scholarly journals Structural and Phase Transformations and Physical and Mechanical Properties of Cu-Al-Ni Shape Memory Alloys Subjected to Severe Plastic Deformation and Annealing

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4394
Author(s):  
Alexey E. Svirid ◽  
Vladimir G. Pushin ◽  
Natalia N. Kuranova ◽  
Vladimir V. Makarov ◽  
Yuri M. Ustyugov

Using the methods of electron microscopy and X-ray analysis in combination with measurements of the electrical resistance and magnetic susceptibility, the authors have obtained data on the peculiar features of pre-martensitic states and martensitic transformations, as well as subsequent decomposition, in the alloys with shape memory effect of Cu–14wt%Al–3wt%Ni and Cu–13.5wt%Al–3.5wt%Ni. For the first time, we established the microstructure, phase composition, mechanical properties, and microhardness of the alloys obtained in the nanocrystalline state as a result of severe plastic deformation under high pressure torsion and subsequent annealing. A crystallographic model of the martensite nucleation and the rearrangements β1→β1' and β1→γ1ꞌ are proposed based on the analysis of the observed tweed contrast and diffuse scattering in the austenite and the internal defects in the substructure of the martensite.

2013 ◽  
Vol 738-739 ◽  
pp. 491-495 ◽  
Author(s):  
Igor Litovchenko ◽  
Alexander Tyumentsev ◽  
Alexander V. Korznikov

The peculiarities of martensitic transformations and formation of nanostructured states in metastable austenitic steel (Fe-18Cr-8Ni-Ti) after severe plastic deformation by high pressure torsion are investigated. It is shown that during severe plastic deformation with increased strain rate not only direct (γ→α΄) but also reverse (α΄→γ) martensitic transformations occur, which is revealed by the changes in the volume content of α΄ - martensite during deformation. The fragments thought to be formed by direct and reverse martensitic transformations and those of dynamic recrystallization of austenite are observed.


2017 ◽  
Vol 743 ◽  
pp. 203-206 ◽  
Author(s):  
Alexander A. Kozulin ◽  
Vladimir A. Krasnoveikin ◽  
Vladimir A. Skripnyak ◽  
Evgeny N. Moskvichev ◽  
Valery E. Rubtsov

This study examines the effect of severe plastic deformation on the physical and mechanical properties of a light structural Al-Mg alloy. Severe plastic deformation has been performed by equal channel angular pressing through a die with an angle of 90° between the channels to produce ultrafine-grained structure in specimens of studied alloy. A complex investigation of the physical and mechanical properties of the processed alloy has been carried out to examine the microstructure and texture, and to measure microhardness, yield stress and ultimate tensile strength. The obtained results demonstrate high efficiency of the chosen treatment method and mode of producing a light ultrafine-grained alloy.


Author(s):  
Georgy I. Raab ◽  
Ilyas S. Kodirov ◽  
Gennady N. Aleshin ◽  
Arseniy G. Raab ◽  
Nikolai K. Tsenev

Problem Statement (Relevance): The paper describes some features and prospective benefits of deformation by methods of drawing with shear (SD) and high pressure torsion (HPT) in a temperature range of dynamic strain aging (DSA) effect, which allow receiving a high complex of physical and mechanical properties. Objectives: The study aims to investigate and analyze features of the structure formation with the combined application of severe plastic deformation (SPD) and the DSA effect during deformation by drawing with shear and high pressure torsion, to establish patterns of the gradient structure formation. Methods Applied: 1. Computer simulation in Deform 3D software to investigate the stress-strain state on materials with various types of a crystalline lattice: copper grade M1 (FCC), Steel 10 (BCC) and titanium VT1-0 (HCP) and a further comparison with experimental results. 2. Microhardness measurement 3. Scanning and transmission electron microscopy. Originality: This research resulted in investigation of the combined effect of the DSA effect and SPD on the gradient structure formation and mechanical properties of metals with various crystalline lattices. Findings: the paper presents the results of the study of the structure formation during non-monotonous plastic deformation of the alloys (steel 10, copper and titanium) with various crystalline lattice types by SD, as well as ECAP and HPT of low-carbon steel in the temperature range of the DSA effect. Deformation mechanisms and features of the deformation behavior on a mesoscopic scale under various deformation treatment modes are analyzed. The temperature range of the DSA effect in steel 10 under ECAP and the fact of the gradient structure formation under HPT are established. Practical Relevance: The study helped to obtain data that can be used to choose the optimal deformation treatment mode with the DSA effect.


Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1939 ◽  
Author(s):  
Gheorghe Gurau ◽  
Carmela Gurau ◽  
Felicia Tolea ◽  
Vedamanickam Sampath

Severe plastic deformation (SPD) is widely considered to be the most efficient process in obtaining ultrafine-grained bulk materials. The aim of this study is to examine the effects of the SPD process on Ni-Fe-Ga ferromagnetic shape memory alloys (FSMA). High-speed high-pressure torsion (HSHPT) was applied in the as-cast state. The exerted key parameters of deformation are described. Microstructural changes, including morphology that were the result of processing, were investigated by optical and scanning electron microscopy. Energy-dispersive X-ray spectroscopy was used to study the two-phase microstructure of the alloys. The influence of deformation on microstructural features, such as martensitic plates, intragranular γ phase precipitates, and grain boundaries’ dependence of the extent of deformation is disclosed by transmission electron microscopy. Moreover, the work brings to light the influence of deformation on the characteristics of martensitic transformation (MT). Vickers hardness measurements were carried out on disks obtained by SPD so as to correlate the hardness with the microstructure. The method represents a feasible alternative to obtain ultrafine-grained bulk Ni-Fe-Ga alloys.


2012 ◽  
Vol 715-716 ◽  
pp. 373-373
Author(s):  
Anahita Khorashadizadeh ◽  
Myrjam Winning ◽  
Stefan Zaefferer ◽  
Dierk Raabe

Investigations of the microstructure of materials processed via severe plastic deformation methods such as high pressure torsion (HPT) and their recrystallization behaviour is of great interest as they are capable of producing ultra fine grained material (UFD) with good mechanical properties.


2013 ◽  
Vol 738-739 ◽  
pp. 530-534 ◽  
Author(s):  
Natalia N. Kuranova ◽  
Vladimir V. Makarov ◽  
Vladimir G. Pushin ◽  
Alexey N. Uksusnikov

Results of investigations of structure and phase transformations and properties of the TiNi-based alloys with a shape memory effect (SME) after severe plastic deformation (SPD) by cold rolling, cold drawing, high pressure torsion and subsequent annealing are reported. It is found that the baroelastic effects related to the highly reversible martensitic transformations can occur in alloys, subjected to high pressure. The evolution of fine structure of the alloys into nanocrystalline and then amorphous state during SPD and after subsequent annealing have been studied. The effect of grain size on the martensitic transformations and properties of the alloys is discussed.


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