scholarly journals The Effect of Drawing Deformation Rate Induced Inhomogeneous Local Distortion on Phase Transformation of 304H Stainless Wire

Metals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1304
Author(s):  
Qinhua Xu ◽  
Zhixian Peng ◽  
Jianxin Zhu ◽  
Mingyang Li ◽  
Yong Zong ◽  
...  

The micro/macro magnetic properties, local element distribution, martensite transformation, and mechanical properties of 304H stainless wires are determined for two cold drawing chains. Finite element simulations are used to analyse the local strain and heat generation. The results show that there is obvious inhomogeneity in the magnetic properties, strain/stress relationship, and strain-induced heat within the drawn wires. Comparing wires with the same total strain, a larger area reduction of previous drawing processes contributes to a higher volume of the martensite phase, while a smaller area reduction of the first process results in an inhibited phase transformation. A higher single strain in the first drawing process leads to additional heat generation at the subsurface of the wire, which would eventually retard the martensite transformation. The inhomogeneous deformation-induced differences in the grain size affect the stability of austenite and transform the final martensite.

2010 ◽  
Vol 168-169 ◽  
pp. 204-207 ◽  
Author(s):  
E.G. Gerasimov ◽  
S.M. Podgonykh ◽  
N.V. Mushnikov ◽  
V.P. Dyakina ◽  
T. Kanomata

Magnetic properties, electrical resistivity and magnetoresistance of the Ni50Mn37(Sn1 xInx)13 (x=0.2, 0.5) Heusler alloys were studied in magnetic fields up to 360 kOe in the temperature range 4-400 K. It was found that the alloys exhibit a martensite phase transformation at a critical temperature TM240 K for x=0.2 and TM350 K for x=0.5. The TM temperature is lower than the Curie temperature of the austenite phase TCA in the alloy with x=0.2 and is higher than TCA in the alloy with x=0.5. The spontaneous martensite transformation in both alloys is accompanied by a large change (~48%) of the electrical resistivity. A large negative magnetoresistance (~45%) is observed for the alloy with x=0.2 upon the field-induced martensite transformation. The analysis of the obtained results allows us to conclude that the large magnetoresistance in the alloys is mainly due to the changes in the crystal structure and only slightly depends on the changes in the magnetic ordering.


2019 ◽  
Vol 116 (6) ◽  
pp. 614
Author(s):  
Li Chang ◽  
Gao Jingxiang ◽  
Zhang Dacheng ◽  
Chen Zhengwei ◽  
Han Xing

Obtaining an accurate microscopic representation of the martensitic transformation process is key to realizing the best performance of materials and is of great significance in the field of material design. Due to the martensite phase transformation is rapidly, the current experimental is hard to capture all the information in the Martensite phase transformation process. Combining the phase-field method with the finite-element method, a model of martensitic transformation from a metastable state to a steady state is established. The law of a single martensite nucleus during martensitic transformation is accurately described. By changing the key materials that affect martensite transformation and the phase-field parameters, the effects of the parameters on the single martensitic nucleation process are obtained. This study provides an important theoretical basis for effectively revealing the essence of martensite transformation and can determine effective ways to influence martensite transformation, obtain the optimal parameters and improve the mechanical properties of such materials.


2009 ◽  
Vol 79-82 ◽  
pp. 1699-1702
Author(s):  
Xiao Peng Gao ◽  
Fu Shun Liu

The phase transformation characteristics, the dynamic elastic modulus and the static tensile elastic modulus of Ti50Ni47.5Fe2.5 alloy were investigated. It is found that, the two mutations in the dynamic elastic modulus is caused by reverse martensite phase transformation and austenite phase transformation respectively; Static tensile test can not reflect the intrinsic elastic modulus when the test temperature is close to martensite transformation temperature(Ms). The static elastic modulus and the dynamic elastic modulus have the same trend when the test temperature is enough higher than Ms.


2014 ◽  
Vol 682 ◽  
pp. 3-8 ◽  
Author(s):  
Svetlana A. Barannikova ◽  
Galina V. Shlyakhova ◽  
Lev Zuev

Using atomic force, optical and electron microscopy methods, the changes in the microstructure and phase composition were investigated for the alloy Nb47%Ti used for the manufacture of superconducting cable employed as current-carrying elements in the ITER magnetic system (abbr. for International Thermonuclear Experimental Reactor). The test samples were prepared from the superconducting wire at an intermediate step of the drawing process for the area reduction Ø1.3→Ø1.2 mm. The effect of cold drawing and intermediate annealing on the properties of as-worked Nb-Ti alloy was assessed. Local strain zones were found to occur in the rupture area. The shape and chemical composition of Nb-Ti wire was examined for both a defect-free area and the rupture area. A Nb diffusion barrier was found to occur in the copper matrix of Nb-Ti wire.


2018 ◽  
Vol 183 ◽  
pp. 03029
Author(s):  
Lin Wang ◽  
Anjin Liu ◽  
Huaxiang Dai ◽  
Feng Xu ◽  
Xinhua Min

In this paper, microstructure evolution and mechanic properties of metastable near β Ti-5553 alloy were investigated. SHPB, SHTB and light gas gun were employed to carry out the dynamic loadings. Microstructure evolution were characterized by OM, quantitative metallography and XRD. The experimental results demonstrated that stress-induced martensite transformation occur in metastable Ti-5553 alloy through SHPB, SHTB and plate impact loadings. In SHPB loading test, stress-induced martensite transformation is one of the methods that dissipate energy besides of adiabatic shear band, and also occur before ASB. In SHTB and SHPB+SHTB loading tests, the transformation amount of stressinduced martensite exhibit similar trend. In plate impact experiment, the content of martensite phase transformation increased with the impact velocity.


1999 ◽  
Vol 577 ◽  
Author(s):  
Q. Chen ◽  
B. M. Ma ◽  
B. Lu ◽  
M. Q. Huang ◽  
D. E. Laughlin

ABSTRACTThe phase transformation and the exchange coupling in (Ndo095Lao005)9.5FebaICOsNb 2BI05 have been investigated. Nanocomposites were obtained by treating amorphous precursors at temperatures ranging from 650TC to 9500C for 10 minutes. The magnetic properties were characterized via the vibrating sample magnetometer (VSM). X-ray diffraction (XRD), thermomagnetic analysis (TMA), and transmission electron microscopy (TEM) were used to perform phase identification, measure grain size, and analyze phase distribution. The strength of the exchange coupling between the magnetically hard and soft phases in the corresponding nanocomposite was analyzed via the AM-versus-H plot. It was found that the remanence (Br), coercivity (Hci), and maximum energy product (BHmax) obtained were affected by the magnetic phases present as well as the grain size of constituent phases and their distribution. The optimal magnetic performance, BHm, occurred between 700°C to 750°C, where the crystallization has completed without excessive grain growth. TMA and TEM indicated that the system was composed of three phases at this point, Nd2(Fe Co) 14B, ca-Fe, and Fe3B. The exchange coupling interaction among these phases was consistently described via the AM-versus-H plot up to 750°C. The Br, Hci, and BHmax degraded severely when the thermal treatment temperature increased from 750°C. This degradation may be attributed to the grain growth of the main phases, from 45 to 68nm, and the development of precipitates, which grew from 5nm at 750°C to 12nm at 850°C. Moreover, the amount of the precipitates was found to increase with the thermal treatment temperatures. The precipitates, presumably borides, may cause a decrease in the amount of the a-Fe and Fe 3B and result in a redistribution of the Co in the nanocomposites. The increase of the Co content in the Nd 2(Fe Co) 14B may explain the increase of its Curie temperature with the thermal treatment temperatures. In this paper, we examine the impacts of these factors on the magnetic properties of (Ndo 95Lao 05)9 5FebaICosNb2B10.5 nanocomposite.


2009 ◽  
Vol 479 (1-2) ◽  
pp. 78-81 ◽  
Author(s):  
L.Y. Li ◽  
A. Yan ◽  
J.H. Yi ◽  
G.T. Zhang ◽  
W. Xie ◽  
...  

Crystals ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 345 ◽  
Author(s):  
Weiya Li ◽  
Chunwang Zhao

The microstructure and martensitic transformation behavior of Ni50−xTi50Lax (x = 0.1, 0.3, 0.5, 0.7) shape memory alloys were investigated experimentally. Results show that the microstructure of Ni50−xTi50Lax alloys consists of a near-equiatomic TiNi matrix, LaNi precipitates, and Ti2Ni precipitates. With increasing La content, the amounts of LaNi and Ti2Ni precipitates demonstrate an increasing tendency. The martensitic transformation start temperature increases gradually with increasing La content. The Ni content is mainly responsible for the change in martensite transformation behavior in Ni50−xTi50Lax alloys.


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