scholarly journals Evaluation of Inconel 718 Metallic Powder to Optimize the Reuse of Powder and to Improve the Performance and Sustainability of the Laser Powder Bed Fusion (LPBF) Process

Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1538
Author(s):  
Konrad Gruber ◽  
Irina Smolina ◽  
Marcin Kasprowicz ◽  
Tomasz Kurzynowski

In this paper, a detailed assessment of Inconel 718 powder, with varying degrees of degradation due to repeated use in the Laser Powder Bed Fusion (LPBF) process, has been undertaken. Four states of IN718 powder (virgin, used, overflow and spatter) were characterized in terms of their morphology, flowability and physico-chemical properties. Studies showed that used and overflow powders were almost identical. The fine particle-size distribution of the virgin powder, in which 50% of particles were found to be below the nominal particle-size distribution (PSD), was recognized as the main reason for its lower flowability and the main cause of the differentiation between virgin, used and overflow powders. Only spatter powder was found to be degraded enough to preclude its direct LPBF reuse. The oxygen content in the spatter powder exceeded the limit value for IN718 by 290 ppm, and aluminum oxide spots were found on the spatter particles surfaces. Laser absorption analysis showed 10 pp higher laser absorption compared to the other powders. The results of evaluation showed that IN718 powder is resistant to multiple uses in the LPBF process. Due to the low degradation rate of IN718 powder, overflow powder can be re-enabled for multiple uses with a proper recycling strategy.

Author(s):  
Massimiliano Bonesso ◽  
Pietro Rebesan ◽  
Claudio Gennari ◽  
Simone Mancin ◽  
Razvan Dima ◽  
...  

AbstractOne of the major benefits of the Laser Powder Bed Fusion (LPBF) technology is the possibility of fabrication of complex geometries and features in only one-step of production. In the case of heat exchangers in particular, this is very convenient for the fabrication of conformal cooling channels which can improve the performance of the heat transfer capability. Yet, obtaining dense copper parts printed via LPBF presents two major problems: the high reflectivity of 1 μm (the wavelength of commonly used laser sources) and the high thermal conductivity of copper that limits the maximum local temperature that can be attained. This leads to the formation of porous parts.In this contribution, the influence of the particle size distribution of the powder on the physical and mechanical properties of parts produced via LPBF is studied. Three copper powders lots with different particle size distributions are used in this study. The effect on densification from two laser scan parameters (scan speed and hatching distance) and the influence of contours scans on the lateral surface roughness is reported. Subsequently, samples manufactured with the optimal process parameters are tested for thermal and mechanical properties evaluation.


Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1763
Author(s):  
Nthateng Nkhasi ◽  
Willie du Preez ◽  
Hertzog Bissett

Metal powders suitable for use in powder bed additive manufacturing processes should ideally be spherical, dense, chemically pure and of a specified particle size distribution. Ti6Al4V is commonly used in the aerospace, medical and automotive industries due to its high strength-to-weight ratio and excellent corrosion resistance properties. Interstitial impurities in titanium alloys have an impact upon mechanical properties, particularly oxygen, nitrogen, hydrogen and carbon. The plasma spheroidisation process can be used to spheroidise metal powder consisting of irregularly shaped particles. In this study, the plasma spheroidisation of metal powder was performed on Ti6Al4V powder consisting of irregularly shaped particles. The properties of the powder relevant for powder bed fusion that were determined included the particle size distribution, morphology, particle porosity and chemical composition. Conclusions were drawn regarding the viability of using this process to produce powder suitable for additive manufacturing.


Metals ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1700
Author(s):  
Ryan Harkin ◽  
Hao Wu ◽  
Sagar Nikam ◽  
Justin Quinn ◽  
Shaun McFadden

Titanium alloy powder used for laser-based powder bed fusion (L-PBF) process is costly. One of the solutions is the inclusion of a powder recycling strategy, allowing unused or exposed powder particles to be recuperated post manufacture, replenished and used for future builds. However, during a L-PBF process, powder particles are exposed to high levels of concentrated energy from the laser. Particularly those in close proximity to the melt pool, leading to the formation of spatter and agglomerated particles. These particles can settle onto the powder bed, which can then influence the particle size distribution and layer uniformity. This study analysed extra-low interstitial (ELI) Ti6Al4V (Grade 23) powder when subjected to nine recycle iterations, tracking powder property variation across the successive recycling stages. Characterisation included chemical composition focusing upon O, N, and H content, particle size distribution, morphology and tapped and bulk densities. On review of the compositional analysis, the oxygen content exceeded the 0.13% limit for the ELI grade after 8 recycles, resulting in the degradation from Grade 23 level.


2021 ◽  
pp. 109858
Author(s):  
Galina Kasperovich ◽  
Ralf Becker ◽  
Katia Artzt ◽  
Pere Barriobero-Vila ◽  
Guillermo Requena ◽  
...  

Metals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 144
Author(s):  
Eslam M. Fayed ◽  
Mohammad Saadati ◽  
Davood Shahriari ◽  
Vladimir Brailovski ◽  
Mohammad Jahazi ◽  
...  

In the present study, multi-objective optimization is employed to develop the optimum heat treatments that can achieve both high-mechanical performance and non-distinctive crystallographic texture of 3D printed Inconel 718 (IN718) fabricated by laser powder bed fusion (LPBF). Heat treatments including homogenization at different soaking times (2, 2.5, 3, 3.5 and 4 h) at 1080 °C, followed by a 1 h solution treatment at 980 °C and the standard aging have been employed. 2.5 h is found to be the homogenization treatment threshold after which there is a depletion of hardening precipitate constituents (Nb and Ti) from the γ-matrix. However, a significant number of columnar grains with a high fraction (37.8%) of low-angle grain boundaries (LAGBs) have still been retained after the 2.5 h homogenization treatment. After a 4 h homogenization treatment, a fully recrystallized IN718 with a high fraction of annealing twins (87.1%) is obtained. 2.5 and 4 h homogenization treatments result in tensile properties exceeding those of the wrought IN718 at both RT and 650 °C. However, considering the texture requirements, it is found that the 4 h homogenization treatment offers the optimum treatment, which can be used to produce IN718 components offering a balanced combination of high mechanical properties and adequate microstructural isotropy.


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