scholarly journals Effect of Cleaning Protocol on Bond Strength between Resin Composite Cement and Three Different CAD/CAM Materials

Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 4150
Author(s):  
Nina Lümkemann ◽  
Lisa Marie Schönhoff ◽  
Ramona Buser ◽  
Bogna Stawarczyk
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Resin Composite ◽  
Composite Cement ◽  
Fracture Patterns ◽  
Computer Aided ◽  
Cad Cam ◽  
The Impact ◽  
Resin Composite Cement ◽  
Cleaning Protocol

The present investigation tested the effect of the cleaning method on the tensile bond strength (TBS) between one resin composite cement (RCC) and three different computer aided design/computer aided manufacturing (CAD/CAM) materials, namely zirconia, lithium disilicate ceramic and resin composite. Ninety specimens were prepared from each CAD/CAM material (N = 270). The specimens were pre-treated respectively, divided into five subgroups and subjected to five different cleaning protocols, namely i. 37% phosphoric acid, ii. ethanol, iii. phosphoric acid + ethanol, iv. cleaning paste, v. distilled water. After cleaning, the specimens were either conditioned using a universal primer or a universal adhesive and bonded using a dual-curing RCC. After thermo-cycling (20,000x at 5 °C/55 °C), TBS and fracture patterns were evaluated. The data was analyzed using 1- and 2-way Analysis of Variance (ANOVA) with post-hoc Scheffé and partial eta-squared (ƞP²), Kruskal–Wallis, Mann–Whitney U and Chi2 tests (p < 0.05). The CAD/CAM material showed an impact on the BS while the cleaning protocol did not affect the results. Zirconia obtained the highest BS, followed by lithium-disilicate-ceramic. Resin composite resulted in the overall lowest BS. For most fracture patterns, the cohesive type occurred. All tested cleaning protocols resulted in same BS values within one CAD/CAM material indicating that the impact of the cleaning method for the restorative material seems to play a subordinate role in obtaining durable bond strength to resin composite cement. Further, it indicates that the recommended bonding protocols are well adjusted to the respective materials and might be able to compensate the impact of not accurately performed cleaning protocols.

Impact of Recently Developed Universal Adhesives on Tensile Bond Strength to Computer-aided Design/Manufacturing Ceramics

2019 ◽  
Vol 44 (4) ◽  
pp. 386-395 ◽  
Author(s):  
A Liebermann ◽  
J Detzer ◽  
B Stawarczyk
Keyword(s):  
Bond Strength ◽  
Computer Aided Design ◽  
Resin Composite ◽  
Tensile Bond Strength ◽  
Adhesive Systems ◽  
Computer Aided ◽  
Cad Cam ◽  
Aided Design ◽  
Failure Types ◽  
Resin Composite Cement

SUMMARY Objectives: The aim of this investigation was to test the tensile bond strength (TBS) between different computer-aided-design/manufacturing (CAD/CAM) ceramics after conditioning using different universal adhesive systems and resin composite cement. Methods and Materials: Substrates of four CAD/CAM ceramics—1) VITABLOCS Mark II, 2) Initial LRF, 3) Celtra Duo, and 4) IPS e.max CAD (N=648, n=162)—were fabricated. VITABLOCS Mark II and Initial LRF were etched using 9% hydrofluoric acid for 60 seconds, Celtra Duo for 30 seconds, and IPS e.max CAD for 20 seconds. Substrates for conditioning using Monobond Etch & Prime were untreated. The following adhesive systems were used: All-Bond Universal (ABU), Clearfil Universal Bond (CUB), G-Multi Primer (GMP), iBond Universal (IBU), Monobond Etch & Prime (MEP), Monobond Plus (MBP), One Coat 7 Universal (OCU), Prime&Bond Active (PBA), and Scotchbond Universal (SBU). Conditioned substrates were bonded using a resin composite cement (Variolink Esthetic DC), thermal cycled (20,000×, 5°C/55°C), and TBS was measured using a universal testing machine. Data were analyzed using univariate analysis with partial eta-squared, Kolmogorov-Smirnov, Kruskal-Wallis, Mann-Whitney U, and Spearman-Rho tests (α=0.05). Results: ABU, MEP, and MBP obtained the significantly highest TBS, while CUB, IBU, and OCO resulted in the lowest, regardless of the CAD/CAM ceramic. SBU showed varying TBS results depending on the CAD/CAM ceramic used. ABU, MEP, and MBP showed no impact of CAD/CAM ceramic on TBS values. ABU, GMP, MEP, and MBP showed predominantly cohesive failure types in luting composite, while CUB and OCU demonstrated adhesive failure types.

scholarly journals Effects of Immediate and Delayed Cementations for CAD/CAM Resin Block after Alumina Air Abrasion on Adhesion to Newly Developed Resin Cement

Materials ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 7058
Author(s):  
Akane Chin ◽  
Masaomi Ikeda ◽  
Tomohiro Takagaki ◽  
Toru Nikaido ◽  
Alireza Sadr ◽  
...  
Keyword(s):  
Bond Strength ◽  
Water Sorption ◽  
Resin Composite ◽  
Resin Cement ◽  
Air Abrasion ◽  
Resin Cements ◽  
Significant Difference ◽  
Computer Aided ◽  
Cad Cam ◽  
Curing Methods

The purpose of this study was to evaluate the effect of one week of Computer-aided design/Computer-aided manufacturing (CAD/CAM) crown storage on the μTBS between resin cement and CAD/CAM resin composite blocks. The micro-tensile bond strength (μTBS) test groups were divided into 4 conditions. There are two types of CAD/CAM resin composite blocks, namely A block and P block (KATANA Avencia Block and KATANA Avencia P Block, Kuraray Noritake Dental, Tokyo, Japan) and two types of resin cements. Additionally, there are two curing methods (light cure and chemical cure) prior to the μTBS test—Immediate: cementation was performed immediately; Delay: cementation was conducted after one week of storage in air under laboratory conditions. The effect of Immediate and Delayed cementations were evaluated by a μTBS test, surface roughness measurements, light intensity measurements, water sorption measurements and Scanning electron microscope/Energy dispersive X-ray spectrometry (SEM/EDS) analysis. From the results of the μTBS test, we found that Delayed cementation showed significantly lower bond strength than that of Immediate cementation for both resin cements and both curing methods using A block. There was no significant difference between the two types of resin cements or two curing methods. Furthermore, water sorption of A block was significantly higher than that of P block. Within the limitations of this study, alumina air abrasion of CAD/CAM resin composite restorations should be performed immediately before bonding at the chairside to minimize the effect of humidity on bonding.

The effect of ceramic primer on shear bond strength of resin composite cement to zirconia

2013 ◽  
Vol 144 (11) ◽  
pp. 1261-1271 ◽  
Author(s):  
Christine Keul ◽  
Anja Liebermann ◽  
Malgorzata Roos ◽  
Julia Uhrenbacher ◽  
Bogna Stawarczyk
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Composite Cement ◽  
Resin Composite Cement

scholarly journals The Bond of Different Post Materials to a Resin Composite Cement and a Resin Composite Core Material

2012 ◽  
Vol 37 (6) ◽  
pp. E38-E49 ◽  
Author(s):  
D Stewardson ◽  
A Shortall ◽  
P Marquis
Keyword(s):  
Bond Strength ◽  
Chemical Interaction ◽  
Resin Composite ◽  
Resin Cement ◽  
Core Material ◽  
Composite Cement ◽  
Grit Blasting ◽  
Bond Strengths ◽  
Push Out ◽  
Resin Composite Cement

SUMMARY Purpose To investigate the bond of endodontic post materials, with and without grit blasting, to a resin composite cement and a core material using push-out bond strength tests. Materials and Methods Fiber-reinforced composite (FRC) posts containing carbon (C) or glass (A) fiber and a steel (S) post were cemented into cylinders of polymerized restorative composite without surface treatment (as controls) and after grit blasting for 8, 16, and 32 seconds. Additional steel post samples were sputter-coated with gold before cementation to prevent chemical interaction with the cement. Cylindrical composite cores were bonded to other samples. After sectioning into discs, bond strengths were determined using push-out testing. Profilometry and electron microscopy were used to assess the effect of grit blasting on surface topography. Results Mean (standard deviation) bond strength values (MPa) for untreated posts to resin cement were 8.41 (2.80) for C, 9.61(1.88) for A, and 19.90 (3.61) for S. Prolonged grit blasting increased bond strength for FRC posts but produced only a minimal increase for S. After 32 seconds, mean values were 20.65 (4.91) for C, 20.41 (2.93) for A, and 22.97 (2.87) for S. Gold-coated steel samples produced the lowest bond strength value, 7.84 (1.40). Mean bond strengths for untreated posts bonded to composite cores were 6.19 (0.95) for C, 13.22 (1.61) for A, and 8.82 (1.18) for S, and after 32 seconds of grit blasting the values were 17.30 (2.02) for C, 26.47 (3.09) for A, and 20.61 (2.67) for S. FRC materials recorded higher roughness values before and after grit blasting than S. With prolonged grit blasting, roughness increased for A and C, but not for S. Conclusions There was no evidence of significant bonding to untreated FRC posts, but significant bonding occurred between untreated steel posts and the resin cement. Increases in the roughness of FRC samples were material dependent and roughening significantly increased bond strength values (p&lt;0.05). Surface roughening of the tested FRC posts is required for effective bonding.

Influence of resin composite cement on the final color of fixed rehabilitation

2019 ◽  
pp. 53-56
Author(s):  
Joana F. Piloto ◽  
Claudia A.M. Volpato ◽  
Paulo Rocha ◽  
Paulo Júlio Almeida ◽  
César Silva ◽  
...  
Keyword(s):  
Resin Composite ◽  
Composite Cement ◽  
Resin Composite Cement ◽  
Final Color

Effect of In-office Bleaching on Color, Translucency, and Whiteness Variations in CAD-CAM Monolithic Materials

2021 ◽  
Author(s):  
RG Fonseca ◽  
RC Peńa ◽  
R Simóes ◽  
AC Ramos ◽  
LN Dovigo
Keyword(s):  
Optical Properties ◽  
Computer Aided Design ◽  
Calculated Data ◽  
Color Difference ◽  
Deionized Water ◽  
Stain Removal ◽  
Computer Aided ◽  
Cad Cam ◽  
Aided Design ◽  
The Impact

SUMMARY Little is known about the impact of bleaching on the optical properties of computer-aided design and computer-aided manufactured (CAD-CAM) monolithic materials. The aim of the present study was to evaluate the effect of one session of in-office bleaching on stain removal, staining susceptibility, translucency, and whiteness variations of CADCAM monolithic materials. Disks were fabricated from Lava Ultimate (LU), Vita Enamic (VE), Vita Suprinity (VS), and IPS e.max CAD (IPS). A spectrophotometer was used to register Commission Internationale de l’Eclairage L*a*b* coordinates. For stain removal, 80 specimens from each material were assessed at baseline (R0) and after immersion in deionized water or coffee for 365 days followed or not by bleaching with 40% hydrogen peroxide (R1). For staining susceptibility, 80 specimens from each material were analyzed at baseline (R0’), and after having been bleached or not and immersed in deionized water or coffee (R1’). Both analyses were calculated as the color difference (ΔE00) between R1-R0 and R1’-R0’, respectively. Differences in translucency (ΔTP00) and whiteness (ΔWID) between R1-R0 and R1’-R0’ were also calculated. Data were analyzed by three-way ANOVA and the Games-Howell post hoc test (α=0.05). Clinical significance was based on 50%:50% perceptibility and acceptability thresholds for ΔE00, ΔTP00 and ΔWID, respectively. Surfaces were analyzed by scanning electron microscopy. Coffee increased ΔE00 in LU, VE, and VS, and decreased their translucency and whiteness, whereas the IPS had only its whiteness affected. Bleaching after immersion in coffee decreased ΔE00 in LU and VE, and increased translucency and whiteness of LU, VE, and VS. No effect was observed on IPS. Bleaching before immersion in coffee decreased translucency of LU, but within the acceptable interval, while VE exhibited lower ΔE00, and became more translucent and less dark. Both VS and IPS were not affected. One session of in-office bleaching benefited optical properties of the previously stained LU, VE, and VS, without increasing their susceptibility to staining or adversely providing clinically unacceptable variations in their translucency and whiteness. All variations exhibited by the IPS were below the perceptible threshold.

scholarly journals A comparative study of the microtensile bond strength and microstructural differences between sclerotic and Normal dentine after surface pretreatment

2019 ◽  
Vol 19 (1) ◽  
Author(s):  
Jinhua Wang ◽  
Weijian Song ◽  
Lei Zhu ◽  
Xin Wei
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Sodium Hypochlorite ◽  
Resin Composite ◽  
The Other ◽  
Tensile Bond Strength ◽  
Strength Analysis ◽  
Class Iii ◽  
Surface Pretreatment ◽  
Dentine Surface

Abstract Background The resin bond strength of sclerotic dentine is significantly lower than that of the normal dentine, which paused a challenge for bonding procedures clinically. The aim of this study was to compare the effects of different surface pretreatments on the micro-tensile bond strength and microstructure between sclerotic dentine and normal dentine. Methods Eighty teeth that were collected, forty premolars with typical wedge-shaped defects visually graded as class III were assigned as the sclerotic dentine group (SD), the other forty normal premolars with artificial wedge-shaped defects were assigned as the normal dentine group (ND). Each group was randomly subdivided into eight subgroups according to the solution used: 35% phosphoric acid, 15% EDTA, 5% or 10% NaClO. Then the dentine surface was examined using a scanning electron microscope (SEM). The lesions were restored using self-etching adhesive and the subsequent resin composite. The teeth were sectioned into sticks for the micro-tensile bond strength analysis, and the data were analysed using the SPSS17.0 software package (α = 0.05). Results First, for the ND groups, after pretreatment using 35% phosphoric acid, and 35% phosphoric acid + 5% or 10% sodium hypochlorite, the bonding strengths of the normal dentine were higher than that of the other groups (P < 0.05). Second, for the SD groups, after pretreatment using 35% phosphoric acid, 15% EDTA, and 35% phosphoric acid + 5% or 10% sodium hypochlorite, the bonding strengths of the sclerotic dentine were higher than that of the other groups (P < 0.05). Third, the bond strengths of the sclerotic dentine were lower than that of the normal dentine without any pretreatment (P < 0.05). After pretreatment using 35% phosphoric acid + 5% or 10% sodium hypochlorite, the bonding strengths of the sclerotic dentine were higher than that of the normal dentine (P < 0.05). SEM observation showed that the appearances of dentine surface were changed after pretreatment using the above solutions, with the reduced smear layer, opened small groove and increased dentinal tubules. Conclusion Pretreatment of dentine using 35% phosphoric acid+ 5% or + 10% sodium hypochlorite changed the microstructure of the sclerotic dentine surface and subsequently increased the micro-tensile bond strength.

scholarly journals Effects of Contamination by Hemostatic Agents and Use of Cleaning Agent on Etch-and-Rinse Dentin Bond Strength

2016 ◽  
Vol 27 (6) ◽  
pp. 688-692 ◽  
Author(s):  
César Rogério Pucci ◽  
Rodrigo Maximo de Araújo ◽  
Ana Julia Farias de Lacerda ◽  
Mirella Anjos de Souza ◽  
Maria Filomena Rocha Lima Huhtala ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Control Group ◽  
Hemostatic Agents ◽  
Diamond Bur ◽  
Mechanical Cycling ◽  
Etch And Rinse ◽  
Post Hoc ◽  
Push Out ◽  
Cleaning Protocol

Abstract The aim of this study was to evaluate the influence of contamination by hemostatic agents and rinsing with chlorhexidine on bond strength between dentin and resin composite. Ninety-six bovine teeth were sectioned to expose a flat dentin surface area. A standardized cavity with 2.0 mm in thickness, superficial diameter of 4.0 mm and bottom diameter of 3.0 mm was prepared with a diamond bur in each dentin specimen. The teeth were divided into four groups according to the hemostatic employed: G1: control; G2: use of ViscoStat, Ultradent; G3: Hemosthasegel, FGM; and G4: Hemostop, Dentsply. The groups were divided into two subgroups according to the cleaning protocol method (n=12): A: without any further cleaning; and B: cleaning with chlorhexidine at 0.2%. All cavities were filled using a dentin adhesive and a resin composite, following the manufacturer's instructions. After 24 h, the specimens were aged by thermal and mechanical cycling. The bond strength was determined by the push out bond test (MPa), Statistical analysis was performed using two-way ANOVA and Tukey test (p<0.05). Statistically significant differences were detected among all groups treated with hemostatic agents and the control group. The post-hoc test showed that cleaning the cavity with chlorhexidine significantly improves the bond strength between dentin and resin composite. Our results suggested that the use of chlorhexidine can reestablish the bond strength between dentin and resin composite when a hemostatic agent was applied.

Synthesis, formulation and evaluation of novel zinc-calcium phosphate-based adhesive resin composite cement

2004 ◽  
Vol 40 (8) ◽  
pp. 1723-1731 ◽  
Author(s):  
Dong Xie ◽  
IL-Doo Chung ◽  
Guigui Wang ◽  
Dingsong Feng ◽  
Jimmy Mays
Keyword(s):  
Calcium Phosphate ◽  
Resin Composite ◽  
Adhesive Resin ◽  
Composite Cement ◽  
Resin Composite Cement
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