scholarly journals In Situ Formation of ZrB2 and Its Influence on Wear and Mechanical Properties of ADC12 Alloy Mixed Matrix Composites

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2141
Author(s):  
Lalta Prasad ◽  
Niteesh Kumar ◽  
Anshul Yadav ◽  
Anil Kumar ◽  
Virendra Kumar ◽  
...  
Keyword(s):  
Xrd Analysis ◽  
Inorganic Salts ◽  
Dry Sliding ◽  
Matrix Composites ◽  
Mixed Matrix ◽  
Sem Images ◽  
Mechanical And Tribological Properties ◽  
In Situ Formation

In this work, aluminium alloy ADC12 reinforced with various amounts of ZrB2 (0 wt.%, 3 wt.%, 6 wt.%, 9 wt.%) were synthesized by an in-situ reaction of molten aluminium with inorganic salts K2ZrF6 & KBF4. XRD, EDAX, and SEM techniques are used for the characterization of the fabricated composite. XRD analysis revealed the successful in situ formation of ZrB2 in the composite. From the SEM images, it was concluded that the distribution of reinforcement was homogeneous in the composites. A study of mechanical and tribological properties under the dry sliding condition of ZrB2-reinforced ADC12 alloy has also been carried out. It is seen that there is an increase in tensile strength by 18.8%, hardness by 64.2%, and an increase in wear resistance of the material after reinforcement. The ductility of the material decreased considerably with an increase in the amount of reinforcement. The composite’s impact strength decreased by 27.7% because of the addition of hard ZrB2 particulates.

Synthesis and Characterization of In Situ AlN Reinforced Magnesium Matrix Composites

2012 ◽  
Vol 710 ◽  
pp. 377-382
Author(s):  
Sreeja Kumari Sukumaran Suseelammaa ◽  
Uma Thanu Subramonia Pillai ◽  
Sujayakumar Prasanth ◽  
Bellampettu Chandrasekhar Pai
Keyword(s):  
Grain Size ◽  
Xrd Analysis ◽  
Synthesis And Characterization ◽  
Matrix Composites ◽  
Nitrogen Gas ◽  
Magnesium Matrix ◽  
Magnesium Matrix Composites ◽  
Gas Bubbling

In situ Mg-AlN composite has been synthesized by nitrogen gas bubbling method. The morphology of the particles is found to be hexagonal by SEM. The size of the AlN particles is found to be in the range from nano, submicron to a few microns. XRD analysis of the samples confirms the formation of AlN in the melt. Further, the grain size of the magnesium matrix has been reduced by the presence of AlN particles. Hardness of the composite is significantly increased in the particle rich area due to the presence of hard AlN particles.

Effect of pouring temperature on A356-TiB2 MMCs cast in sand and permanent moulds by in-situ method

2016 ◽  
Vol 25 (5-6) ◽  
pp. 165-169
Author(s):  
C. Rajaravi ◽  
P.R. Lakshminarayanan
Keyword(s):  
Evaluation Studies ◽  
Physical And Mechanical Properties ◽  
Xrd Analysis ◽  
Matrix Composites ◽  
Structure Property ◽  
Pouring Temperature ◽  
Matrix Metal ◽  
Property Evaluation ◽  
The Matrix

AbstractThe paper describes a different condition of pouring temperature by sand and permanent mould to produce A356-6 wt% TiB2 metal matrix composites by in-situ method salt metal reaction route. The observation of SEM micrographs shows particle distribution of the TiB2 and it appears in hexagonal shape in Al matrix. The results of X-ray diffraction (XRD) analysis confirmed the formation of those TiB2 particulates and the results showed TiB2 particles are homogeneously dispersed throughout the matrix metal. Subsequent structure-property evaluation studies indicated sub-micron size reinforcement of in-situ formed TiB2 particles with improved physical and mechanical properties as compared to sand and permanent mould of Al-TiB2 composites. From, the permanent mould Al-TiB2 composite has an advantage of increase the properties over sand mould Al-TiB2 composite.

scholarly journals Sintering and Mechanical Properties of (SiC + TiCx)p/Fe Composites Synthesized from Ti3AlC2, SiC, and Fe Powders

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2453
Author(s):  
Mingtao Wang ◽  
Zecheng Wang ◽  
Zhiyue Yang ◽  
Jianfeng Jin ◽  
Guoping Ling ◽  
...  
Keyword(s):  
Ceramic Particle ◽  
Matrix Composites ◽  
Plastic Response ◽  
Excellent Performance ◽  
Iron Matrix ◽  
Particle Content ◽  
Reinforcing Effect ◽  
In Situ Formation ◽  
Hybrid Reinforcement

Ceramic-particle-reinforced iron matrix composites (CPR-IMCs) have been used in many fields due to their excellent performance. In this study, using the fast resistance-sintering technology developed by our team, iron matrix composites (IMCs) reinforced by both SiC and TiCx particles were fabricated via the addition of SiC and Ti3AlC2 particles, and the resulting relative densities of the sintering products were up to 98%. The XRD and EDS analyses confirmed the in situ formation of the TiCx from the decomposition of Ti3AlC2 during sintering. A significant hybrid reinforcing effect was discovered in the (SiC + TiCx)p/Fe composites, where the experimental strength and hardness of the (SiC + TiCx)p/Fe composites were higher than the composites of monolithic SiCp/Fe and (TiCx)p/Fe. While, under the condition of constant particle content, the elongation of the samples reinforced using TiCx was the best, those reinforced by SiC was the lowest, and those reinforced by (SiC + TiCx) fell in between, which means the plastic response of (SiC + TiCx)p/Fe composites obeyed the rule of mixture. The successful preparation of IMCs based on the hybrid reinforcement mechanism provides an idea for the optimization of IMCs.

Polysulfide Networks. In Situ Formation and Characterization of the Elastomeric Behavior

2007 ◽  
Vol 40 (14) ◽  
pp. 5141-5149 ◽  
Author(s):  
Giona Kilcher ◽  
Lei Wang ◽  
Craig Duckham ◽  
Nicola Tirelli
Keyword(s):  
In Situ Formation

scholarly journals CAAC Boranes. Synthesis and characterization of cyclic (alkyl) (amino) carbene borane complexes from BF3 and BH3

2010 ◽  
Vol 6 ◽  
pp. 709-712 ◽  
Author(s):  
Julien Monot ◽  
Louis Fensterbank ◽  
Max Malacria ◽  
Emmanuel Lacôte ◽  
Steven J Geib ◽  
...  
Keyword(s):  
Silica Gel ◽  
Synthesis And Characterization ◽  
Gel Chromatography ◽  
Nmr Analysis ◽  
X Ray ◽  
X Ray Crystallography ◽  
In Situ Formation ◽  
Silica Gel Chromatography

In situ formation of two cyclic (alkyl) (amino) carbenes (CAACs) followed by addition of BF3•Et2O provided the first two examples of CAAC–BF3 complexes: 1-(2,6-diisopropylphenyl)-3,5,5-trimethyl-3-phenylpyrrolidin-2-ylidene trifluoroborane, and 2-(2,6-diisopropylphenyl)-3,3-dimethyl-2-azaspiro[4.5]decan-1-ylidene trifluoroborane. These CAAC–BF3 complexes are robust compounds that are stable to ambient laboratory conditions and silica gel chromatography. They were characterized by spectroscopy and X-ray crystallography. In contrast, a CAAC complex with borane (BH3) was readily formed in situ according to 1H and 11B NMR analysis, but did not survive the workup conditions. These results set the stage for further studies of the chemistry of CAAC boranes.

Characterization of the Aniline.DBSA/Thermoplastic Polyurethane Blends for the Thermo-Mechanical and Electro-Mechanical Properties

2021 ◽  
Vol 875 ◽  
pp. 96-103
Author(s):  
Ayesha Afzal ◽  
Iqra Abdul Rashid ◽  
H.M. Faizan Shakir ◽  
Asra Tariq
Keyword(s):  
Mechanical Properties ◽  
Thermoplastic Polyurethane ◽  
Strain Sensors ◽  
Sem Images ◽  
Dynamic Mechanical Thermal Analyzer ◽  
Thermal Analyzer ◽  
Uniform Dispersion ◽  
Polymerization Method

Conducting polymer blends Polyaniline-Dodecylbenzene sulfonic acid (Pani.DBSA) and thermoplastic polyurethane (TPU) were prepared using in-situ emulsion polymerization method by dissolving both components in DMF. Ani.DBSA/TPU blends were prepared with different compositions 20/80, 30/70, 40/60 and 50/50 wt%. Theses blends have good conducting and mechanical properties. Blends were characterized by Potentiostate, Thermogravimetric analysis (TGA), Infrared spectroscopy (FTIR) and Dynamic mechanical thermal analyzer (DMTA). The electrical conductivity increases up to 30 wt% loading of aniline.DBSA after that it decreases gradually. The uniform dispersion of aniline.DBSA showed in SEM images which is the indication of a strong connection between aniline.DBSA and TPU which increase the conductivity. These blends can be used as strain sensors.

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