scholarly journals Microstructure and Mechanical Properties Evolution during Solution and Ageing Treatment for a Hot Deformed, above β-transus, Ti-6246 Alloy

Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1114
Author(s):  
Mohammed Hayder Ismail Alluaibi ◽  
Elisabeta Mirela Cojocaru ◽  
Adrian Rusea ◽  
Nicolae Șerban ◽  
George Coman ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Mechanical Behaviour ◽  
Rolling Direction ◽  
Processing Route ◽  
Thermal Treatments ◽  
Deformation Degree ◽  
Fixed Temperature ◽  
Ageing Treatment ◽  
Thermal Solution ◽  
Strength And Ductility

The present study investigates the influence of hot-deformation, above β-transus and different thermal treatments on the microstructural and mechanical behaviour of a commercially available Ti-6246 titanium-based alloy, by SEM (scanning electron microscopy), tensile and microhardness testing techniques. The as-received Ti-6246 alloy was hot-deformed—HR by rolling, at 1000 °C, with a total thickness reduction (total deformation degree) of 65%, in 4 rolling passes. After HR, different thermal (solution—ST and ageing—A) treatments were applied in order to induce changes in the alloy’s microstructure and mechanical behaviour. The applied solution treatments (ST) were performed at temperatures below and above β-transus (α → β transition temperature; approx. 935 °C), to 800 °C, 900 °C and 1000 °C respectively, while ageing treatment at a fixed temperature of 600 °C. The STs duration was fixed at 27 min while A duration at 6 h. Microstructural characteristics of all thermomechanical (TM) processed samples and obtained mechanical properties were analysed and correlated with the TM processing conditions. The microstructure analysis shows that the applied TM processing route influences the morphology of the alloy’s constituent phases. The initial AR microstructure shows typical Widmanstätten/basket-weave-type grains which, after HR, are heavily deformed along the rolling direction. The STs induced the regeneration of α-Ti and β-Ti phases, as thin alternate lamellae/plate-like structures, showing preferred spatial orientation. Also, the STs induced the formation of α′-Ti/α″-Ti martensite phases within parent α-Ti/β-Ti phases. The ageing treatment (A) induces reversion of α′-Ti/α″-Ti martensite phases in parent α-Ti/β-Ti phases. Mechanical behaviour showed that both strength and ductility properties are influenced, also, by applied TM processing route, optimum properties being obtained for a ST temperature of 900 °C followed by ageing (ST2 + A state), when both strength and ductility properties are at their maximum (σUTS = 1279 ± 15 MPa, σ0.2 = 1161 ± 14 MPa, εf = 10.1 ± 1.3%).

Effect of Thermomechanical Treatment on Mechanical Behaviour and Microstructure of Low Alloy Steel

2012 ◽  
Vol 184-185 ◽  
pp. 838-849
Author(s):  
Mahmoud M. Tash
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Impact Toughness ◽  
Alloy Steel ◽  
Mechanical Behaviour ◽  
Hot Forging ◽  
Weight Ratio ◽  
Ultimate Tensile Stress ◽  
Low Alloy Steel ◽  
Strength And Ductility

The present study was undertaken to investigate the effect of thermo-mechanical treatment (TMT) on the microstructure and mechanical behaviour of low alloy steel. Hot forging is carried out at 1200°C using mechanical press of 500 and 800 ton. The effect of hot forging reduction ratios (1.11 and 1.29) on the hardness and mechanical properties are studied. TMT samples are given different heat treatment i.e. annealing (A), normalizing (N), hardening (H), hardening and tempering (H/T) and their corresponding impact toughness are obtained. Selected heat treatment (normalizing and annealing) are given to tensile test samples and their corresponding strength and ductility are obtained. Ultimate tensile, 0.2% offset yield strength and percent elongation are measured. Hardness and impact toughness measurements were carried out for all alloy conditions. Hardness (HV), ultimate tensile stress (UTS-MPa) and 0.2% offset yield stress (MPa) increases with increasing reduction ratio. TMT leads to a sharp rise in alloy hardness and strength. Normalizing and annealing following TMT revealed a low hardness values compared to those observed in the TMT condition. Annealing reduces hardness and strength but increases ductility and impact toughness. This could be attributed to the recovery and coarsening effect. Pro-eutectoid ferrite phase are observed along the grain boundaries of low alloy steel in the TMT conditions regardless of the reduction ratios. Normalized samples show a refined pearlitic microstructure while coarse pearlite is observed in the annealed one. Good mechanical properties can be obtained by a combination of plastic deformation and thermal treatment. Heat treatment is one of the major factors used to enhance the mechanical properties of low alloy steel. An understanding of the combined effect of TMT and subsequent heat treatment on the structure and mechanical properties of low alloy steel would help in selecting conditions required to achieve the optimum mechanical properties and alloy high strength to weight ratio. This may be achieved by measuring hardness, impact toughness, strength and ductility resulting from different heat treatment following TMT.

Mechanical Properties and Microstructure Observation with Grain Refinement in CuZnAl Alloy

2008 ◽  
Vol 569 ◽  
pp. 173-176 ◽  
Author(s):  
Gwon Seung Yang ◽  
Jong Kook Lee ◽  
Woo Yang Jang
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Refinement ◽  
Fracture Strength ◽  
Void Formation ◽  
Ageing Treatment ◽  
Microstructure Observation ◽  
Misch Metal ◽  
Coarse Grains ◽  
Strength And Ductility

A small amount of misch metal was added to CuZnAl alloy in order to study the effect of grain refinement and mechanical properties, phase transformation behavior and stabilization of martensite. It was found that the addition of misch metal was very effective for reducing the grain size. The coarse grains over 1000 μm have been refined to the size of 30 μm by the addition of 0.43wt% misch metal. The grain size of thermo-mechanically treated alloys was barely affected by cold working. The fracture strength and ductility have been significantly increased with the increase of misch metal content when tensile test is carried out below Mf temperature. Also, the fracture strength has been more increased in the case of post-quench ageing treatment than the direct quench ageing treatment. The fracture mode has been changed from transgranular brittle fracture to ductile fracture with void formation and coalescence by the addition of misch metal.

scholarly journals Influence of Post-Deposition Heat Treatments on the Microstructure and Tensile Properties of Ti-6Al-4V Parts Manufactured by CMT-WAAM

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1161
Author(s):  
Lexuri Vazquez ◽  
Maria Nieves Rodriguez ◽  
Iker Rodriguez ◽  
Pedro Alvarez
Keyword(s):  
Mechanical Properties ◽  
State Of The Art ◽  
Microstructural Analysis ◽  
Thermal Treatments ◽  
Cold Metal Transfer ◽  
Α Phase ◽  
Different Temperatures ◽  
Cold Metal ◽  
Post Deposition ◽  
Strength And Ductility

Cold metal transfer (CMT)-based wire and arc additive manufacturing (WAAM) of Ti-6Al-4V alloy has been investigated to manufacture walls with two different building strategies. This study focuses on the influence of the application of thermal treatments on the resulting microstructure and mechanical properties. Deep microstructural analysis revealed different grades of growth of lamellae α phase after several thermal treatments at different temperatures, which lead to different tensile mechanical properties and better strength and ductility balance compared to the as-built condition. Results are compared with equivalent forged and casting standards and the state of the art for WAAM of Ti-6Al-4V alloy. At temperatures of 920 °C, anisotropy was maintained and elongation increased by 70% while yield strength and UTS was slightly decreased by 8%.

Effect of Cold Rolling on Microstructure and Mechanical Properties of an Al-Mg-Sc-Zr Alloy

2014 ◽  
Vol 922 ◽  
pp. 388-393
Author(s):  
Vladislav Kulitskiy ◽  
Sergey Malopheyev ◽  
Rustam Kaibyshev
Keyword(s):  
Mechanical Properties ◽  
Cold Rolling ◽  
Shear Bands ◽  
Rolling Direction ◽  
Strong Increase ◽  
Deformation Bands ◽  
High Anisotropy ◽  
Order Deformation ◽  
Strength And Ductility ◽  
Zr Alloy

The microstructural evolution and mechanical properties of an Al-5.4Mg-0.4Mn-0.2Sc-0.09Zr alloy subjected to cold rolling with a total strain up to ~1.6 was studied using high resolution EBSD analysis and TEM. It was shown that cold rolling induces elongation of initial grains and the formation of deformation bands along rolling direction in addition to dramatic increase in density of lattice dislocations. Two types of deformation bands evolve. Deformation bands initially bounded by low-angle boundaries (LABs) with misorientation higher than 2o and spacing ranging from 0.8 to 4 μm gradually transform to lamellas delimited by high-angle boundaries (HABs). Thin deformation bands delimited by LABs with misorientation of 2o or less evolve within these coarse bands. First type of deformation bands is subdivided due to mutual intersection with second order deformation bands or shear bands to elongated crystallite evolving to micron scale grains with strain. The thin deformation bands may be also subdivided to nanoscale crystallites. It was shown that the formation of well-defined deformation bands yield very high anisotropy in strength and ductility, while a strong increase in lattice dislocation density with strain diminishes this anisotropy.

Comparing fast inductive tempering and conventional tempering: Effects on microstructure and mechanical properties

2018 ◽  
Vol 115 (4) ◽  
pp. 407 ◽  
Author(s):  
Annika Eggbauer Vieweg ◽  
Gerald Ressel ◽  
Peter Raninger ◽  
Petri Prevedel ◽  
Stefan Marsoner ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Impact Energy ◽  
Charpy Impact ◽  
Heat Treating ◽  
Processing Route ◽  
High Heating Rate ◽  
Heating Rates ◽  
High Heating ◽  
Tempering Treatment ◽  
Carbide Distribution

Induction heating processes are of rising interest within the heat treating industry. Using inductive tempering, a lot of production time can be saved compared to a conventional tempering treatment. However, it is not completely understood how fast inductive processes influence the quenched and tempered microstructure and the corresponding mechanical properties. The aim of this work is to highlight differences between inductive and conventional tempering processes and to suggest a possible processing route which results in optimized microstructures, as well as desirable mechanical properties. Therefore, the present work evaluates the influencing factors of high heating rates to tempering temperatures on the microstructure as well as hardness and Charpy impact energy. To this end, after quenching a 50CrMo4 steel three different induction tempering processes are carried out and the resulting properties are subsequently compared to a conventional tempering process. The results indicate that notch impact energy raises with increasing heating rates to tempering when realizing the same hardness of the samples. The positive effect of high heating rate on toughness is traced back to smaller carbide sizes, as well as smaller carbide spacing and more uniform carbide distribution over the sample.

scholarly journals Novel Co-Cu-Based Immiscible Medium-Entropy Alloys with Promising Mechanical Properties

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 238
Author(s):  
Sujung Son ◽  
Jongun Moon ◽  
Hyeonseok Kwon ◽  
Peyman Asghari Rad ◽  
Hidemi Kato ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Binary System ◽  
Design Methodology ◽  
Miscibility Gap ◽  
Face Centered Cubic ◽  
Solid Solution Strengthening ◽  
Solution Strengthening ◽  
Face Centered ◽  
Strength And Ductility ◽  
Cobalt Copper

New AlxCo50−xCu50−xMnx (x = 2.5, 10, and 15 atomic %, at%) immiscible medium-entropy alloys (IMMEAs) were designed based on the cobalt-copper binary system. Aluminum, a strong B2 phase former, was added to enhance yield strength and ultimate tensile strength, while manganese was added for additional solid solution strengthening. In this work, the microstructural evolution and mechanical properties of the designed Al-Co-Cu-Mn system are examined. The alloys exhibit phase separation into dual face-centered cubic (FCC) phases due to the miscibility gap of the cobalt-copper binary system with the formation of CoAl-rich B2 phases. The hard B2 phases significantly contribute to the strength of the alloys, whereas the dual FCC phases contribute to elongation mitigating brittle fracture. Consequently, analysis of the Al-Co-Cu-Mn B2-strengthened IMMEAs suggest that the new alloy design methodology results in a good combination of strength and ductility.

scholarly journals Evolution of the viscoelastic properties of painting stratigraphies: a moisture weathering and nanoindentation approach

2021 ◽  
Vol 9 (1) ◽  
Author(s):  
Mathilde Tiennot ◽  
Davide Iannuzzi ◽  
Erma Hermens
Keyword(s):  
Mechanical Properties ◽  
Relative Humidity ◽  
Cultural Heritage ◽  
Mechanical Behaviour ◽  
Viscoelastic Properties ◽  
Viscoelastic Behaviour ◽  
Storage And Loss Moduli ◽  
Heritage Studies ◽  
Paint Films ◽  
The Impact

AbstractIn this investigation on the mechanical behaviour of paint films, we use a new ferrule-top nanoindentation protocol developed for cultural heritage studies to examine the impact of repeated relative humidity variations on the viscoelastic behaviour of paint films and their mechanical properties in different paint stratigraphies through the changes in their storage and loss moduli. We show that the moisture weathering impact on the micromechanics varies for each of these pigment-oil systems. Data from the nanoindentation protocol provide new insights into the evolution of the viscoelastic properties dsue to the impact of moisture weathering on paint films.

scholarly journals Directionally-Dependent Mechanical Properties of Ti6Al4V Manufactured by Electron Beam Melting (EBM) and Selective Laser Melting (SLM)

Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3603
Author(s):  
Tim Pasang ◽  
Benny Tavlovich ◽  
Omry Yannay ◽  
Ben Jakson ◽  
Mike Fry ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Surface Roughness ◽  
Tensile Strength ◽  
Electron Beam ◽  
Additive Manufacturing ◽  
Selective Laser Melting ◽  
Electron Beam Melting ◽  
Rolling Direction ◽  
Laser Melting ◽  
Plate Rolling

An investigation of mechanical properties of Ti6Al4V produced by additive manufacturing (AM) in the as-printed condition have been conducted and compared with wrought alloys. The AM samples were built by Selective Laser Melting (SLM) and Electron Beam Melting (EBM) in 0°, 45° and 90°—relative to horizontal direction. Similarly, the wrought samples were also cut and tested in the same directions relative to the plate rolling direction. The microstructures of the samples were significantly different on all samples. α′ martensite was observed on the SLM, acicular α on EBM and combination of both on the wrought alloy. EBM samples had higher surface roughness (Ra) compared with both SLM and wrought alloy. SLM samples were comparatively harder than wrought alloy and EBM. Tensile strength of the wrought alloy was higher in all directions except for 45°, where SLM samples showed higher strength than both EBM and wrought alloy on that direction. The ductility of the wrought alloy was consistently higher than both SLM and EBM indicated by clear necking feature on the wrought alloy samples. Dimples were observed on all fracture surfaces.

Effect of Small Iron, Chromium and Boron Additions as Alloying Elements on Microstructure and Mechanical Properties of Ni3Al

2007 ◽  
Vol 23 ◽  
pp. 123-126
Author(s):  
Radu L. Orban ◽  
Mariana Lucaci
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Room Temperature ◽  
Alloying Elements ◽  
Alloyed Powder ◽  
Mechanically Alloyed ◽  
Powder Mixtures ◽  
B Additions ◽  
Strength And Ductility ◽  
Iron Chromium

This paper investigates the effect of Fe, Cr and B additions, in small proportions, as alloying elements in Ni3Al with the purpose to reduce its intrinsic fragility and extrinsic embrittlement and to enhance, in the same time, its mechanical properties. It represents a development of some previous research works of the authors, proving that Ni3Al-Fe-Cr-B alloys obtained by reactive synthesis (SHS) starting from Mechanically Alloyed powder mixtures have superior both room temperature tensile strength and ductility, and compression ones at temperatures up to 800 °C, than pure Ni3Al. These create premises for their using as superalloys substitutes.

Effect of Minor Additives on First Stage Graphitisation in White Cast Iron

1984 ◽  
Vol 34 ◽  
Author(s):  
P. L. Roy ◽  
A. K. Chakrabart ◽  
P. Banerjee
Keyword(s):  
Mechanical Properties ◽  
Cast Iron ◽  
Sodium Chloride ◽  
Yield Strength ◽  
White Cast Iron ◽  
Elemental Sulphur ◽  
Optimum Dose ◽  
White Iron ◽  
Kinetics Of ◽  
Strength And Ductility

ABSTRACTMinor additions (0.05-0.2 wt.%) of sodium chloride, hexachloroethane and elemental sulphur to commercial white iron melts have been found to enhance the kinetics of first stage graphitisation during subsequent annealing of white iron samples. The optimum dose of sodium chloride and hexachloroethane addition is around 0.1%. Yield strength and ductility of annealed test bars treated with NaCl or C2Cl6 compare favourably with those of untreated test bars. Sulphur treatment causes slight deterioration in mechanical properties. Fully grown nodules in both treated and untreated samples appear porous under SEM. Possible mechanisms of acceleration of graphitisation in the treated samples have been suggested.

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