s):  
Plasma Electrolytic Oxidation ◽  
Dc Plasma ◽  
Phosphate Coatings ◽  
Electrolytic Oxidation ◽  
Titanium Grade ◽  
Plasma Electrolytic ◽  
Porous Phosphate

scholarly journals Characterization of Porous Phosphate Coatings Created on CP Titanium Grade 2 Enriched with Calcium, Magnesium, Zinc and Copper by Plasma Electrolytic Oxidation

2018 ◽  
Author(s):  
Krzysztof Rokosz ◽  
Tadeusz Hryniewicz ◽  
Steinar Raaen ◽  
Sofia Gaiaschi ◽  
Patrick Chapon ◽  
...  
Keyword(s):  
Amorphous Phase ◽  
Plasma Electrolytic Oxidation ◽  
Titanium Substrate ◽  
Porous Coating ◽  
Phosphate Coatings ◽  
Electrolytic Oxidation ◽  
Calcium Magnesium ◽  
Titanium Grade ◽  
Plasma Electrolytic ◽  
Peo Coatings

In the paper, the effect of voltage increasing (from 500 VDC up to 650 VDC) on the structure and chemical composition of porous coating on titanium made by Plasma Electrolytic Oxidation, is presented. In the present paper, phosphates based coatings enriched with calcium, magnesium, zinc and copper in electrolyte based on 1 L of 85% concentrated H3PO4 with additions of Ca(NO3)2·4H2O, and Mg(NO3)2∙6H2O, and Zn(NO3)2∙6H2O, and Cu(NO3)2∙3H2O, are described. The morphology, chemical and phase composition, are evaluated using SEM, EDS, XRD, XPS, GDOES. Based on all the analyses, it was found out that the PEO coatings are porous and enriched with calcium, magnesium, zinc and copper. They consist mainly of the amorphous phase, which is more visible for higher voltages, and it is correlated with the increasing of the total PEO coating thickness (the higher the voltage, the thicker the PEO coating). However, for 650 VDC an amorphous phase and titanium substrate was also recorded with a signal from Ti2P2O7 crystalline, that was not observed for lower voltages. It was also found out that all the obtained coatings may be divided in three sub-layers, i.e. porous, semiporous, and transition one.

scholarly journals SEM and EDS Characterization of Porous Coatings Obtained On Titaniumby Plasma Electrolytic Oxidation in Electrolyte Containing Concentrated Phosphoric Acid with Zinc Nitrate

2017 ◽  
Vol 17 (2) ◽  
pp. 41-54 ◽  
Author(s):  
K. Rokosz ◽  
T. Hryniewicz ◽  
K. Pietrzak ◽  
W. Malorny
Keyword(s):  
Phosphoric Acid ◽  
Plasma Electrolytic Oxidation ◽  
Pure Titanium ◽  
Zinc Nitrate ◽  
Porous Coatings ◽  
Electrolytic Oxidation ◽  
Micro Arc Oxidation ◽  
Plasma Electrolytic ◽  
Peo Coatings

AbstractThe SEM and EDS results of porous coatings formed on pure titanium by Plasma Electrolytic Oxidation (Micro Arc Oxidation) under DC regime of voltage in the electrolytes containing of 500 g zinc nitrate Zn(NO3)2·6H2O in 1000 mL of concentrated phosphoric acid H3PO4at three voltages, i.e. 450 V, 550 V, 650 V for 3 minutes, are presented. The PEO coatings with pores, which have different shapes and the diameters, consist mainly of phosphorus, titanium and zinc. The maximum of zinc-to-phosphorus (Zn/P) ratio was found for treatment at 650 V and it equals 0.43 (wt%) | 0.20 (at%), while the minimum of that coefficient was recorded for the voltage of 450 V and equaling 0.26 (wt%) | 0.12 (at%). Performed studies have shown a possible way to form the porous coatings enriched with zinc by Plasma Electrolytic Oxidation in electrolyte containing concentrated phosphoric acid H3PO4with zinc nitrate Zn(NO3)2·6H2O.

scholarly journals Microstructure and Corrosion Characterization of a MgO/Hydroxyapatite Bilayer Coating by Plasma Electrolytic Oxidation Coupled with Flame Spraying on a Mg Alloy

ACS Omega ◽  
2020 ◽  
Vol 5 (38) ◽  
pp. 24186-24194
Author(s):  
Marzieh Mardali ◽  
Hamidreza Salimijazi ◽  
Fathallah Karimzadeh ◽  
Carsten Blawert ◽  
Bérengère J. C. Luthringer-Feyerabend ◽  
...  
Keyword(s):  
Plasma Electrolytic Oxidation ◽  
Mg Alloy ◽  
Flame Spraying ◽  
Bilayer Coating ◽  
Electrolytic Oxidation ◽  
Plasma Electrolytic
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