scholarly journals In Situ Alloying of a Modified Inconel 625 via Laser Powder Bed Fusion: Microstructure and Mechanical Properties

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 988
Author(s):  
Giulio Marchese ◽  
Margherita Beretta ◽  
Alberta Aversa ◽  
Sara Biamino
Keyword(s):  
Mechanical Properties ◽  
Base Alloy ◽  
Heat Treatments ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Composition Modification

This study investigates the in situ alloying of a Ni-based superalloy processed by means of laser powder bed fusion (LPBF). For this purpose, Inconel 625 powder is mixed with 1 wt.% of Ti6Al4V powder. The modified alloy is characterized by densification levels similar to the base alloy, with relative density superior to 99.8%. The material exhibits Ti-rich segregations along the melt pool contours. Moreover, Ti tends to be entrapped in the interdendritic areas during solidification in the as-built state. After heat treatments, the modified Inconel 625 version presents greater hardness and tensile strengths than the base alloy in the same heat-treated conditions. For the solution annealed state, this is mainly attributed to the elimination of the segregations into the interdendritic structures, thus triggering solute strengthening. Finally, for the aged state, the further increment of mechanical properties can be attributed to a more intense formation of phases than the base alloy, due to elevated precipitation strengthening ability under heat treatments. It is interesting to note how slight chemical composition modification can directly develop new alloys by the LPBF process.

scholarly journals In Situ Formation of a Metastable β-Ti Alloy by Laser Powder Bed Fusion (L-PBF) of Vanadium and Iron Modified Ti-6Al-4V

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1067 ◽  
Author(s):  
Florian Huber ◽  
Thomas Papke ◽  
Christian Scheitler ◽  
Lukas Hanrieder ◽  
Marion Merklein ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Homogeneous Element ◽  
Alloy Formation ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Β Phase ◽  
Stabilizing Effect

The aim of this work is to investigate the β-Ti-phase-stabilizing effect of vanadium and iron added to Ti-6Al-4V powder by means of heterogeneous powder mixtures and in situ alloy-formation during laser powder bed fusion (L-PBF). The resulting microstructure was analyzed by metallographic methods, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). The mechanical properties were characterized by compression tests, both prior to and after heat-treating. Energy dispersive X-ray spectroscopy showed a homogeneous element distribution, proving the feasibility of in situ alloying by LPBF. Due to the β-phase-stabilizing effect of V and Fe added to Ti-6Al-4V, instead of an α’-martensitic microstructure, an α/β-microstructure containing at least 63.8% β-phase develops. Depending on the post L-PBF heat-treatment, either an increased upsetting at failure (33.9%) compared to unmodified Ti-6Al-4V (28.8%), or an exceptional high compressive yield strength (1857 ± 35 MPa compared to 1100 MPa) were measured. The hardness of the in situ alloyed material ranges from 336 ± 7 HV0.5, in as-built condition, to 543 ± 13 HV0.5 after precipitation-hardening. Hence, the range of achievable mechanical properties in dependence of the post-L-PBF heat-treatment can be significantly expanded in comparison to unmodified Ti-6Al-4V, thus providing increased flexibility for additive manufacturing of titanium parts.

scholarly journals Microstructure and Residual Stress Evolution of Laser Powder Bed Fused Inconel 718 under Heat Treatments

2020 ◽  
Author(s):  
Giulio Marchese ◽  
Eleonora Atzeni ◽  
Alessandro Salmi ◽  
Sara Biamino
Keyword(s):  
Residual Stresses ◽  
Inconel 718 ◽  
Heat Treatments ◽  
Powder Bed Fusion ◽  
Stress Evolution ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Sintering Mechanisms ◽  
Dendritic Structures

AbstractThe current work aimed to study the influence of various heat treatments on the microstructure, hardness, and residual stresses of Inconel 718 processed by laser powder bed fusion process. The reduction in residual stresses is crucial to avoid the deformation of the component during its removal from the building platform. Among the different heat treatments, 800 °C kept almost unaltered the original microstructure, reducing the residual stresses. Heat treatments at 900, 980, and 1065 °C gradually triggered the melt pool and dendritic structures dissolution, drastically reducing the residual stresses. Heat treatments at 900 and 980 °C involved the formation of δ phases, whereas 1065 °C generated carbides. These heat treatments were also performed on components with narrow internal channels revealing that heat treatments up to 900 °C did not trigger sintering mechanisms allowing to remove the powder from the inner channels.

scholarly journals In situ microstructure analysis of Inconel 625 during laser powder bed fusion

2021 ◽  
Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  
Keyword(s):  
Laser Power ◽  
Scanning Speed ◽  
High Energy ◽  
Mechanical Anisotropy ◽  
Ex Situ ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract

scholarly journals In Situ Thermography During Laser Powder Bed Fusion of a Nickel Superalloy 625 Artifact with Various Overhangs and Supports

2021 ◽  
Vol 126 ◽  
Author(s):  
Benjamin Molnar ◽  
Jarred C. Heigel ◽  
Eric Whitenton
Keyword(s):  
Cooling Rate ◽  
High Speed ◽  
Nickel Superalloy ◽  
Powder Bed Fusion ◽  
Support Structures ◽  
Radiance Temperature ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool

This document provides details on the experiment and associated measurement files available fordownload in the dataset “In Situ Thermography During Laser Powder Bed Fusion of a Nickel Superalloy 625 Artifact with Various Overhangs and Supports.” The measurements were acquired during the fabrication of a small nickel superalloy 625 (IN625) artifact using a commercial laser powder bed fusion (LPBF) system. The artifact consists of two half-arch features with increasing slopes for overhangs. These overhangs range from 5° from vertical to 85° from vertical in increments of 10°. The artifact geometry and process are controlled to ensure consistent processing along the overhang geometry. This control enables the effect of overhang geometry and support structures to be isolated from effects of inter-layer scan strategy variations. The measurements include high-speed thermography of each layer, from which radiance temperature, cooling rate, and melt pool length are calculated.

scholarly journals Linking In Situ Melt Pool Monitoring to Melt Pool Size Distributions and Internal Flaws in Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1856
Author(s):  
Claudia Schwerz ◽  
Lars Nyborg
Keyword(s):  
Near Infrared ◽  
In Situ Monitoring ◽  
Ex Situ ◽  
Process Conditions ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Melt Pool Size

In situ monitoring of the melt pools in laser powder bed fusion (LPBF) has enabled the elucidation of process phenomena. There has been an increasing interest in also using melt pool monitoring to identify process anomalies and control the quality of the manufactured parts. However, a better understanding of the variability of melt pools and the relation to the incidence of internal flaws are necessary to achieve this goal. This study aims to link distributions of melt pool dimensions to internal flaws and signal characteristics obtained from melt pool monitoring. A process mapping approach is employed in the manufacturing of Hastelloy X, comprising a vast portion of the process space. Ex situ measurements of melt pool dimensions and analysis of internal flaws are correlated to the signal obtained through in situ melt pool monitoring in the visible and near-infrared spectra. It is found that the variability in melt pool dimensions is related to the presence of internal flaws, but scatter in melt pool dimensions is not detectable by the monitoring system employed in this study. The signal intensities are proportional to melt pool dimensions, and the signal is increasingly dynamic following process conditions that increase the generation of spatter.

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