scholarly journals Increasing Fatigue Life of 09Mn2Si Steel by Helical Rolling: Theoretical–Experimental Study on Governing Role of Grain Boundaries

Materials ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 4531
Author(s):  
Sergey Panin ◽  
Ilya Vlasov ◽  
Pavel Maksimov ◽  
Dmitry Moiseenko ◽  
Pavlo Maruschak ◽  
...  
Keyword(s):  
Fatigue Life ◽  
Grain Boundaries ◽  
Elastic Energy ◽  
High Strength ◽  
Coarse Grained ◽  
Material Structure ◽  
Structure Transformation ◽  
Helical Rolling ◽  
Fine Grained ◽  
Fine Grained Structure

The structure and mechanical properties of the 09Mn2Si high-strength low-alloyed steel after the five-stage helical rolling (HR) were studied. It was revealed that the fine-grained structure had been formed in the surface layer ≈ 1 mm deep as a result of severe plastic strains. In the lower layers, the “lamellar” structure had been formed, which consisted of thin elongated ferrite grains oriented in the HR direction. It was shown that the five-stage HR resulted in the increase in the steel fatigue life by more than 3.5 times under cyclic tension. The highest values of the number of cycles before failure were obtained for the samples cut from the bar core. It was demonstrated that the degree of the elastic energy dissipation in the steel samples under loading directly depended on the area of the grain boundaries as well as on the grain shapes. The fine-grained structure possessed the maximum value of the average torsional energy among all the studied samples, which caused the local material structure transformation and the decrease in the elastic energy level. This improved the crack resistance under the cyclic mechanical loading. The effect of the accumulation of the rotational strain modes at the grain boundaries was discovered, which caused the local structure transformation at the boundary zones. In the fine-grained structure, the formation of grain conglomerates was observed, which increased the values of the specific modulus of the moment of force. This could be mutually compensated due to the small sizes of grains. At the same time, the coarse-grained structures were characterized by the presence of the small number of grains with a high level of the moments of forces at their boundaries. They could result in trans-crystalline cracking.

Microstructural Refinement in a Commercial Aluminum Alloy Processed by ECAP Using a Die Channel Angle of 110 Degrees

2015 ◽  
Vol 1114 ◽  
pp. 3-8
Author(s):  
Nicolae Şerban ◽  
Doina Răducanu ◽  
Nicolae Ghiban ◽  
Vasile Dănuţ Cojocaru
Keyword(s):  
Grain Refinement ◽  
Cross Section ◽  
High Strength ◽  
Secondary Phase ◽  
Coarse Grained ◽  
Metallographic Analysis ◽  
Second Phase ◽  
Channel Angle ◽  
Ambient Temperatures ◽  
Fine Grained

The properties of ultra-fine grained materials are superior to those of corresponding conventional coarse grained materials, being significantly improved as a result of grain refinement. Equal channel angular pressing (ECAP) is an efficient method for modifying the microstructure by refining grain size via severe plastic deformation (SPD) in producing ultra-fine grained materials (UFG) and nanomaterials (NM). The grain sizes produced by ECAP processing are typically in the submicrometer range and this leads to high strength at ambient temperatures. ECAP is performed by pressing test samples through a die containing two channels, equal in cross-section and intersecting at a certain angle. The billet experiences simple shear deformation at the intersection, without any precipitous change in the cross-section area because the die prevents lateral expansion and therefore the billet can be pressed more than once and it can be rotated around its pressing axis during subsequent passes. After ECAP significant grain refinement occurs together with dislocation strengthening, resulting in a considerable enhancement in the strength of the alloys. A commercial AlMgSi alloy (AA6063) was investigated in this study. The specimens were processed for a number of passes up to nine, using a die channel angle of 110°, applying the ECAP route BC. After ECAP, samples were cut from each specimen and prepared for metallographic analysis. The microstructure of the ECAP-ed and as-received material was investigated using optical (OLYMPUS – BX60M) and SEM microscopy (TESCAN VEGA II – XMU). It was determined that for the as-received material the microstructure shows a rough appearance, with large grains of dendritic or seaweed aspect and with a secondary phase at grain boundaries (continuous casting structure). For the ECAP processed samples, the microstructure shows a finished aspect, with refined, elongated grains, also with crumbled and uniformly distributed second phase particles after a typical ECAP texture.

Influence of cooling media in achieving grain refinement of AA2014 alloy using friction stir processing

2020 ◽  
Vol 234 (22) ◽  
pp. 4520-4534
Author(s):  
MVNV Satyanarayana ◽  
Adepu Kumar
Keyword(s):  
Grain Boundaries ◽  
Friction Stir Processing ◽  
Heat Dissipation ◽  
Electron Backscattered Diffraction ◽  
Friction Stir ◽  
Fine Grained ◽  
Fine Grained Structure ◽  
Cooling Media ◽  
Processing Zone ◽  
Friction Stir Processing Sample

The present paper studies the influence of different cooling media (water and cryogenic media) on microstructure, mechanical, and corrosion behavior of friction stir processing of AA2014. From the electron backscattered diffraction results, it was observed that the grain size in stir zone of air-cooled friction stir processing, dry ice-cooled friction stir processing, and underwater friction stir processing are 4.9 µm, 3.5 µm, and 0.9 µm respectively, and the fraction of high angle grain boundaries are more in underwater friction stir processing sample compared to other conditions. The ultra-fine grained structure (0.9 µm) was achieved in underwater friction stir processing due to uniform heat dissipation from the processing zone to the water. Mechanical properties such as hardness and strength were improved in underwater friction stir processing compared to other conditions. The fine precipitates formed in the underwater friction stir processing sample were distributed randomly at grain boundaries, and hence corrosion resistance was improved in underwater friction stir processing sample compared to other conditions.

scholarly journals Microstructural and Mechanical Characterization of Multilayered Iron Electrodeposits

2011 ◽  
Vol 409 ◽  
pp. 474-479 ◽  
Author(s):  
C. Chan ◽  
J.L. McCrea ◽  
G. Palumbo ◽  
Uwe Erb
Keyword(s):  
Mechanical Properties ◽  
Columnar Structure ◽  
Multilayered Structure ◽  
Structure Design ◽  
Coarse Grained ◽  
Fine Grained ◽  
Microstructure And Mechanical Properties ◽  
Fine Grained Structure ◽  
Iron Coatings

Monolithic and multilayered iron electrodeposits were successfully synthesized by the pulse plating electrodeposition method. Electron microscopy and Vickers microhardness measurements were used to investigate the microstructure and mechanical properties of the iron electrodeposits produced. Two types of monolithic iron coatings were produced, one with a coarse grained, columnar structure and the other with an ultra-fine grained structure. Hall-Petch type grain size strengthening was observed in these monolithic coatings. Multilayered iron coatings composed of alternating layers of coarse grained and fine grained structures were also produced. The hardness value of the multilayered coatings falls between the hardness values for the two types of monolithic coatings produced. This study has demonstrated the possibility of applying a multilayered structure design to tailor the microstructure and mechanical properties of electrodeposited iron coatings.

Mössbauer Spectroscopy of Grain Boundaries in Ultrafine-Grained Metal Materials

2014 ◽  
Vol 783-786 ◽  
pp. 2671-2676 ◽  
Author(s):  
Vladimir V. Popov
Keyword(s):  
Grain Boundaries ◽  
The State ◽  
Coarse Grained ◽  
Resonance Spectroscopy ◽  
Fine Grained ◽  
Nuclear Gamma Resonance ◽  
Ultrafine Grained ◽  
Emission Mode ◽  
Metal Materials

Capabilities of the Mössbauer (nuclear gamma-resonance) spectroscopy for investigation of the state of grain boundaries in ultra-fine grained materials are analyzed, and the main problems of such studies are discussed. The emission and absorption NGR spectroscopy are compared, and it is demonstrated that the emission mode of the Mössbauer spectroscopy is preferential for GB studies. These studies enable to reveal differences in the state of GBs in ultra-fine grained materials and coarse-grained polycrystals with GBs of recrystallization origin.

Influence of Physical Properties of B4C Powder on the Strength Properties of the Ceramics Manufactured by SPS Sintering

2015 ◽  
Vol 1085 ◽  
pp. 312-315
Author(s):  
Oleg L. Khasanov ◽  
Edgar S. Dvilis ◽  
Zulfa G. Bikbaeva ◽  
Valentina V. Polisadova ◽  
Alexey O. Khasanov ◽  
...  
Keyword(s):  
Physical Properties ◽  
Boron Carbide ◽  
Physical And Mechanical Properties ◽  
High Strength ◽  
Strength Properties ◽  
Carbide Powder ◽  
Fine Grained ◽  
Fine Grained Structure ◽  
Determining Factor ◽  
Sps Sintering

Ceramics samples in the form of a parallelepiped with high strength characteristics have been made. For the manufacture of the ceramics samples a powder mixture from submicron В4С powder with additives (1 wt%, 5 wt%, 10 wt%) of boron carbide nanopowder was used. The physical properties of the powder mixtures and strength properties of sintered ceramics have been studied. It was shown that the use of submicron fractions of the boron carbide powder together with nanoadditives is a determining factor in the formation of dense fine-grained structure providing improved physical and mechanical properties of the ceramics.

Hybrid Design Concept Using High-Strength Cast Steel Inserts for Tubular Joints of Offshore Structures

1998 ◽  
Vol 120 (1) ◽  
pp. 10-19 ◽  
Author(s):  
C. M. Sonsino ◽  
R. Umbach
Keyword(s):  
Fatigue Life ◽  
Crack Initiation ◽  
Large Scale ◽  
Fatigue Behavior ◽  
Cast Steel ◽  
High Strength ◽  
Offshore Structures ◽  
Fine Grained ◽  
Tubular Joints ◽  
Medium Strength

In a joint project of a German working group supported by the ECSC and the Studiengesellschaft fu¨r Stahlanwendung e.V., the fatigue behavior of large-scale hybrid tubular joints with inserts manufactured from the high-strength cast steel GS-12 MnMo 7 4 welded into tubular members formed from the fine-grained steel StE 500 were compared to the behavior of large-scale welded tubular joints. The latter were made from medium-strength fine-grained steel StE 355 and high-strength StE 690. In addition, data from hybrid joints with cast steel inserts of medium-strength GS-8 Mn 7 welded into StE 355 tubulars is available for comparison. The tests were carried out under variable amplitude loading in artificial seawater. The results were evaluated for the failure criteria fatigue life to crack initiation (a = 1 mm) and through crack. With medium-strength (Rp0.2 > 355 N/mm2) hybrid tubulars, where by the use of cast steel inserts the welds were removed into areas of lower stress concentration, fatigue lives higher than a factor of 100 were achieved compared to the welded nodes, even those made from StE 690. However, by the use of high-strength (Rp0.2 > 500 N/mm2) cast steel inserts and tubular members of corresponding strength, the fatigue life to crack initiation was improved by a factor of two despite a thickness reduction compared to the medium-strength design. Post-weld treatments of the welded tubulars without cast steel inserts like shot-peening, TIG-dressing, or their combination resulted only in a slight increase of fatigue life. The results of this investigation do not only show how to improve the fatigue life by a new design using cast steel inserts, but indicate also how to revise design codes from the point of damage calculation (damage sum of 0.50 for welded nodes and 0.25 for cast steel inserts instead of the conventional value of 1.00), as well as consideration of fatigue life to initiation of a technically detectable crack with a defined depth e.g., a = 1 mm.

The Influence of Addition of the Rare Earth Elements on the Structure and Hardness of AlZn12Mg3.5Cu2.5 Alloy

2015 ◽  
Vol 226 ◽  
pp. 39-42
Author(s):  
Rafał Michalik ◽  
Tomasz Mikuszewski
Keyword(s):  
Rare Earth ◽  
Automotive Industry ◽  
Electrical Power ◽  
High Strength ◽  
Hardness Test ◽  
Relative Strength ◽  
Zinc Alloys ◽  
Fine Grained ◽  
Fine Grained Structure ◽  
High Strength Aluminum Alloys

Aluminium alloys are characterized by a number of advantageous properties , which include: low density ,high relative strength , high electrical and thermal conductivity , ease of machining and good dumping features. Particular interesting are high-strength aluminum alloys of zinc, magnesium and copper. These alloys are used mainly in aircraft, building &structure, electrical, electrical power and automotive industry. A significant problem associated with the use of high-strength aluminium-zinc alloys is their insufficient resistance to corrosion. Improvement of corrosion resistance can be obtained by application of alloy micro-additives. The article shows results of examinations related to influence of rare earth additive on the structure and hardness of AlZn12Mg3.5Cu2.5 alloy. The scope of examination included: structure testing using scanning microscope, X – ray microanalysis, hardness test. Examinations have shown higher hardness of samples with rare earth additives. Was found , that rare earth addition influences on more fine –grained structure of the AlZn12Mg3.5Cu2.5 alloy.

The critical influence of La content on the microstructure-toughness relationship in the simulated coarse-grained heat-affected zone of high-strength low-alloy steels

2021 ◽  
Vol 118 (2) ◽  
pp. 212
Author(s):  
Yuxin Cao ◽  
Xiangliang Wan ◽  
Feng Zhou ◽  
Hangyu Dong ◽  
Kaiming Wu ◽  
...  
Keyword(s):  
Heat Affected Zone ◽  
Acicular Ferrite ◽  
High Strength ◽  
Coarse Grained ◽  
Low Alloy Steels ◽  
Fine Grained ◽  
Welding Thermal Cycle ◽  
Alloy Steels ◽  
High Fraction ◽  
The Impact

The present study was envisaged to investigate the role of La content on the particle, microstructure and toughness in the simulated coarse-grained heat-affected zone (CGHAZ) of high-strength low-alloy steels. Three steels with La content of 0.016 wt.%, 0.046 wt.% and 0.093 wt.% were prepared and simulated in a 100 kJ/cm heat input welding thermal cycle. Subsequently, the particle and microstructure of selected specimens were characterized and the impact absorb energy was measured at −20 °C. The results indicated that the La2O2S inclusions in 0.016 wt.%-La steel were gradually modified to LaS-LaP in 0.046 wt.%-La steel and to LaP in 0.093 wt.%-La steel. A higher fraction of acicular ferrite was obtained in the simulated CGHAZ of 0.016 wt.%-La steel, since the inclusion of La2O2S was more powerful to induce the formation of acicular ferrite. Furthermore, the fraction of M-A constituents in the simulated CGHAZ increased with increasing La content. The impact toughness in the simulated CGHAZ of 0.016 wt.%-La steel was the highest, owing to the high fraction of the fine-grained acicular ferrite and low fraction of M-A constituent.

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