scholarly journals Influence and Sensitivity of Temperature and Microstructure on the Fluctuation of Creep Properties in Ni-Base Superalloy

Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 4758
Author(s):  
Zhihao Yao ◽  
Biao Zhou ◽  
Kaijun Yao ◽  
Hongying Wang ◽  
Jianxin Dong ◽  
...  

In this work, the sensitivity zone of microstructure and temperature for precipitation-strengthened nickel-based superalloys, used for turbine applications in aero-engines, has been firstly established. Heat treatment experiments with different solution temperatures were carried out. The microstructure evolution and creep residual strain sensitivity, low cycle fatigue properties, and tensile properties are analyzed, and the essential reason for the fluctuation of the mechanical properties of nickel-based superalloys was revealed. The main results obtained are as follows: following subsolvus solution heat treatment with a temperature of 1020 °C, samples have a high primary γ′I phase content, which is beneficial to low creep residual strain. Above the supersolvus solution temperature of 1040 °C, the creep residual strain value and low cycle fatigue performance fluctuate significantly. The essential reason for the dramatic fluctuation of performance is the presence of γ′ phases in different sizes and quantities, especially following the solution heat treatment in the temperature-sensitive zone of the γ′I phase, which is likely to cause huge fluctuations in the microstructure of tertiary γ′III phases. A zone of particular sensitivity in terms of temperature and microstructure for the γ′I phase is proposed. The range of suitable solution temperatures are discussed. In order to maintain stable mechanical properties without large fluctuations, the influence of the sensitivity within this temperature and microstructure zone on the γ′ phase should be considered.

2006 ◽  
Vol 118 ◽  
pp. 71-76 ◽  
Author(s):  
Jae Keun Hong ◽  
Ji Hong Park ◽  
Nho Kwang Park ◽  
Seong Jun Kim ◽  
Chung Yun Kang

Effects of solution treatment on the microstructure and mechanical properties in wrought Alloy 718 were investigated. For the improvement of tensile and fatigue properties of wrought Alloy 718, a modified solution heat treatment(MSHT), heating at 1000 for 3 minutes followed by furnace cooling at the rate of 3/minute and holding at 985 for 8 minutes, was proposed. This treatment was performed repeatedly 3 times and the samples were subject to the standard aging treatment. For the purpose of comparison, a standard heat treatment(SHT) was also performed. The microstructures of modified solution heat treated specimens showed that small spherical shaped δ- phases were precipitated without grain growth, and the amount of δ-phases was smaller than that of standard heat treated specimens. However, the δ-phases of the standard heat-treated specimen showed needle-like morphologies. Tensile and low cycle fatigue tests were performed on both modified heat-treated and standard heat-treated specimens at room temperature, 350 and 650. Low cycle fatigue tests on the modified heat treated specimens showed promising results without reduction of strength. However, the tensile properties of modified solution treated specimens was almost the same as those of standard heat treated materials both at room temperature and 650.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4237
Author(s):  
Takuma Tanaka ◽  
Togo Sugioka ◽  
Tatsuya Kobayashi ◽  
Ikuo Shohji ◽  
Yuya Shimada ◽  
...  

The effect of heat treatment on tensile and low cycle fatigue properties of the oxygen-free copper for electric power equipment was investigated. The heat treatment at 850 °C for 20 min, which corresponds to the vacuum brazing process, caused the grain growth and relaxation of strain by recrystallization, and thus, the residual stress in the oxygen-free copper was reduced. The tensile strength and 0.2% proof stress were decreased, and elongation was increased by the heat treatment accompanying recrystallization. The plastic strain in the heat-treated specimen was increased compared with that in the untreated specimen under the same stress amplitude condition, and thus, the low cycle fatigue life of the oxygen-free copper was degraded by the heat treatment. Striation was observed in the crack initiation area of the fractured surface in the case of the stress amplitude less than 100 MPa regardless of the presence of the heat treatment. With an increase in the stress amplitude, the river pattern and the quasicleavage fracture were mainly observed in the fracture surfaces of the untreated specimens, and they were observed with striations in the fracture surfaces of the heat-treated ones. The result of the electron backscattered diffraction (EBSD) analysis showed that the grain reference orientation deviation (GROD) map was confirmed to be effective to investigate the fatigue damage degree in the grain by low cycle fatigue. In addition, the EBSD analysis revealed that the grains were deformed, and the GROD value reached approximately 28° in the fractured areas of heat-treated specimens after the low cycle fatigue test.


2010 ◽  
Vol 638-642 ◽  
pp. 455-460 ◽  
Author(s):  
A. Rutecka ◽  
L. Dietrich ◽  
Zbigniew L. Kowalewski

The AlSi8Cu3 and AlSi7MgCu0.5 cast aluminium alloys of different composition and heat treatment were investigated to verify their applicability as cylinder heads in the car engines [1]. Creep tests under the step-increased stresses at different temperatures, and low cycle fatigue (LCF) tests for a range of strain amplitudes and temperatures were carried out. The results exhibit a significant influence of the heat treatment on the mechanical properties of the AlSi8Cu3 and AlSi7MgCu0.5. An interesting fact is that the properties strongly depend on the type of quenching. Lower creep resistance (higher strain rates) and lower stress response during fatigue tests were observed for the air quenched materials in comparison to those in the water quenched. Cyclic hardening/softening were also observed during the LCF tests due to the heat treatment applied. The mechanical properties determined during the tests can be used to identify new constitutive equations and to verify existing numerical models.


Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5737
Author(s):  
Janusz Kluczyński ◽  
Lucjan Śnieżek ◽  
Krzysztof Grzelak ◽  
Janusz Torzewski ◽  
Ireneusz Szachogłuchowicz ◽  
...  

The paper is a project continuation of the examination of the additive-manufactured 316L steel obtained using different process parameters and subjected to different types of heat treatment. This work contains a significant part of the research results connected with material analysis after low-cycle fatigue testing, including fatigue calculations for plastic metals based on the Morrow equation and fractures analysis. The main aim of this research was to point out the main differences in material fracture directly after the process and analyze how heat treatment affects material behavior during low-cycle fatigue testing. The mentioned tests were run under conditions of constant total strain amplitudes equal to 0.30%, 0.35%, 0.40%, 0.45%, and 0.50%. The conducted research showed different material behaviors after heat treatment (more similar to conventionally made material) and a negative influence of precipitation heat treatment of more porous additive manufactured materials during low-cycle fatigue testing.


2018 ◽  
Vol 157 ◽  
pp. 02053 ◽  
Author(s):  
Eva Tillová ◽  
Mária Chalupová ◽  
Lenka Kuchariková ◽  
Juraj Belan ◽  
Denisa Závodská

The effect of solution treatment on mechanical properties (UTS, elongation, Brinell hardness) and microstructure (Si-morphology and Si-size) of an aluminium alloy (A356) used for casting cylinder heads was studied. The tests were carried out with specimens machined from the bulkheads of V8 engine blocks cast by the low pressure process. The samples were tested in as-cast and T6 heat treating conditions (solution heat treatment at 530°C with different time - 2, 3, 4, 5, 6, 7 hours, quenching in water at 20°C and precipitation hardened for 4 hour at 160°C). The results show that used heat treatment improves mechanical properties of the cylinder head casts. Tensile strength and hardness of specimens increase with solution treatment time. The hardness is a reflection of solution strengthening and silicon particle distribution in matrix. Solution temperature 530°C and 5 hours solution time is appropriate to obtain better morphology and distribution of Si particles in microstructure. Prolonged solution treatment (more than 5 hours) leads to a coarsening of the Si particles, while the numerical Si density decreases. As the particle density decreases, a fewer number of sites are available for crack nucleation, and hence, the fracture properties are improved. The data obtained from this study will be used to improve process control, and to help the selection of heat treatment of the casting for future products.


2021 ◽  
Author(s):  
Ke Wang

A newly-developed rare earth-containing ME20 magnesium alloy was studied in this thesis. As a potential structural material for applications in automotive industry, low cycle fatigue properties are inevitably required. Strain-controlled low cycle fatigue tests were conducted on this wrought alloy with different specimen orientations. Microstructure, tensile behaviors and low cycle fatigue properties were studied. The effect of different specimen orientations on microstructures and mechanical properties were also discussed. Results show that rare earth element addition in this alloy helped weaken the texture and specimen orientations had little influence over microstructure and fatigue properties of this magnesium alloy.


2020 ◽  
Vol 405 ◽  
pp. 357-364
Author(s):  
Lenka Kuchariková ◽  
Eva Tillová ◽  
Ivana Švecová

Al-Si-Cu alloy systems have a great importance in the casting industry due to their excellent castability, good mechanical properties and wear resistance. Addition of alloying elements, such as Mg and Cu, makes these alloys heat treatable. Improving of their mechanical properties allows their using in new, more demanding applications (e.g. engines, cylinder heads etc.). The most applied heat treatment for this alloy is a T6 (age hardening). Such a heat treatment is required for precipitation of the Al2Cu hardening dispersed phase that increases the mechanical properties of Al alloys. Therefore, the consequences of different solution heat treatment temperatures 505, 515 and 525 °C for AlSi9Cu3 and 515, 525 and 545 °C for AlSi12Cu1Fe cast alloys, with holding times 2, 4, 8, 16 and 32 hours, were investigated in this study. The effect of solution treatment was evaluated based on changes in microstructure (optical microscopy) and mechanical properties (hardness, impact energy and ultimate tensile strength). The study confirms the strengthening of the experimental alloys caused by application of optimum conditions of T6 and melting of the Cu-rich phases with application of inappropriate solution temperature, as well as distortion and changes of the testing bars.


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