scholarly journals On Phase Identification of Hardened Cement Pastes by Combined Nanoindentation and Mercury Intrusion Method

Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3349
Author(s):  
Jingwei Ying ◽  
Xiangxin Zhang ◽  
Zhijun Jiang ◽  
Yijie Huang
Keyword(s):  
Mechanical Properties ◽  
Pore Structure ◽  
Cement Paste ◽  
Phase Distribution ◽  
Gaussian Mixture ◽  
Hardened Cement ◽  
Phase Identification ◽  
Hardened Cement Paste ◽  
Cement Pastes ◽  
Mercury Intrusion

The micro-mechanical properties of hardened cement paste can be obtained by nanoindentation. Phases at different locations can generally be determined by using the Gaussian mixture model (GMM) method and the K-means clustering (KM) method. However, there are differences between analysis methods. In this study, pore structure and porosity of hardened cement paste aged three, seven, and 28 days were obtained by mercury intrusion porosimetry (MIP), and their micro-mechanical properties were obtained by the nanoindentation method. A new method, GMM-MIP and KM-MIP, was proposed to determine the phase of hardened cement paste based on the pore structure and nanoindentation results. The results show that GMM-MIP and KM-MIP methods are more reasonable than GMM and KM methods in determining the phase of hardened cement paste. GMM-MIP can be used to obtain reasonable phase distribution. If the micro-mechanical properties of each phase in hardened cement paste do not satisfy the normal distribution, the GMM method has significant defects.

The Influence of Pore-Strucrure on the Campressive Strength of Hardened Cement Paste

1984 ◽  
Vol 42 ◽  
Author(s):  
Huang Yiun-Yuan ◽  
Ding Wei ◽  
Lu Ping
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Pore Structure ◽  
Cement Paste ◽  
Total Porosity ◽  
Hardened Cement ◽  
Hardened Cement Paste ◽  
New Information ◽  
The Relationship ◽  
Empirical Constants

AbstractThe pore-structure strongly influences the carpressive strength of hardened cement paste (hcp) and other porous materials, as well as other mechanical properties. The simplest but most currently used expression representing the relationship between the pore-structure and compressive strength is fram Balshin: σ = σ0 (l-P)A, in which only the total porosity P is involved as a single parameter and σ0 and A are empirical constants. The influence of pore size distribution and pore shapes etc. are not considered.The authors introduce second parameter w - the factor of relative specific surface area of the pores other than the total porosity P into consideration and a new expression is proposed:σc=K11-p/1+2p(K2(1-p))K3w+K4 all the constants K1 - K4 can be determined experimentally. By using of this expression the new information relating the influence of pore-structure on the caopressive strength of hcp can be predicted.

scholarly journals Hydration characteristics and structure formation of cement pastes containing metakaolin

2018 ◽  
Vol 149 ◽  
pp. 01013 ◽  
Author(s):  
Leonid Dvorkin ◽  
Nataliya Lushnikova ◽  
Oleksandr Bezusyak ◽  
Mohammed Sonebi ◽  
Jamal Khatib
Keyword(s):  
Pore Structure ◽  
Cement Paste ◽  
Average Diameter ◽  
Cementitious Materials ◽  
Mineral Admixture ◽  
Mineral Admixtures ◽  
Hardened Cement ◽  
Initial Structure ◽  
Hardened Cement Paste ◽  
Cement Pastes

Metakaolin (MK) is one of the most effective mineral admixtures for cement-based composites. The deposits of kaolin clays are wide-spread in the world. Metakaolin is comparable to silica fume as an active mineral admixture for cement-based composites. In this paper, the rheological and mechanical properties of cement paste containing metakaolin are investigated. The effect of MK is more evident at “tight” hydration conditions within mixtures with low water-cement ratio, provided by application of superplasticizers. The cement is replaced with 0 to 15% metakaolin, and superplasticizer content ranged from 0 to 1.5% by weight of cementitious materials (i.e. cement and metakaolin). An equation is derived to describe the relationship between the metakaolin and superplasticizer content and consistency of pastes. There is a linear dependence between metakalolin content and water demand. Second-degree polynomial describe the influence of superplasticizer content. The application of SP and MK may produce cement-water suspensions with water-retaining capacity at 50-70% higher than control suspensions. The investigation of initial structure forming of cement pastes with SP-MK composite admixture indicates the extension of coagulation structure forming phase comparing to the pastes without additives. Crystallization stage was characterized by more intensive strengthening of the paste with SP-MK admixture comparing to the paste without admixtures and paste with SP. Results on the porosity parameters for hardened cement paste indicate a decrease in the average diameter of pores and refinement of pore structure in the presence of metakaolin. A finer pore structure associated with an increase in strength. X-ray analysis data reveal a growing number of small-crystalline low-alkaline calcium hydrosilicates and reducing portlandite content, when MK dosage increases. Scanning electron microscopy (SEM) data confirm, that hardened cement paste containing MK has crystalline structure with dominance of partially crystalized hydrosilicates and gel-like formations.

scholarly journals Effect of Ground Slag on Mechanical Properties of Concrete under Low Temperature

2021 ◽  
Vol 2109 (1) ◽  
pp. 012019
Author(s):  
Xuelian Yuan ◽  
Jie Hu
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Compressive Strength ◽  
Low Temperature ◽  
Cement Paste ◽  
High Volume ◽  
Hardened Cement ◽  
Micro Structure ◽  
Hardened Cement Paste ◽  
Fracture Properties

Abstract Through using cube resisting compression test, fracture properties and micro-structure, the mechanical properties of high volume ground slag concrete under low temperature are studied in this paper. The results show that low temperature can improve the compressive strength of high volume ground slag concrete. And strength increased with the decreased of temperature. Low temperature can also improve the fracture energy and fracture toughness. Not only can ground slag reduce the content of calcium hydroxide in hardened cement paste, but ground slag can improve the compactness of hardened cement paste, reduce porosity and improve the strength of the interface.

Sensitivity of concrete properties to the pore structure of hardened cement paste

1996 ◽  
Vol 26 (11) ◽  
pp. 1619-1627 ◽  
Author(s):  
Osman N. Oktar ◽  
Harun Moral ◽  
Mehmet A. Taşdemir
Keyword(s):  
Pore Structure ◽  
Cement Paste ◽  
Hardened Cement ◽  
Hardened Cement Paste ◽  
Concrete Properties
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