scholarly journals Room Temperature Co-Precipitation Synthesis of Magnetite Nanoparticles in a Large pH Window with Different Bases

Materials ◽  
2013 ◽  
Vol 6 (12) ◽  
pp. 5549-5567 ◽  
Author(s):  
Maria Mascolo ◽  
Yongbing Pei ◽  
Terry Ring
2014 ◽  
Vol 40 (1) ◽  
pp. 1519-1524 ◽  
Author(s):  
Lazhen Shen ◽  
Yongsheng Qiao ◽  
Yong Guo ◽  
Shuangming Meng ◽  
Guochen Yang ◽  
...  

2020 ◽  
Vol 1 (1) ◽  
pp. 10-13
Author(s):  
Cathrin Kronenbitter ◽  
Hironobu Watanabe ◽  
Sadahito Aoshima ◽  
Helmut Cölfen

In this study we describe the green synthesis of temperature-switchable polymer-magnetite nanoparticles (PMNPs) in water at room temperature via an improved co-precipitation pathway for reversible switchable superstructures.


2019 ◽  
Vol 779 ◽  
pp. 698-705 ◽  
Author(s):  
Laura Bissoli de Mello ◽  
Laudemir Carlos Varanda ◽  
Fernando Aparecido Sigoli ◽  
Italo Odone Mazali

2011 ◽  
Vol 324 ◽  
pp. 129-132 ◽  
Author(s):  
Wegdan Ramadan ◽  
Marwa Kareem ◽  
Béatrice Hannoyer ◽  
Shanta Saha

Magnetite, Fe3O4, nanoparticles were synthesized using co-precipitation aqueous method at room temperature and at different pH, from 8 to 12.5. The pH value was found to influence greatly the resulting phases and has no significant effect on the particle size. In all cases, magnetite was found to be the main phase but the contribution of Goethite phase was identified clearly with the increase in pH. Significant reduction in saturation magnetization was evident. Structural and magnetic properties of the nanoparticles were examined using; XRD, TEM, Raman Spectroscopy and SQUID.


Nanomaterials ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 715
Author(s):  
Radenka Krsmanović Whiffen ◽  
Amelia Montone ◽  
Loris Pietrelli ◽  
Luciano Pilloni

Pyroelectric materials can harvest energy from naturally occurring ambient temperature changes, as well as from artificial temperature changes, notably from industrial activity. Wurtzite- based materials have the advantage of being cheap, non-toxic, and offering excellent opto-electrical properties. Due to their non-centrosymmetric nature, all wurtzite crystals have both piezoelectric and pyroelectric properties. Nanocrystalline wurtzite ZnS, being a room temperature stable material, by contrast to its bulk counterpart, is interesting due to its still not well-explored potential in piezoelectric and pyroelectric energy harvesting. An easy synthesis method—a co-precipitation technique—was selected and successfully tailored for nanocrystalline wurtzite ZnS production. ZnS nanopowder with nanoparticles of 3 to 5 nm in size was synthesized in ethyl glycol under medium temperature conditions using ZnCl2 and thiourea as the sources of Zn and S, respectively. The purified and dried ZnS nanopowder was characterized by conventional methods (XRD, SEM, TEM, TG and FTIR). Finally, a constructed in-house pilot plant that is able to produce substantial amounts of wurtzite ZnS nanopowder in an environmentally friendly and cost-effective way is introduced and described.


2009 ◽  
Vol 470 (1-2) ◽  
pp. 497-501 ◽  
Author(s):  
Y.J. Wu ◽  
H.P. Fu ◽  
R.Y. Hong ◽  
Y. Zheng ◽  
D.G. Wei

2020 ◽  
Vol 27 (3) ◽  
pp. 919-927 ◽  
Author(s):  
Eldar T. Talgatov ◽  
Assemgul S. Auyezkhanova ◽  
Kuralai S. Seitkalieva ◽  
Nurmukhamet Zh. Tumabayev ◽  
Sandugash N. Akhmetova ◽  
...  

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