scholarly journals Biotribology of Synovial Cartilage: A New Method for Visualization of Lubricating Film and Simultaneous Measurement of the Friction Coefficient

Materials ◽  
2020 ◽  
Vol 13 (9) ◽  
pp. 2075
Author(s):  
Pavel Čípek ◽  
Martin Vrbka ◽  
David Rebenda ◽  
David Nečas ◽  
Ivan Křupka

A healthy natural synovial joint is very important for painless active movement of the natural musculoskeletal system. The right functioning of natural synovial joints ensures well lubricated contact surfaces with a very low friction coefficient and wear of cartilage tissue. The present paper deals with a new method for visualization of lubricating film with simultaneous measurements of the friction coefficient. This can contribute to better understanding of lubricating film formation in a natural synovial joint. A newly developed device, a reciprocating tribometer, is used to allow for simultaneous measurement of friction forces with contact visualization by fluorescence microscopy. The software allowing for snaps processing and subsequent evaluation of fluorescence records is developed. The evaluation software and the follow-up evaluation procedure are also described. The experiments with cartilage samples and model synovial fluid are carried out, and the new software is applied to provide their evaluation. The primary results explaining a connection between lubrication and friction are presented. The results show a more significant impact of albumin proteins on the lubrication process, whereas its clusters create a more stable lubrication layer. A decreasing trend of protein cluster count, which corresponds to a decrease in the thickness of the lubrication film, is found in all experiments. The results highlight a deeper connection between the cartilage friction and the lubrication film formation, which allows for better understanding of the cartilage lubrication mechanism.

Nanomaterials ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 2126
Author(s):  
Yanjie Chen ◽  
Enzhu Hu ◽  
Hua Zhong ◽  
Jianping Wang ◽  
Ayush Subedi ◽  
...  

Graphene has been widely used as a lubricating additive to reduce the energy consumption of engines and improve fuel economy because of its unique crystal structure. Herein, graphene (GR) and fluorinated graphene (F-GR) nanoparticles were prepared by ball milling and liquid-phase exfoliation. The SEM/EDS, HRTEM, XPS, Raman spectrometer, X-ray spectrometer, FTIR were used to investigate the morphologies, surface groups, and crystal structure of two kinds of graphene materials. The influence of loads on the tribological properties of two kinds of particles was investigated in Poly Alpha Olefin (PAO6) using a UMT-2 reciprocating tribometer. Results showed that the crystal structure of GR is better than F-GR. F-GR can improve the lubrication performance of PAO6. For PAO6 containing 1 wt% F-GR at 10 N, the average friction coefficient and average wear rate decreased by 12.3% and 87% relative to pure PAO6, respectively. However, the high load resulted in an inconspicuous anti-wear and anti-friction effect. The influence of F-GR on the tribological behavior of PAO6 was more substantial than that of GR. The friction and wear mechanisms attributed to F-GR quickly entered the interface between the friction pairs. Friction-induced F-GR nanosheets mainly took the tribo-chemical reactions to participate in the lubrication film formation and helped achieve a low friction coefficient and wear rate.


Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 773
Author(s):  
Elisabet Benedicto ◽  
Eva María Rubio ◽  
Laurent Aubouy ◽  
María Ana Sáenz-Nuño

The machinability of titanium alloys still represents a demanding challenge and the development of new clean technologies to lubricate and cool is greatly needed. As a sustainable alternative to mineral oil, esters have shown excellent performance during machining. Herein, the aim of this work is to investigate the influence of esters’ molecular structure in oil-in-water emulsions and their interaction with the surface to form a lubricating film, thus improving the efficiency of the cutting fluid. The lubricity performance and tool wear protection are studied through film formation analysis and the tapping process on Ti6Al4V. The results show that the lubricity performance is improved by increasing the formation of the organic film on the metal surface, which depends on the ester’s molecular structure and its ability to adsorb on the surface against other surface-active compounds. Among the cutting fluids, noteworthy results are obtained using trimethylolpropane trioleate, which increases the lubricating film formation (containing 62% ester), thus improving the lubricity by up to 12% and reducing the torque increase due to tool wear by 26.8%. This work could be very useful for fields where often use difficult-to-machine materials—such as Ti6Al4V or γ-TiAl – which require large amounts of cutting fluids, since the formulation developed will allow the processes to be more efficient and sustainable.


Lubricants ◽  
2020 ◽  
Vol 8 (5) ◽  
pp. 54
Author(s):  
Valdicleide Silva Mello ◽  
Marinalva Ferreira Trajano ◽  
Ana Emilia Diniz Silva Guedes ◽  
Salete Martins Alves

Additives are essential in lubricant development, improving their performance by the formation of a protective film, thus reducing friction and wear. Some such additives are extreme pressure additives. However, due to environmental issues, their use has been questioned because their composition includes sulfur, chlorine, and phosphorus. Nanoparticles have been demonstrated to be a suitable substitute for those additives. This paper aims to make a comparison of the tribological performance of conventional EP additives and oxides nanoparticles (copper and zinc) under boundary lubrication conditions. The additives (nanoparticles, ZDDP, and sulfur) were added to mineral and synthetic oils. The lubricant tribological properties were analyzed in the tribometer HFRR (high frequency reciprocating rig), and during the test, the friction coefficient and percentual of film formation were measured. The wear was analyzed by scanning electron microscopy. The results showed that the conventional EP additives have a good performance owing to their anti-wear and small friction coefficient in both lubricant bases. The oxides nanoparticles, when used as additives, can reduce the friction more effectively than conventional additives, and displayed similar behavior to the extreme pressure additives. Thus, the oxide nanoparticles are more environmentally suitable, and they can replace EP additives adapting the lubricant to current environmental requirements.


2016 ◽  
Vol 87 (12) ◽  
pp. 124901 ◽  
Author(s):  
Xu He ◽  
Junyou Yang ◽  
Qinghui Jiang ◽  
Yubo Luo ◽  
Dan Zhang ◽  
...  

2013 ◽  
Vol 683 ◽  
pp. 90-93 ◽  
Author(s):  
Koshiro Mizobe ◽  
Takashi Honda ◽  
Hitonobu Koike ◽  
Edson Costa Santos ◽  
Yuji Kashima ◽  
...  

Polyetheretherketone (PEEK) is a tough semi-crystalline thermoplastic polymer with excellent mechanical properties. While abilities of polyphenylenesulfide (PPS) are similar to PEEK, former material cost was lower than later. Polytetrafluoroethylene (PTFE) is well known because of its low friction coefficient and self lubrication ability. The objective of this study is to observe the friction coefficient of hybrid bearings, PTFE retainer sandwiched with PPS-races or PEEK-races. Rolling contact fatigue tests were performed and in situ friction forces wear measured. It is concluded that the PTFE retainer reduced friction coefficient.


2021 ◽  
Author(s):  
Weiping Lin ◽  
Zhengmeng Yang ◽  
Liu Shi ◽  
Haixing Wang ◽  
Qi Pan ◽  
...  

Abstract Background: Osteoarthritis (OA) is a chronic joint disease, characterized by articular cartilage degradation, subchondral bone hardening, and inflammation of the whole synovial joint. There is no pharmacological treatment in slowing down OA progression, leading to costly surgical interventions eventually. Cell therapy using chondrocytes or progenitor cells from different sources has been reported in clinical trials for OA management with some success, but outcomes are varied. Peripheral blood derived mesenchymal stem cells (PB-MSCs) are promising cells owing to their easy collection, superior migration, and differentiation potentials. In the current study, we evaluated the effect of intra-articular administration of PB-MSCs on the progression of OA in mice.Methods: C57BL/6J mice (8-10 weeks old male) were subjected to destabilization of the medial meniscus surgeries (DMM) on their right joints following protocols as previously reported. The mice after DMM were randomly treated with saline (vehicle control), PB-MSCs, or adipose tissue derived MSCs (AD-MSCs) (n = 7 per group). The mice treated with sham surgery were regarded as sham controls (n = 7). PB-MSCs and AD-MSCs were harvested and cultured according to previous published protocols, and pre-labeled with BrdU for 48 h before use. PB-MSCs or AD-MSCs (5 × 105 cells/mouse; passage 3~5) were injected into the right knee joints thrice post-surgery (except sham surgery group). The mice were euthanized at 8 weeks post-surgery and knee joint samples were collected for micro-CT and histological examinations.Results: PB-MSCs administration significantly reduced hardening of subchondral bone comparing to vehicle controls. Safranin O staining showed that PB-MSCs treatment ameliorated degeneration of articular cartilage, which is comparable to AD-MSCs treatment. The expression of catabolic marker MMP13 was significantly reduced in articular cartilage of PB-MSCs-treated groups comparing to vehicle controls. Co-expression of BrdU and Sox9 were detected, indicating injected PB-MSCs differentiated towards chondrocytes in situ. Reduced level of IL-6 in the peripheral sera of PB-MSCs- and AD-MSCs-treated mice was also determined. Conclusions: Repetitive administration of PB-MSCs or AD-MSCs halted OA progression through inhibiting cartilage degradation and inflammation. PB-MSCs may become a promising cell source for cartilage tissue repair and alleviation of OA progression.


Author(s):  
Jin-Jang Liou ◽  
Grodrue Huang ◽  
Wensyang Hsu

Abstract A variable pressure damper (VPD) is used here to adjusted the friction force on the valve spring to investigate the relation between the friction force and the valve bouncing phenomenon. The friction force on the valve spring is found experimentally, and the corresponding friction coefficient is also determined. Dynamic valve displacements at different speeds with different friction forces are calibrated. Bouncing and floating of the valve are observed when the camshaft reaches high speed. From the measured valve displacement, the VPD is shown to have significant improvement in reducing valve bouncing distance and eliminating floating. However, experimental results indicate that the valve bouncing can not be eliminated completely when the camshaft speed is at 2985 rpm.


2009 ◽  
pp. 84-85
Author(s):  
I. Křupka ◽  
R. Poliščuk ◽  
M. Vaverka ◽  
M. Hartl ◽  
M. Vrbka ◽  
...  

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