scholarly journals The Effect of Annealing on Additive Manufactured ULTEM™ 9085 Mechanical Properties

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2907
Author(s):  
Yongjie Zhang ◽  
Seung Ki Moon

Fused filament fabrication (FFF) is increasingly adopted for direct manufacturing of end use parts in an aviation industry. However, the application of FFF technique is still restricted to manufacturing low criticality lightly loaded parts, due to poor mechanical performance. To alleviate the mechanical performance issue, thermal annealing process is frequently utilized. However, problems such as distortion issues and the need for jigs and fixtures limit the effectiveness of the thermal annealing process, especially for low volume complex FFF parts. In this research, a novel low temperature thermal annealing is proposed to address the limitations in conventional annealing. A modified orthogonal array design is applied to investigate the performance of ULTEM™ 9085 FFF coupons. Further, the coupons are annealed with specialized support structures, which are co-printed with the coupons during the manufacturing process. Once the annealing process is completed, multiscale characterizations are performed to identify the mechanical properties of the specimens. Geometrical measurement of post annealed specimens indicates an expansion in the layering direction, which indicates relief of thermal stresses. Moreover, annealed coupons show an improvement in tensile strength and reduction in strain concentration. Mesostructure and fracture surface analysis indicate an increase in ductility and enhanced coalescence. This research shows that the proposed annealing methodology can be applied to enhance the mechanical performance of FFF parts without significant distortion.

2014 ◽  
Vol 887-888 ◽  
pp. 240-247
Author(s):  
Xun Zeng Huang ◽  
Si Yue Chen ◽  
Xin Zhang ◽  
Yi Tao Yang

In this research, influence of annealing process on microstructure and mechanical performance of Nb-Ti-stabilized 430 ferritic stainless steel were investigated. In order to obtain the optimal annealing process, metallographic observation, SEM detection and tensile test were carried out. It is found that the microscopic structure is composed of fine and uniform isometric recrystallization grain after annealing. Optimum microstructure and mechanical properties can be achieved while annealed at 950 °Cfor 90 seconds. The annealed sample can obtain the optimum microstructure and mechanical properties under such annealing process. The yield platform is eliminated and the average plastic strain ratio is further improved to 1.269, which reflected a well deep drawability of the Nb-Ti-stabilized 430 ferritic stainless steel compared to SUS 430 stainless steel.


1996 ◽  
Vol 424 ◽  
Author(s):  
S. S. He ◽  
V. L. Shannon ◽  
T. Nguyen

AbstractPECVD silicon nitride was deposited by silane and deuterium ammonia. Silicon rich and nitrogen rich silicon nitride were deposited by varying the ratio of the SiH4/DH3. From FTIR, we found that the wave numbers of SiD and ND shifted lower when compared to SiH and NH bond in the NH3 nitride. In Si-rich nitride, both Si-H and Si-D bonds were found, which is different from N-rich nitride, where only an ND bond was found. Most of the hydrogen in NH(D) comes from the ammonia during PECVD deposition. We found that some of the deuterium exchanges its bonding to silicon from the initial bonding to nitrogen during a rapid thermal annealing process.


Author(s):  
G M Alonzo-Medina ◽  
A González-González ◽  
J L Sacedón ◽  
A I Oliva

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