scholarly journals Texture Selection Mechanisms during Recrystallization and Grain Growth of a Magnesium-Erbium-Zinc Alloy

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 171
Author(s):  
Fatim-Zahra Mouhib ◽  
Fengyang Sheng ◽  
Ramandeep Mandia ◽  
Risheng Pei ◽  
Sandra Korte-Kerzel ◽  
...  
Keyword(s):  
Grain Growth ◽  
Ternary Alloy ◽  
Solute Drag ◽  
Tensile Tests ◽  
Electron Back Scatter Diffraction ◽  
Zinc Alloy ◽  
Uniaxial Tensile ◽  
Microstructural Stability ◽  
Solid Solution Strengthening ◽  
Zener Drag

Binary and ternary Mg-1%Er/Mg-1%Er-1%Zn alloys were rolled and subsequently subjected to various heat treatments to study texture selection during recrystallization and following grain growth. The results revealed favorable texture alterations in both alloys and the formation of a unique ±40° transvers direction (TD) recrystallization texture in the ternary alloy. While the binary alloy underwent a continuous alteration of its texture and grain size throughout recrystallization and grain growth, the ternary alloy showed a rapid rolling (RD) to transvers direction (TD) texture transition occurring during early stages of recrystallization. Targeted electron back scatter diffraction (EBSD) analysis of the recrystallized fraction unraveled a selective growth behavior of recrystallization nuclei with TD tilted orientations that is likely attributed to solute drag effect on the mobility of specific grain boundaries. Mg-1%Er-1%Zn additionally exhibited a stunning microstructural stability during grain growth annealing. This was attributed to a fine dispersion of dense nanosized particles in the matrix that impeded grain growth by Zener drag. The mechanical properties of both alloys were determined by uniaxial tensile tests combined with EBSD assisted slip trace analysis at 5% tensile strain to investigate non-basal slip behavior. Owing to synergic alloying effects on solid solution strengthening and slip activation, as well as precipitation hardening, the ternary Mg-1%Er-1%Zn alloy demonstrated a remarkable enhancement in the yield strength, strain hardening capability, and failure ductility, compared with the Mg-1%Er alloy.

Effects of Driving Force and Boundary Migration Velocity on Formation of Recrystallization Texture in Cold Rolled Pure Aluminum Sheets

2013 ◽  
Vol 753 ◽  
pp. 257-262 ◽  
Author(s):  
Wei Min Mao ◽  
Ping Yang
Keyword(s):  
Grain Growth ◽  
Driving Force ◽  
Recrystallization Texture ◽  
Pure Aluminum ◽  
Solute Drag ◽  
Texture Formation ◽  
Oriented Growth ◽  
Aluminum Sheets ◽  
Zener Drag ◽  
Cold Rolled

The effects of net driving force for migration of high angle grain boundaries were emphasized beside many other factors which could influence the process of texture formation during recrystallization annealing of 95% cold rolled pure aluminum sheets. The net driving force consists basically of stored energy. However, it could be reduced by recovery, boundary drag, solute drag and Zener drag in different extents, in which only boundary drag is mis-orientation dependent. It was indicated that both oriented nucleation and oriented growth have obvious influence on recrystallization texture, and how far they influence the texture depends also on the level of net driving force when the grain growth starts during annealing. Oriented growth, which is induced by the differences in boundary drag of differently oriented grains, and the corresponding texture formation, could be observed easily when the recrystallization proceeds under relative higher solute drag and Zener drag in commercial purity aluminum. The oriented nucleation process prevails during recrystallization of sufficiently recovered high purity aluminum with very low solute drag and Zener drag, after which strong cube texture forms. In this case the oriented growth indicates limited effect. Both the oriented growth and oriented nucleation will fail if high purity deformation matrix without clear solute drag and Zener drag has not experienced an obvious recovery before recrystallization grain growth, since extremely high net driving force leads to very small critical nucleus size and multiplicity of growing grains, which results in randomization of recrystallization texture.

The Effect of Cooling Rate on the Damage Micromechanisms of DP Steels

2010 ◽  
Vol 638-642 ◽  
pp. 3337-3342 ◽  
Author(s):  
Orlando León-García ◽  
Roumen H. Petrov ◽  
Leo Kestens
Keyword(s):  
Void Nucleation ◽  
Shear Bands ◽  
Tensile Tests ◽  
Electron Back Scatter Diffraction ◽  
Uniaxial Tensile ◽  
Localized Deformation ◽  
Slow Cooling ◽  
Dp Steel ◽  
Carry Capacity ◽  
Steel Sheets

The microstructural failure mechanisms of two DP steel sheets cooled with different cooling rates during their heat treatment are compared in the present study. The as-cold rolled DP steel sheets were annealed at intercritical temperature and cooled down with rates of 45°C/s (quenching) and 2 °C/s (slow cooling). Uniaxial tensile tests were carried out on samples from both sheets and the microstructure of undeformed samples and the broken tensile specimens was evaluated by optical microscopy, scanning electron microscopy and electron back-scatter diffraction technique. Although the grain size did not show significant differences, the amount and size of the constituents, e.g. martensite and bainite, differ between both alloys. Concerning the mechanical properties, the quenched material showed superior strength and ductility besides a less localized deformation at higher strains. The area fraction of voids in the broken specimens was low for both steels. In the slow cooled samples the nucleation of shear bands was on the large voids and cracks were observed along these shears bands. It was concluded that the detrimental effect of void nucleation on both steels is not only attributed to their null-carry capacity but more to the stress concentration close to the voids which gives rise to strain localization in the form of shear bands.

Superplasticity in CP-Titanium Alloys

2007 ◽  
Vol 551-552 ◽  
pp. 373-378 ◽  
Author(s):  
X.J. Zhu ◽  
Ming Jen Tan ◽  
K.M. Liew
Keyword(s):  
High Temperature ◽  
Grain Growth ◽  
Initial Strain Rate ◽  
Tensile Tests ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Uniaxial Tensile ◽  
Step Method ◽  
Commercially Pure ◽  
Effects Of Temperature

In this work, studies were carried out to investigate the superplasticity of a commercially pure (CP) titanium alloy during high temperature deformation. Uniaxial tensile tests were carried out at 600, 750 and 800°C with an initial strain rate from 10-1s-1 to 10-4s-1. It was found that the alloy do not show good superplasticity due fast grain growth at high temperature and cavity. The effects of temperature on the grain growth and cavity phenomena as well as the dynamic recrystallization of the alloy were studied and a ‘two-step-method’ was introduced to increase the superplasticity of the alloy.

Microstructure Instability during Particle and Solute Inhibited Grain Growth

2012 ◽  
Vol 715-716 ◽  
pp. 528-528
Author(s):  
Massimiliano Buccioni ◽  
Giuseppe Carlo Abbruzzese
Keyword(s):  
Grain Size ◽  
Size Distribution ◽  
Grain Growth ◽  
Grain Size Distribution ◽  
Ostwald Ripening ◽  
Secondary Recrystallization ◽  
Solute Drag ◽  
Abnormal Grain Growth ◽  
Second Phase ◽  
Zener Drag

Grain growth processes in real polycrystalline materials are mostly characterized by the presence of restraining forces, originating, among others, from second phase particles dispersion (Zener drag) or solute atoms segregating at the grain boundaries (solute drag). Both the restraining mechanisms were introduced in the framework of the statistical theory of grain growth, showing their peculiar effects on kinetics and on grain size distribution evolution [1,2,. The present work moves from the previous results and gives a further clarification of pseudo-steady state kinetics occurring under particular solute drag inhibition intensity and will discuss it in comparison with grain growth stagnation conditions produced by Zener drag. In case of second phase particle inhibiting grain growth, the normal case in real systems is the time and temperature dependence of the inhibition intensity due to the evolution of precipitates (e.g. Ostwald ripening. Such evolutions of inhibition, which typically drops with increasing temperature, can cause microstructure instabilities like abnormal grain growth or secondary recrystallization. It is thus introduced in the model a time-temperature depending inhibition drop, which influences both kinetics and grain size distribution evolution. Conditions for the onset of particular effects like abnormal grain growth are assessed and discussed.

Microstructural characterization of a rapidly solidified Al-Fe-V-Si alloy for elevated temperature applications

1988 ◽  
Vol 46 ◽  
pp. 550-551
Author(s):  
R. E. Franck ◽  
J. A. Hawk ◽  
G. J. Shiflet
Keyword(s):  
High Temperature ◽  
Elevated Temperature ◽  
Grain Growth ◽  
Volume Fraction ◽  
Microstructural Characterization ◽  
Second Phase ◽  
Microstructural Stability ◽  
Elevated Temperature Strength ◽  
Temperature Applications

Rapid solidification processing (RSP) is one method of producing high strength aluminum alloys for elevated temperature applications. Allied-Signal, Inc. has produced an Al-12.4 Fe-1.2 V-2.3 Si (composition in wt pct) alloy which possesses good microstructural stability up to 425°C. This alloy contains a high volume fraction (37 v/o) of fine nearly spherical, α-Al12(Fe, V)3Si dispersoids. The improved elevated temperature strength and stability of this alloy is due to the slower dispersoid coarsening rate of the silicide particles. Additionally, the high v/o of second phase particles should inhibit recrystallization and grain growth, and thus reduce any loss in strength due to long term, high temperature annealing.The focus of this research is to investigate microstructural changes induced by long term, high temperature static annealing heat-treatments. Annealing treatments for up to 1000 hours were carried out on this alloy at 500°C, 550°C and 600°C. Particle coarsening and/or recrystallization and grain growth would be accelerated in these temperature regimes.

Comprehensive study on mechanical properties of coated biaxial warp-knitted fabrics

2021 ◽  
pp. 073168442110204
Author(s):  
Bin Yang ◽  
Yingying Shang ◽  
Zeliang Yu ◽  
Minger Wu ◽  
Youji Tao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Failure Modes ◽  
Least Squares Method ◽  
Tensile Tests ◽  
Tensile Creep ◽  
Base Layer ◽  
Sustained Load ◽  
Uniaxial Tensile ◽  
Membrane Structures ◽  
Knitted Fabrics

In recent years, coated fabrics have become the major material used in membrane structures. Due to the special structure of base layer and mechanical properties, coated biaxial warp-knitted fabrics are increasingly applied in pneumatic structures. In this article, the mechanical properties of coated biaxial warp-knitted fabrics are investigated comprehensively. First, off-axial tensile tests are carried out in seven in-plane directions: 0°, 15°, 30°, 45°, 60°, 75°, and 90°. Based on the stress–strain relationship, tensile strengths are obtained and failure modes are studied. The adaptability of Tsai–Hill criterion is analyzed. Then, the uniaxial tensile creep test is performed under 24-h sustained load and the creep elongation is calculated. Besides, tearing strengths in warp and weft directions are obtained by tearing tests. Finally, the biaxial tensile tests under five different load ratios of 1:1, 2:1, 1:2, 1:0, and 0:1 are carried out, and the elastic constants and Poisson’s ratio are calculated using the least squares method based on linear orthotropic assumption. Moreover, biaxial specimens under four load ratios of 3:1, 1:3, 5:1, and 1:5 are further tensile tested to verify the adaptability of linear orthotropic model. These experimental data offer a deeper and comprehensive understanding of mechanical properties of coated biaxial warp-knitted fabrics and could be conveniently adopted in structural design.

The Effect of Grain Size on Superplastic Deformation of Ti-6Al-4V Alloy

2007 ◽  
Vol 551-552 ◽  
pp. 387-392 ◽  
Author(s):  
Wen Juan Zhao ◽  
Hua Ding ◽  
D. Song ◽  
F.R. Cao ◽  
Hong Liang Hou
Keyword(s):  
Grain Size ◽  
Grain Growth ◽  
Superplastic Deformation ◽  
Initial Strain Rate ◽  
Deformation Mode ◽  
Tensile Tests ◽  
Optical Microscope ◽  
Coarse Grained ◽  
Transmission Electron ◽  
Grain Growth Model

In this study, superplastic tensile tests were carried out for Ti-6Al-4V alloy using different initial grain sizes (2.6 μm, 6.5μm and 16.2 μm) at a temperature of 920°C with an initial strain rate of 1×10-3 s-1. To get an insight into the effect of grain size on the superplastic deformation mechanisms, the microstructures of deformed alloy were investigated by using an optical microscope and transmission electron microscope (TEM). The results indicate that there is dramatic difference in the superplastic deformation mode of fine and coarse grained Ti-6Al-4V alloy. Meanwhile, grain growth induced by superplastic deformation has also been clearly observed during deformation process, and the grain growth model including the static and strain induced part during superplastic deformation was utilized to analyze the data of Ti-6Al-4V alloy.

scholarly journals A Flow Stress Model of 300M Steel for Isothermal Tension

Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 252
Author(s):  
Rongchuang Chen ◽  
Shiyang Zhang ◽  
Xianlong Liu ◽  
Fei Feng
Keyword(s):  
Flow Stress ◽  
Constitutive Model ◽  
Tensile Deformation ◽  
Flow Behavior ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Model Parameters ◽  
Average Deviation ◽  
Cross Sectional ◽  
300M Steel

To investigate the effect of hot working parameters on the flow behavior of 300M steel under tension, hot uniaxial tensile tests were implemented under different temperatures (950 °C, 1000 °C, 1050 °C, 1100 °C, 1150 °C) and strain rates (0.01 s−1, 0.1 s−1, 1 s−1, 10 s−1). Compared with uniaxial compression, the tensile flow stress was 29.1% higher because dynamic recrystallization softening was less sufficient in the tensile stress state. The ultimate elongation of 300M steel increased with the decrease of temperature and the increase of strain rate. To eliminate the influence of sample necking on stress-strain relationship, both the stress and the strain were calibrated using the cross-sectional area of the neck zone. A constitutive model for tensile deformation was established based on the modified Arrhenius model, in which the model parameters (n, α, Q, ln(A)) were described as a function of strain. The average deviation was 6.81 MPa (6.23%), showing good accuracy of the constitutive model.

Recrystallization, Grain Growth in Copper Foil at High Temperature Studied By Electron Back Scatter Diffraction

2011 ◽  
Author(s):  
Pragya Tiwari ◽  
Himanshu Srivastava ◽  
Sanjay Rai ◽  
S. K. Deb ◽  
Alka B. Garg ◽  
...  
Keyword(s):  
High Temperature ◽  
Grain Growth ◽  
Copper Foil ◽  
Electron Back Scatter Diffraction

Experimental Investigation of Ti-6Al-4V with a Biaxial Tensile Test Setup at Elevated Temperature

2014 ◽  
Vol 622-623 ◽  
pp. 273-278 ◽  
Author(s):  
Marion Merklein ◽  
Sebastian Suttner ◽  
Adam Schaub
Keyword(s):  
Elevated Temperature ◽  
Elevated Temperatures ◽  
Tensile Tests ◽  
Advanced Materials ◽  
Uniaxial Tensile ◽  
Plastic Yielding ◽  
Characterization Methods ◽  
Specific Strength ◽  
Biaxial Tensile ◽  
Stress States

The requirement for products to reduce weight while maintaining strength is a major challenge to the development of new advanced materials. Especially in the field of human medicine or aviation and aeronautics new materials are needed to satisfy increasing demands. Therefore the titanium alloy Ti-6Al-4V with its high specific strength and an outstanding corrosion resistance is used for high and reliable performance in sheet metal forming processes as well as in medical applications. Due to a meaningful and accurate numerical process design and to improve the prediction accuracy of the numerical model, advanced material characterization methods are required. To expand the formability and to skillfully use the advantage of Ti-6Al-4V, forming processes are performed at elevated temperatures. Thus the investigation of plastic yielding at different stress states and at an elevated temperature of 400°C is presented in this paper. For this reason biaxial tensile tests with a cruciform shaped specimen are realized at 400°C in addition to uniaxial tensile tests. Moreover the beginning of plastic yielding is analyzed in the first quadrant of the stress space with regard to complex material modeling.

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