scholarly journals Fractional Factorial Design Study on the Performance of GAC-Enhanced Electrocoagulation Process Involved in Color Removal from Dye Solutions

Materials ◽  
2013 ◽  
Vol 6 (7) ◽  
pp. 2723-2746 ◽  
Author(s):  
Marius Secula ◽  
Igor Cretescu ◽  
Benoit Cagnon ◽  
Liliana Manea ◽  
Corneliu Stan ◽  
...  
Keyword(s):  
Factorial Design ◽  
Fractional Factorial Design ◽  
Fractional Factorial ◽  
Color Removal ◽  
Design Study ◽  
Electrocoagulation Process ◽  
Dye Solutions

scholarly journals Fractional Factorial Design Study for the Extraction of Cannabinoids from CBD-Dominant Cannabis Flowers by Supercritical Carbon Dioxide

Processes ◽  
2022 ◽  
Vol 10 (1) ◽  
pp. 93
Author(s):  
Sadia Qamar ◽  
Yady J. M. Torres ◽  
Harendra S. Parekh ◽  
James Robert Falconer
Keyword(s):  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Organic Solvent ◽  
Factorial Design ◽  
Fractional Factorial Design ◽  
Fractional Factorial ◽  
Extraction Time ◽  
High Yield ◽  
Design Study ◽  
Supercritical Carbon

The optimization of the supercritical fluid extraction (SFE) of cannabinoids, using supercritical carbon dioxide (scCO2), was investigated in a fractional factorial design study. It is hypothesized that four main parameters (temperature, pressure, dry flower weight, and extraction time) play an important role. Therefore, these parameters were screened at predetermined low, medium, and high relative levels. The density of scCO2 was used as a factor for the extraction of cannabinoids by changing the pressure and temperature. The robustness of the mathematical model was also evaluated by regression analysis. The quantification of major (cannabidiol (CBD), cannabidiolic acid (CBDA), delta 9-tetrahydrocannabinol (Δ9-THC), delta 8-tetrahydrocannabinol (Δ8-THC), and delta 9-tetrahydrocannabinol acid (THCA-A)) and minor (cannabidivann (CBDV), tetrahydrocannabivann (THCV), cannabigerolic acid (CBG), cannabigerol (CBGA), cannabinol (CBN), and cannabichomere (CBC)) cannabinoids in the scCO2 extract was performed by RP-HPLC analysis. From the model response, it was identified that long extraction time is a significant parameter to obtain a high yield of cannabinoids in the scCO2 extract. Higher relative concentrations of CBD(A) (0.78 and 2.41% w/w, respectively) and THC(A) (0.084 and 0.048% w/w, respectively) were found when extraction was performed at high relative pressures and temperatures (250 bar and 45 °C). The higher yield of CBD(A) compared to THC(A) can be attributed to the extract being a CBD-dominant cannabis strain. The study revealed that conventional organic solvent extraction, e.g., ethanol gives a marginally higher yield of cannabinoids from the extract compared to scCO2 extraction. However, scCO2 extraction generates a cleaner (chlorophyll-free) and organic solvent-free extract, which requires less downstream processing, such as purification from waxes and chlorophyll.

Optimization of PES Nanocomposite Membrane Preparation Using Statistical Analysis and Experimental Design

2019 ◽  
Author(s):  
Yasin Orooji ◽  
Fatemeh Noorisafa ◽  
Nahid Imami ◽  
Amir R. Chaharmahali
Keyword(s):  
Statistical Analysis ◽  
Experimental Design ◽  
Factorial Design ◽  
Fractional Factorial Design ◽  
Fractional Factorial ◽  
Nanocomposite Membrane ◽  
Membrane Preparation ◽  
Membrane Fabrication

<p>Using experimental design and statistical analysis (½ Fractional Factorial Design), this study investigates the effect of different parameters in the membrane fabrication on the performance of nanocomposite PES/TiO<sub>2</sub> membrane. </p>

scholarly journals Fabrication of a Silicide Thermoelectric Module Employing Fractional Factorial Design Principles

2021 ◽  
Author(s):  
Joachim S. Graff ◽  
Raphael Schuler ◽  
Xin Song ◽  
Gustavo Castillo-Hernandez ◽  
Gunstein Skomedal ◽  
...  
Keyword(s):  
Factorial Design ◽  
Fractional Factorial Design ◽  
Waste Heat ◽  
Thermoelectric Module ◽  
Fractional Factorial ◽  
Taguchi Methods ◽  
Dimensional Parameter ◽  
Cu Metallization ◽  
Manganese Silicide ◽  
And Performance

AbstractThermoelectric modules can be used in waste heat harvesting, sensing, and cooling applications. Here, we report on the fabrication and performance of a four-leg module based on abundant silicide materials. While previously optimized Mg2Si0.3Sn0.675Bi0.025 is used as the n-type leg, we employ a fractional factorial design based on the Taguchi methods mapping out a four-dimensional parameter space among Mnx-εMoεSi1.75−δGeδ higher manganese silicide compositions for the p-type material. The module is assembled using a scalable fabrication process, using a Cu metallization layer and a Pb-based soldering paste. The maximum power output density of 53 μW cm–2 is achieved at a hot-side temperature of 250 °C and a temperature difference of 100 °C. This low thermoelectric output is related to the high contact resistance between the thermoelectric materials and the metallic contacts, underlining the importance of improved metallization schemes for thermoelectric module assembly.

scholarly journals Producing Magnetic Nanocomposites from Paper Sludge for the Adsorptive Removal of Pharmaceuticals from Water—A Fractional Factorial Design

Nanomaterials ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 287
Author(s):  
Luciana S. Rocha ◽  
Érika M. L. Sousa ◽  
María V. Gil ◽  
João A. B. P. Oliveira ◽  
Marta Otero ◽  
...  
Keyword(s):  
Activated Carbon ◽  
Factorial Design ◽  
Fractional Factorial Design ◽  
Metal Oxide Nanoparticles ◽  
Aqueous Media ◽  
Fractional Factorial ◽  
Paper Sludge ◽  
Synthesis Conditions ◽  
Adsorptive Removal ◽  
Iron Salts

In view of a simple after-use separation, the potentiality of producing magnetic activated carbon (MAC) by intercalation of ferromagnetic metal oxide nanoparticles in the framework of a powder activated carbon (PAC) produced from primary paper sludge was explored in this work. The synthesis conditions to produce cost effective and efficient MACs for the adsorptive removal of pharmaceuticals (amoxicillin, carbamazepine, and diclofenac) from aqueous media were evaluated. For this purpose, a fractional factorial design (FFD) was applied to assess the effect of the most significant variables (Fe3+ to Fe2+ salts ratio, PAC to iron salts ratio, temperature, and pH), on the following responses concerning the resulting MACs: Specific surface area (SBET), saturation magnetization (Ms), and adsorption percentage of amoxicillin, carbamazepine, and diclofenac. The statistical analysis revealed that the PAC to iron salts mass ratio was the main factor affecting the considered responses. A quadratic linear regression model A = f(SBET, Ms) was adjusted to the FFD data, allowing to differentiate four of the eighteen MACs produced. These MACs were distinguished by being easily recovered from aqueous phase using a permanent magnet (Ms of 22–27 emu g−1), and their high SBET (741–795 m2 g−1) were responsible for individual adsorption percentages ranging between 61% and 84% using small MAC doses (35 mg L−1).

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