scholarly journals Glow Discharge Optical Emission Spectrometer Calibration Using Hydrogenated Zr-2.5Nb Alloy Standard Samples

Metals ◽  
2018 ◽  
Vol 8 (5) ◽  
pp. 372 ◽  
Author(s):  
Tatyana Priamushko ◽  
Andrey Mikhaylov ◽  
Maria Babikhina ◽  
Viktor Kudiiarov ◽  
Roman Laptev
2001 ◽  
Vol 55 (3) ◽  
pp. 292-297 ◽  
Author(s):  
Shigeharu Kimura ◽  
Yasuhiro Mitsui

We have studied the effect of optical interference on element profiles obtained with a glow discharge optical emission spectrometer (GDS). The specimens were borophosphosilicate glass films deposited on polished silicon wafers. We found that in some cases the interference is accompanied with a beat in the profile: a damping of the sinusoidal wave followed by a recovery. Profilometry showed that the depth resolution is better when the interference continues continuously without a beat. We showed by simulation that the cause of the beat came from variation of the penetration rate throughout the sputtered area.


Author(s):  
Monika Gorska ◽  
Pawel Pohl

Atmospheric pressure glow discharge (APGD) microplasma, sustained between a flowing liquid cathode (FLC) and a tungsten anode, was applied for the determination of Ca, K, Mg, and Na in fruit juices with a simplified sample preparation procedure.


2015 ◽  
Vol 754-755 ◽  
pp. 1017-1022 ◽  
Author(s):  
Petrică Vizureanu ◽  
Mirabela Georgiana Minciună ◽  
Dragoş Cristian Achiţei ◽  
Andrei Victor Sandu ◽  
Kamarudin Hussin

.The paper present aspects about the obtaining of non-precious dental alloys (type CoCrMo and CoCrMoSi7), the determination of chemical composition by optical emission spectrometry and the experimental tests for determining the tensile strength, made on standard plate samples. The base material used in experiments was a commercial alloy, from CoCrMo system, which belongs to the class of dental non-precious alloys, intended to medical applications. The obtaining of studied alloy was made on arc re-melting installation, under vacuum, type MRF ABJ 900. The process followed to realize a rapid melting, with a maximum admissible current intensity. The samples for tests were obtained by casting in an electric arc furnace, under vacuum, in optimal conditions for melting and solidification and processing by electro-erosion, to eliminate all the disturbing factors which come by processing conditions for the samples. The determination of chemical composition for cobalt based alloys, by optical emission spectrometry, was made on SpectromaxX equipment with spark. The electrical discharge is made with the elimination of an energy quantity, fact which determine plasma forming and light issue. Tensile tests for standard samples, made from cobalt based alloy, was made on Instron 3382 testing machine, and assisted by computer. The obtained results are: elongation, elasticity modulus, tensile strength and offer complete information about the analyzed mechanical properties. For the certitude of obtained experimental results, the tests were made on samples with specific dimensions according ISO 6892-1:2009(E) standard, both for the tensile strength, and also machine operation.


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