scholarly journals Superelastic Behavior of Ti-Nb Alloys Obtained by the Laser Engineered Net Shaping (LENS) Technique

Materials ◽  
2020 ◽  
Vol 13 (12) ◽  
pp. 2827 ◽  
Author(s):  
Damian Kalita ◽  
Łukasz Rogal ◽  
Piotr Bobrowski ◽  
Tomasz Durejko ◽  
Tomasz Czujko ◽  
...  

The effect of Nb content on microstructure, mechanical properties and superelasticity was investigated for a series of Ti-xNb alloys, fabricated by the laser engineered net shaping method, using elemental Ti and Nb powders. The microstructure of as-deposited materials consisted of columnar β-phase grains, elongated in the built direction. However, due to the presence of undissolved Nb particles during the deposition process, an additional heat treatment was necessary. The observed changes in mechanical properties were explained in relation to the phase constituents and deformation mechanisms. Due to the elevated oxygen content in the investigated materials (2 at.%), the specific deformation mechanisms were observed at lower Nb content in comparison to the conventionally fabricated materials. This made it possible to conclude that oxygen increases the stability of the β phase in β–Ti alloys. For the first time, superelasticity was observed in Ti–Nb-based alloys fabricated by the additive manufacturing method. The highest recoverable strain of 3% was observed in Ti–19Nb alloy as a result of high elasticity and reverse martensitic transformation stress-induced during the loading.

Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 603
Author(s):  
Natalia Rońda ◽  
Krzysztof Grzelak ◽  
Marek Polański ◽  
Julita Dworecka-Wójcik

This work investigates the effect of layer thickness on the microstructure and mechanical properties of M300 maraging steel produced by Laser Engineered Net Shaping (LENS®) technique. The microstructure was characterized using light microscopy (LM) and scanning electron microscopy (SEM). The mechanical properties were characterized by tensile tests and microhardness measurements. The porosity and mechanical properties were found to be highly dependent on the layer thickness. Increasing the layer thickness increased the porosity of the manufactured parts while degrading their mechanical properties. Moreover, etched samples revealed a fine cellular dendritic microstructure; decreasing the layer thickness caused the microstructure to become fine-grained. Tests showed that for samples manufactured with the chosen laser power, a layer thickness of more than 0.75 mm is too high to maintain the structural integrity of the deposited material.


Author(s):  
Fuda Ning ◽  
Yingbin Hu ◽  
Zhichao Liu ◽  
Xinlin Wang ◽  
Yuzhou Li ◽  
...  

Laser engineered net shaping (LENS) has become a promising technology in direct manufacturing or repairing of high-performance metal parts. Investigations on LENS manufacturing of Inconel 718 (IN718) parts have been conducted for potential applications in the aircraft turbine component manufacturing or repairing. Fabrication defects, such as pores and heterogeneous microstructures, are inevitably induced in the parts, affecting part qualities and mechanical properties. Therefore, it is necessary to investigate a high-efficiency LENS process for the high-quality IN718 part fabrication. Ultrasonic vibration has been implemented into various melting material solidification processes for part performance improvements. However, there is a lack of studies on the utilization of ultrasonic vibration in LENS process for IN718 part manufacturing. In this paper, ultrasonic vibration-assisted (UV-A) LENS process is, thus, proposed to fabricate IN718 parts for the potential reduction of fabrication defects. Experimental investigations are conducted to study the effects of ultrasonic vibration on microstructures and mechanical properties of LENS-fabricated parts under two levels of laser power. The results showed that ultrasonic vibration could reduce the mean porosity to 0.1%, refine the microstructure with an average grain size of 5 μm, and fragment the detrimental Laves precipitated phase into small particles in a uniform distribution, thus enhancing yield strength, ultimate tensile strength (UTS), microhardness, and wear resistance of the fabricated IN718 parts.


2018 ◽  
Vol 20 (4) ◽  
pp. 1701043 ◽  
Author(s):  
Guohui Zhang ◽  
Shuai Yan ◽  
Fangyong Niu ◽  
Guangyi Ma ◽  
Dongjiang Wu ◽  
...  

2007 ◽  
Vol 539-543 ◽  
pp. 647-652 ◽  
Author(s):  
Han Sol Kim ◽  
Won Yong Kim

Microstructures and mechanical properties including elastic modulus were investigated in terms of ternary alloying elements Si addition, Nb content variations and tensile test. Martensite structure with α'(hcp) or α"(orthorhombic) was observed in Ti-xNb-1.5at.%Si, where x=10-20at.%. The crystal structure of martensite formed from water quenching process was largely dependent upon Nb content but does not on Si content. On the basis of experimental results obtained, it is suggested that Si has an effective role to suppress the precipitation of ω phase leading to reduction in elastic modulus in the metastable β phase region. Metastable β phase region was superior to reduce the elastic modulus than stable β phase region in the present alloy system. The minimum value of elastic modulus was measured to 48GPa. We have found that stress-induced martensitic transformation takes place during the deformation in the present alloys. Within the alloys having β(bcc) phase studied Nb-poor region appeared to exhibit a dominant behavior for stress-induced martensitic transformation than Nb-rich region. This result suggests that metastable β phase is superior to stable β phase for the occurrence of stress-induced martensitic transformation in the present alloy system.


2019 ◽  
Vol 946 ◽  
pp. 287-292
Author(s):  
Alexander Thoemmes ◽  
Ivan V. Ivanov ◽  
Alexey Ruktuev

The effect of Nb content on microstructure, mechanical properties and phase formation in as-melt and annealed binary Ti-Nb alloys were investigated using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD) analysis. The content of Nb varied in the range 25-35 mass % leading to significant changes in the microstructure. The annealed and furnace-cooled binary Ti-Nb samples exhibited HCP martensitic α` phase at a Nb content below 27.5 mass % and metastable BCC β phase at higher contents of Nb. The mechanical properties of alloys depended strongly on the Nb content and type of the dominating phase.


2018 ◽  
Vol 769 ◽  
pp. 29-34 ◽  
Author(s):  
Alexander Thoemmes ◽  
Ivan V. Ivanov ◽  
Adelya A. Kashimbetova

The effect of Nb content on microstructure, mechanical properties and phase formation in annealed and quenched binary Ti-Nb alloys were investigated using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD) analysis. The content of Nb varied in the range 0-37 mass % leading to significant changes in the microstructure. The annealed and furnace-cooled binary Ti-Nb samples exhibited HCP martensitic α` phase at a Nb content below 14 mass % and stable BCC β phase at higher contents of Nb. The structure of the quenched samples changed with increase of Nb content in the following order: coarse primary martensite → fine acicular (α`+α``) martensite → single β phase structure. The mechanical properties of alloys strongly depended on the Nb content and type of the dominating phase.


Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7302
Author(s):  
Izabela Barwinska ◽  
Mateusz Kopec ◽  
Magdalena Łazińska ◽  
Adam Brodecki ◽  
Tomasz Durejko ◽  
...  

In this paper, the Inconel 625 laser clads characterized by microstructural homogeneity due to the application of the Laser Engineered Net Shaping (LENS, Optomec, Albuquerque, NM, USA) technology were studied in detail. The optimized LENS process parameters (laser power of 550 W, powder flow rate of 19.9 g/min, and heating of the substrate to 300 °C) enabled to deposit defect-free laser cladding. Additionally, the laser clad was applied in at least three layers on the repairing place. The deposited laser clads were characterized by slightly higher mechanical properties in comparison to the Inconel 625 substrate material. Microscopic observations and X-ray Tomography (XRT, Nikon Corporation, Tokyo, Japan) confirmed, that the substrate and cladding interface zone exhibited a defect-free structure. Mechanical properties and flexural strength of the laser cladding were examined using microhardness and three-point bending tests. It was concluded, that the LENS technology could be successfully applied for the repair since a similar strain distribution was found after Digital Image Correlation measurements during three-point bending tests.


Sign in / Sign up

Export Citation Format

Share Document