scholarly journals Estimation of the Adhesion Interface Performance in Aluminum-PLA Joints by Thermographic Monitoring of the Material Extrusion Process

Materials ◽  
2020 ◽  
Vol 13 (15) ◽  
pp. 3371 ◽  
Author(s):  
Stephan Bechtel ◽  
Mirko Meisberger ◽  
Samuel Klein ◽  
Tobias Heib ◽  
Steven Quirin ◽  
...  

Using additive manufacturing to generate a polymer–metal structure offers the potential to achieve a complex customized polymer structure joined to a metal base of high stiffness and strength. A tool to evaluate the generated interface during the process is of fundamental interest, as the sequential deposition of the polymer as well as temperature gradients within the substrate lead to local variations in adhesion depending on the local processing conditions. On preheated aluminum substrates, 0.3 and 0.6 mm high traces of polylactic acid (PLA) were deposited. Based on differential scanning calorimetry (DSC) and rheometry measurements, the substrate temperature was varied in between 150 and 200 °C to identify an optimized manufacturing process. Decreasing the layer height and increasing the substrate temperature promoted wetting and improved the adhesion interface performance as measured in a single lap shear test (up to 7 MPa). Thermographic monitoring was conducted at an angle of 25° with respect to the substrate surface and allowed a thermal evaluation of the process at any position on the substrate. Based on the thermographic information acquired during the first second after extrusion and the preset shape of the polymer trace, the resulting wetting and shear strength were estimated.

Materials ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2512
Author(s):  
Karol Bula ◽  
Tomasz Sterzyński ◽  
Maria Piasecka ◽  
Leszek Różański

In this, work, metal inserts were joined with polyamide 6 by using the injection-molding technique. The metal parts, made of steel grade DC 04, were mechanically interlocked with polyamide 6 (PA6) by rivets as a mechanical connection between both components in the form of s polymer filling the holes in the metallic parts. The mechanical-interlocking joints made of steel/PA6 were mechanically tested in a tensile-lap-shear test. The damage behavior of the joined materials in relation to rivet number and position on the metal plate was studied. The observation of rivet deformation was also conducted by infrared IR thermography. The study showed that, for polymer–metal joined samples with fewer than three rivets, the destruction of rivets by shearing meant sample damage. On the other hand, when the polymer–metal joint was made with three or four rivets, the disruption mechanism was mostly related to the polymer part breaking. The maximal values of the joint’s failure force under tensile-shear tests were achieved for samples where three rivets were used. Moreover, strong correlation was found between the surface temperature of the samples and their maximal force during the tensile-lap-shear test.


2009 ◽  
Vol 13 (9) ◽  
pp. 1073-1082
Author(s):  
Sylvain Chataigner ◽  
Jean-François Caron ◽  
Karim Benzarti ◽  
Marc Quiertant ◽  
Christophe Aubagnac

RSC Advances ◽  
2015 ◽  
Vol 5 (27) ◽  
pp. 21023-21032 ◽  
Author(s):  
Sepideh Khoee ◽  
Zahra Kachoei

Recovery of fracture toughness of a self-healing epoxy adhesive is achieved by using a novel amine nanocontainer.


2021 ◽  
pp. 108201322110692
Author(s):  
Nispa Seetapan ◽  
Bootsrapa Leelawat ◽  
Nattawut Limparyoon ◽  
Rattana Yooberg

Rice noodles have been manufactured in the food industry using different extrusion methods, such as traditional and modern extrusions, which affect the noodle structure and qualities. Therefore, the effects of the extrusion process on qualities of rice noodles using the same blend of rice flour and crosslinked starch were evaluated. In this study, a capillary rheometer was used as an alternative approach to simulate the traditional extrusion method in which the noodles are obtained by continuously pressing the pregelatinized noodle dough through a die. For modern extrusion, a twin-screw extruder was employed to obtain the noodles in a one-step process. The optimal range of moisture content used in the formulation was studied. Upon cooking, the noodles showed a decrease in cooking time and cooking loss with increasing moisture content in the formulation. All cooked noodles showed comparable tensile strength, but those extruded by a twin-screw extruder had substantially greater elongation. Scanning electron micrographs revealed that the noodles prepared using the extruder had a denser starch matrix, while those obtained from a capillary rheometer showed the aggregation of starch fragments relevant to the existence of starch gelatinization endotherm from differential scanning calorimetry. This indicated that the extrusion process using the twin-screw extruder provided a more uniform starch transformation, i.e., more starch granule disruption and gelatinization, thus giving the noodles a more coherent structure and better extensibility after cooking. The obtained results suggested that different thermomechanical processes used in the noodle industry gave the extruded rice noodles different qualities respective to their different microstructures.


Author(s):  
A. F. Galiev ◽  
A. A. Lachinov ◽  
D. D. Karamov ◽  
A. N. Lachinov ◽  
A. R. Yusupov ◽  
...  

1992 ◽  
Vol 06 (08) ◽  
pp. 477-483 ◽  
Author(s):  
QINGXIN SU ◽  
SHIFA XU ◽  
DAFU CUI ◽  
HUIBIN LU ◽  
YONGJUN TIAN ◽  
...  

High-T c superconducting thin films of YBa 2 Cu 3 O 7 were grown in-situ on (100) SrTiO 3 substrates by Nedymium:yttrium aluminum garnet [Nd:YAG] laser ablation. The effects of the substrate temperature on the transition temperature, microcrystalline structure and surface morphology of the films were discussed. Best results were obtained in the 730°–770°C range. X-ray diffraction analysis showed that these films were highly c-oriented with the c-axis perpendicular to the substrate surface. At the optimum substrate temperature, a very smooth morphology with only a few small particles were observed by scanning electron microscopy. The zero resistance temperature of these films were ≥ 90 K with a narrow transition width and the ac susceptibility measurement also gave the same result. The highest critical current density obtained at 77 K and zero magnetic field was 3.8 × 106 A/cm 2.


Author(s):  
T. Renault ◽  
M. Vardelle ◽  
A. Grimaud ◽  
P. Fauchais ◽  
H. Hoffman

Abstract The quality of plasma sprayed coatings depends strongly on substrate surface preparation, especially roughness, grit residue, and oxidation stage; particle spray jet position and size relative to the plasma jet; impacting particle distribution; particle velocity, temperature, and size prior to impact; substrate temperature; and pass thickness. A simple and low-cost spray and deposit control system developed in our laboratory allows to monitor on-line the position, shape, and centroid of the hot particle spray jet. Such a tool has proved to be very sensitive to any drift in powder injection conditions and torch input parameters. Although it gives no direct information on particle velocity and temperature, this system can be easily implemented in an industrial environment and help to maintain constant the particle parameters during spraying. A CCD camera is used in conjunction with a pyrometer making it possible to measure simultaneously substrate temperature. The system can monitor coating parameters such as deposition efficiency and residual stresses. This paper describes how the system can be used to set the tolerance range of process input parameters to obtain coating parameters within given specifications.


Author(s):  
Rupinder Singh ◽  
Gurchetan Singh ◽  
Jaskaran Singh ◽  
Ranvijay Kumar ◽  
Md Mustafizur Rahman ◽  
...  

In this experimental study, a composite of poly-ether-ketone-ketone by reinforcement of hydroxyapatite and chitosan has been prepared for possible applications as orthopaedic scaffolds. Initially, different weight percentages of hydroxyapatite and chitosan were reinforced in the poly-ether-ketone-ketone matrix and tested for melt flow index in order to check the flowability of different compositions/proportions. Suitable compositions revealed by the melt flow index test were then taken forward for the extrusion of filament required for fused deposition modelling. For thermomechanical investigations, Taguchi-based design of experiments has been used with input variables in the extrusion process as follows: temperature, load applied and different composition/proportions. The specimens in the form of feedstock filament produced by the extrusion process were made to undergo tensile testing. The specimens were also inspected by differential scanning calorimetry and photomicrographs. Finally, the specimen showing the best performance from the thermomechanical viewpoint has been selected to extrude the filament for the fused deposition modelling process.


Sign in / Sign up

Export Citation Format

Share Document