scholarly journals Development of Nanobainitic Microstructures in Carbo-Austempered Cast Steels: Heat Treatment, Microstructure and Properties

Metals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 635
Author(s):  
Oscar Ríos-Diez ◽  
Ricardo Aristizábal-Sierra ◽  
Claudia Serna-Giraldo ◽  
Jose A. Jimenez ◽  
Carlos Garcia-Mateo

Carburizing implies the existence of a carbon gradient from the surface to the core of the steel, which in turn will affect both the critical temperature for austenite formation and the kinetics of the bainitic transformation during the austempering treatment. Therefore, for future development of carbo-austempered steels with nanobainitic microstructures in the case, it is key to understand the effect of such carbon gradient has on the final microstructure and the mechanical properties reached by the heat treatments used. This work was divided into two parts, firstly two alloys with similar carbon content to those at the surface and center of the carburized steel were used to establish the optimal heat treatment parameters and to study bainite transformation kinetics by high resolution dilatometry. In a second step, a carburized alloy is produced and subjected to the designed heat treatments, in order to evaluate the microstructure and mechanical properties developed. Results thus obtained are compared with those obtained in the same carburized alloy after following the most common quench and temper treatment.

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 48
Author(s):  
Wenjun Song ◽  
Min Lei ◽  
Mingpan Wan ◽  
Chaowen Huang

In this study, the phase transformation behaviour of the carburised layer and the matrix of 23CrNi3Mo steel was comparatively investigated by constructing continuous cooling transformation (CCT) diagram, determining the volume fraction of retained austenite (RA) and plotting dilatometric curves. The results indicated that Austenite formation start temperature (Ac1) and Austenite formation finish temperature (Ac3) of the carburised layer decreased compared to the matrix, and the critical cooling rate (0.05 °C/s) of martensite transformation is significantly lower than that (0.8 °C/s) of the matrix. The main products of phase transformation in both the carburised layer and the matrix were martensite and bainite microstructures. Moreover, an increase in carbon content resulted in the formation of lamellar martensite in the carburised layer, whereas the martensite in the matrix was still lath. Furthermore, the volume fraction of RA in the carburised layer was higher than that in the matrix. Moreover, the bainite transformation kinetics of the 23CrNi3Mo steel matrix during the continuous cooling process indicated that the mian mechanism of bainite transformation of the 23CrNi3Mo steel matrix is two-dimensional growth and one-dimensional growth.


2018 ◽  
Vol 284 ◽  
pp. 615-620 ◽  
Author(s):  
R.M. Baitimerov ◽  
P.A. Lykov ◽  
L.V. Radionova

TiAl6V4 titanium base alloy is widely used in aerospace and medical industries. Specimens for tensile tests from TiAl6V4 with porosity less than 0.5% was fabricated by selective laser melting (SLM). Specimens were treated using two heat treatment procedures, third batch of specimens was tested in as-fabricated statement after machining. Tensile tests were carried out at room temperature. Microstructure and mechanical properties of SLM fabricated TiAl6V4 after different heat treatments were investigated.


2021 ◽  
Author(s):  
Giuseppe Del Guercio ◽  
Manuela Galati ◽  
Abdollah Saboori

Abstract Additive Manufacturing processes are considered advanced manufacturing methods. It would be possible to produce complex shape components from a Computer-Aided Design model in a layer-by-layer manner. Lattice structures as one of the complex geometries could attract lots of attention for both medical and industrial applications. In these structures, besides cell size and cell type, the microstructure of lattice structures can play a key role in these structures' mechanical performance. On the other hand, heat treatment has a significant influence on the mechanical properties of the material. Therefore, in this work, the effect of the heat treatments on the microstructure and mechanical behaviour of Ti-6Al-4V lattice structures manufactured by EBM was analyzed. The main mechanical properties were compared with the Ashby and Gibson model. It is very interesting to notice that a more homogeneous failure mode was found for the heat-treated samples. The structures' relative density was the main factor influencing their mechanical performance of the heat-treated samples. It is also found that the heat treatments were able to preserve the stiffness and the compressive strength of the lattice structures. Besides, an increment of both the elongation at failure and the absorbed energy was obtained after the heat treatments. Microstructure analysis of the heat-treated samples confirms the increment of ductility of the heat-treated samples with respect to the as-built one.


Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1165 ◽  
Author(s):  
Hannes Fröck ◽  
Lukas Vincent Kappis ◽  
Michael Reich ◽  
Olaf Kessler

Age hardening aluminium alloys obtain their strength by forming precipitates. This precipitation-hardened state is often the initial condition for short-term heat treatments, like welding processes or local laser heat treatment to produce tailored heat-treated profiles (THTP). During these heat treatments, the strength-increasing precipitates are dissolved depending on the maximum temperature and the material is softened in these areas. Depending on the temperature path, the mechanical properties differ between heating and cooling at the same temperature. To model this behavior, a phenomenological material model was developed based on the dissolution characteristics and experimental flow curves were developed depending on the current temperature and the maximum temperature. The dissolution characteristics were analyzed by calorimetry. The mechanical properties at different temperatures and peak temperatures were recorded by thermomechanical analysis. The usual phase transformation equations in the Finite Element Method (FEM) code, which were developed for phase transformation in steels, were used to develop a phenomenological model for the mechanical properties as a function of the relevant heat treatment parameters. This material model was implemented for aluminium alloy 6060 T4 in the finite element software LS-DYNA (Livermore Software Technology Corporation).


2014 ◽  
Vol 783-786 ◽  
pp. 771-776 ◽  
Author(s):  
B. Hernández-Morale ◽  
O. Vázquez-Gómez ◽  
E. López-Martínez ◽  
H.J. Vergara-Hernández ◽  
L. Olmos

The first step in a heat treating cycle is the austenitizing of the as-received material. Despite its importance, this step has received relatively little attention. In this work, the kinetics of austenite formation during continuous heating tests of steel samples with low and high silicon content was determined as a function of heating rate. The microstructural evolution was characterized through dilatometric analysis of cylindrical samples (7 mm × 20 mm), continuously heated in a protective atmosphere at constant heating rates ranging from 2 to 40 °C/min. The critical temperatures and the transformation kinetics were determined from the derivative of the relative length change as a function of temperature. As the heating rate increases the critical temperatures and the transformation temperature range increase; the addition of silicon produces a more marked effect. The transformation kinetics data were correlated using an Avrami-type equation. The kinetic parameter n is nearly independent of heating rate while the parameter k is a strong function of the heating rate; in both cases, slightly larger values were obtained for the high-silicon steel.


2014 ◽  
Vol 59 (4) ◽  
pp. 1637-1640 ◽  
Author(s):  
J. Dworecka ◽  
E. Jezierska ◽  
K. Rozniatowski ◽  
W. Swiatnicki

Abstract The aim of the work was to produce a nanobainitic structure in the commercial bearing steel - 100CrMnSi6-4 and to characterize its structure and mechanical properties. In order to produce this structure the austempering heat treatment was performed, with parameters that have been selected on the basis of dilatometric measurements of phase transformation kinetics in steel. The heat treatment process was performed in laboratory as well as in industrial furnaces. The obtained structure was characterized using transmission electron microscopy. In order to investigate the effect of the microstructure parameters on the material’s mechanical properties, the hardness, impact strength and static tensile tests have been conducted.


2013 ◽  
Vol 834-836 ◽  
pp. 816-819 ◽  
Author(s):  
Li Jun Tan ◽  
Jun Qiao Wang ◽  
Qing Qun Wang ◽  
Xin Long Chen ◽  
Si Zhu Zhou

The tensile and impact properties of SAE4320 and SAE8620 alloys were investigated. Various heat treatments were applied to these two alloys, including different pre-heat treatment. The results shown that after Carburizing and Quenching, both SAE4320 and SAE8620 alloys were highly sensitively to V-notches for their impact samples. In any case, SAE4320 alloy revealed higher tensile strength, better impact toughness and deformation property. Previous work shown that after Carburizing and Quenching, the impact toughness of SAE8620 alloy was too low, the products made of it was very dangerous. Based on the results, a new advanced product was made of SAE4320 alloy instead of SAE8620 alloy. And the new product exhibited good properties. The impact value of the new product far exceeded the older products.


2021 ◽  
Vol 11 (22) ◽  
pp. 10598
Author(s):  
Giulia Stornelli ◽  
Andrea Di Schino ◽  
Silvia Mancini ◽  
Roberto Montanari ◽  
Claudio Testani ◽  
...  

EUROFER97 steel plates for nuclear fusion applications are usually manufactured by hot rolling and subsequent heat treatments: (1) austenitization at 980 °C for 30 min, (2) rapid cooling and (3) tempering at 760 °C for 90 min. An extended experimental campaign was carried out with the scope of improving the strength of the steel without a loss of ductility. Forty groups of samples were prepared by combining cold rolling with five cold reduction ratios (20, 40, 50, 60 and 80%) and heat treatments at eight different temperatures in the range 400–750 °C (steps of 50 °C). This work reports preliminary results regarding the microstructure and mechanical properties of all the cold-rolled samples and the effects of heat treatments on the samples deformed with the greater CR ratio (80%). The strength of deformed samples decreased as heat treatment temperature increased and the change was more pronounced in the samples cold-rolled with greater CR ratios. After heat treatments at temperature up to 600 °C yield stress (YS) and ultimate tensile strength (UTS) of samples deformed with CR ratio of 80% were significantly larger than those of standard EUROFER97 but ductility was lower. On the contrary, the treatment at 650 °C produced a fully recrystallized structure with sub-micrometric grains which guarantees higher strength and comparable ductility. The work demonstrated that EUROFER97 steel can be strengthened without compromising its ductility; the most effective process parameters will be identified by completing the analyses on all the prepared samples.


Metals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 612 ◽  
Author(s):  
Andrés Felipe Santacruz-Londoño ◽  
Oscar Rios-Diez ◽  
José A. Jiménez ◽  
Carlos Garcia-Mateo ◽  
Ricardo Aristizábal-Sierra

Nanoscale bainite is a remarkable microstructure that exhibits a very promising combination of high strength with good ductility and toughness. The development of these types of microstructures has been focused on wrought materials, and very little information is available for steel castings. In this work, a specially designed cast steel with 0.76 wt % C was fabricated, and the heat treatment cycles to develop bainitic nanostructures were determined by studying the kinetics of the bainitic transformation using high-resolution dilatometry. The effects of isothermal holding temperature and time on the final microstructure and mechanical properties were thoroughly characterized in order to evaluate a future industrial implementation of the process in an effort to contribute to enhance and widen the potential applications for cast steels.


2011 ◽  
Vol 690 ◽  
pp. 315-318 ◽  
Author(s):  
Jian Zheng Guo ◽  
Wei Sheng Cao ◽  
Claude Alain Rolle

A comprehensive numerical model has been developed for the calculation of the final microstructure and mechanical properties of aluminium casting alloys after heat treatment. The calculation is chained in such a way that the resultant microstructure of the previous processing step, such as casting, is used as the initial condition of the following step. In this paper an A357 alloy is chosen to study the microstructure and the evolution of the mechanical properties through the process from casting to heat treatment. The microstructure and mechanical properties are predicted and compared with experimental measurements.


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