scholarly journals Hot Deformation Behaviors of the Mg-3Sn-2Al-1Zn Alloy: Investigation on its Constitutive Equation, Processing Map, and Microstructure

Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 312 ◽  
Author(s):  
Yuhang Guo ◽  
Yaodong Xuanyuan ◽  
Xuannam Ly ◽  
Sen Yang
Keyword(s):  
Constitutive Equation ◽  
Strain Rate ◽  
Processing Map ◽  
True Strain ◽  
Strain Rate Range ◽  
Hot Working ◽  
Microstructure Observation ◽  
Stability And Instability ◽  
Deformation Behaviors ◽  
Working Parameters

In this work, the Mg-3Sn-2Al-1Zn (TAZ321, wt. %) alloy with excellent high temperature resistance was compressed using a Gleeble-3500 thermo-mechanical simulator at a wide temperature and the strain rate range. The kinetics analyses showed that the dominant deformation mechanism was likely caused by the cross slipping of dislocations. A constitutive equation which expressed the relationship between the flow stress, deformation temperature, and strain rate was established, and the average activation energy Q was calculated to be 172.1 kJ/mol. In order to delineate the stability and instability working domains, as well as obtain the optimum hot working parameters of the alloy, the hot processing maps in accordance with Prassad’s criterion are constructed at the true strain of 0.2, 0.4, 0.6, and 0.8, respectively. Based on the hot processing map and microstructure observation, the optimum hot working parameter was determined to be 350 °C/1 s−1. The continuous fine dynamic recrystallization (CDRX) grains occurred in the optimum deformation zone. The predicted instability domains was identified as T = 200–300 °C, ε ˙ = 10−2–1 s−1, which corresponded to the microstructure of deformation twinning and micro cracks at the intersection of grain boundaries.

scholarly journals Constitutive Equation and Hot Processing Map of a Nitrogen-Bearing Martensitic Stainless Steel

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1502
Author(s):  
Xiao Li ◽  
Lifeng Hou ◽  
Yinghui Wei ◽  
Zhengyan Wei
Keyword(s):  
Stainless Steel ◽  
Constitutive Equation ◽  
Strain Rate ◽  
Hot Deformation ◽  
Processing Map ◽  
Martensitic Stainless Steel ◽  
True Strain ◽  
True Stress ◽  
Hot Working ◽  
Compression Tests

The hot deformation behavior of a nitrogen-bearing martensitic stainless steel was researched by the isothermal compression test in the temperature range of 950–1150 °C and strain rate range of 0.01–10 s−1 with a Gleeble-3800 thermal-mechanical simulating tester. A strain compensated sine-hyperbolic Arrhenius-type constitutive equation was developed to describe the relationship between true stress and deformation parameters such as temperature, strain rate and true strain. The hot deformation activation energy is calculated to be from 407 to 487 KJ mol−1. It is validated by the standard statistical parameters that the established constitutive equation can accurately predict the true stress. The processing maps at different true strains were constructed based on the dynamic material model (DMM) and the true stress data obtained from the hot compression tests. Two unstable regions which should be avoided during hot working were observed from the processing map. In addition, the optimum hot working parameters are located in the domain of 1000–1150 °C/0.1–1 s−1 with the peak power dissipation efficiency of 39.9%, in which complete dynamic recrystallization (DRX) occurs.

Deformation Behavior and Processing Map of High Temperature of TC21 Titanium Alloy

2013 ◽  
Vol 274 ◽  
pp. 427-431 ◽  
Author(s):  
Ying Gong
Keyword(s):  
Titanium Alloy ◽  
Flow Stress ◽  
Strain Rate ◽  
Deformation Behavior ◽  
Processing Map ◽  
True Strain ◽  
Strain Rate Range ◽  
Peak Region ◽  
Working Zone ◽  
Dynamic Materials

The compression test on TC21 titanium alloy was carried out in the temperature range of 860~940oC and the strain rate range of 0.01~10s-1 on Gleeble-1500D hot simulation machine. And the hot deformation behavior was studied. The processing map was calculated and analyzed according the dynamic materials model. It is found that the flow stress of TC21 decreases with the increasing of the temperature and the decreasing of the strain rate. The flow stress curves are characterized by steady state at low strain rate( s-1）but discontinuous yield at high strain rate( s-1). The processing map established at the true strain of 0.4 shows that there are three regions, instability and safe and peak region, and the efficiencies of power dissipation are 0~25%，31%~37% and 43%~49% respectively. The peak region is the optimum hot working zone of TC21 titanium alloy.

scholarly journals Determination of Constitutive Equation and Thermo–Mechanical Processing Map for Pure Iridium

Metals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 1087
Author(s):  
Mi Zhou ◽  
Rui Hu ◽  
Jieren Yang ◽  
Chuanjun Wang ◽  
Ming Wen
Keyword(s):  
Constitutive Equation ◽  
Strain Rate ◽  
Processing Map ◽  
Frictional Coefficient ◽  
Strain Curve ◽  
Strain Rate Range ◽  
Forming Process ◽  
Thermal Compression ◽  
Rate Range ◽  
Temperature Range

Deformation behavior of pure iridium has been studied during thermal compression testing with the help of Gleeble-1500D in the temperature range of 1200 °C~1500 °C and strain rate range of 10−1 s−1~10−2 s−1. Resistance to deformation, microstructural evolution and hot workability of pure iridium have been used to analyze in detail. Frictional coefficient has been used to modify the experimental stress–strain curve of thermal compression test, and it has been found effective in reducing the influence of friction during thermo–mechanical testing. The hyperbolic sine constitutive equation of pure iridium has been established to give a material processing model for numerical simulation. A very high value of activation energy for iridium, 573 KJ/mol, clearly indicates that it is very hard to deform this material. The deformation mechanism of pure iridium is dependent upon temperature as well as strain rate. At low temperature and strain rate (temperature range of 1200 °C~1300 °C and strain rate range of 10−1 s−1~10−2 s−1), dynamic recovery is active while dynamic recrystallization becomes operative as temperature and stain rate are increased. On further increase in temperature and decrease in strain rate (temperature range of 1400 °C~1500 °C and strain rates of 10−2 s−1~10−3 s−1), abnormal grain growth takes place. On the basis of a constitutive model and processing map, suitable forming process parameters (temperature range of 1400 °C~1500 °C and strain rate range of 0.1 s−1~0.05 s−1) for pure iridium have been worked out.

Characterization of the Hot Deformation Behavior of a Al-Si Alloy Using Processing Maps

2013 ◽  
Vol 873 ◽  
pp. 3-9 ◽  
Author(s):  
Ming Liang Wang ◽  
Pei Peng Jin ◽  
Jin Hui Wang ◽  
Li Han
Keyword(s):  
Strain Rate ◽  
Processing Map ◽  
Shear Bands ◽  
Solution Treatment ◽  
Strain Rate Range ◽  
Hot Working ◽  
Compression Tests ◽  
Optimum Parameters ◽  
Flow Stress Data

The compression tests of solution treatment ZL109 alloy have been performed in the compression temperature range from 250°C to 450°C and the strain rate range from 0.0005s-1to 0.5s-1. A processing map has been developed on the basis of flow stress data obtained as a function of temperature and strain rate, which revealed two domains of hot working for the alloy: one is situated at temperature between 270°C and 340°C with strain rate between 0.05s-1and 0.5s-1, the other is situated at the temperature between 380°C and 450°C with strain rate between 0.0005s-1and 0.004s-1. Combining with the processing map, the optimum parameters of hot working for ZL109 alloy are that 300°C/0.5s-1and 450°C/0.0005s-1, respectively. Microstructure observations indicated that DRX occurred in both these domains. The instable zones, i. e., adiabatic shear bands formation, wedge cracking, were also identified in the processing map and microstructural examination was performed for validation.

scholarly journals Hot Deformation Behaviour and Processing Map of Cast Alloy 825

2021 ◽  
Author(s):  
Munir Al-Saadi ◽  
Christopher Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson
Keyword(s):  
Strain Rate ◽  
Vickers Hardness ◽  
Power Dissipation ◽  
Hot Deformation ◽  
Processing Map ◽  
Cast Alloy ◽  
True Strain ◽  
Processing Conditions ◽  
Temperature Range ◽  
Power Dissipation Efficiency

AbstractAlloy 825 is a nickel-based alloy that is commonly used in applications where both high strength and corrosion resistance are required, such as tanks in the chemical, food and petrochemical industries and oil and gas pipelines. Components made from Alloy 825 are often manufactured using hot deformation. However, there is no systematic study to optimise the processing conditions reported in literature. In this study, a processing map for as-cast Alloy 825 is established to maximise the power dissipation efficiency of hot deformation in the temperature range of 950 to 1250 °C at an interval of 50 °C and strain rate range of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 to $$10.0\, {\text{s}}^{ - 1}$$ 10.0 s - 1 to a true strain of $$0.7$$ 0.7 using a Gleeble-3500 thermomechanical simulator. The processing conditions are also correlated to the Vickers hardness of the final material, which is also characterised using optical microscopy and scanning electron microscopy, including electron backscattered diffraction. The true stress-true strain curves exhibit peak stresses followed by softening due to occurrence of dynamic recrystallization. The activation energy for plastic flow in the temperature range tested is approximately $$450\,{\text{ kJ mol}}^{ - 1}$$ 450 kJ mol - 1 , and the value of the stress exponent in the (hyperbolic sine-based) constitutive equation, $$n = 5.0$$ n = 5.0 , suggests that the rate-limiting mechanism of deformation is dislocation climb. Increasing deformation temperature led to a lower Vickers hardness in the deformed material, due to increased dynamic recrystallization. Raising the strain rate led to an increase in Vickers hardness in the deformed material due to increased work hardening. The maximum power dissipation efficiency is over $$35\%$$ 35 % , obtained for deformation in the temperature range 1100-1250 °C and a strain rate of $$0.01\, {\text{s}}^{ - 1}$$ 0.01 s - 1 -$$0.1\, {\text{s}}^{ - 1}$$ 0.1 s - 1 . These are the optimum conditions for hot working.

The Optimal Selection of Extrusion Parameters of As-Cast TC27 Titanium Alloy Based on Processing-Map

2017 ◽  
Vol 898 ◽  
pp. 1134-1139
Author(s):  
Xue Fei Li ◽  
Ai Xue Sha ◽  
Xu Huang ◽  
Li Jun Huang
Keyword(s):  
Titanium Alloy ◽  
Flow Stress ◽  
Strain Rate ◽  
Processing Map ◽  
True Strain ◽  
Great Influence ◽  
Stable Condition ◽  
Dynamic Materials ◽  
Dynamic Materials Model ◽  
Selection Of

The hot deformation behavior of TC27 titanium alloy at the temperatures of 900-1150 °C and the strain rate of 0.01-10 s-1, the height reduction of 70%, was investigated in the isothermal compression test to identify the optimal extrusion parameters. The processing-map of TC27 titanium alloy was constructed based on dynamic materials model (DMM) and principle of Prasad*s instability. The conclusion shows that temperature and strain rate of deformation had a great influence on flow stress. At the beginning of deformation, the flow stress increased quickly with the augment of true strain and decreased slowly after flow stress reaching to the maximum value. Finally, flow stress tended to relatively stable condition. The flow stress decreased with the increase of temperature and increased with the increase of strain rate. The TC27 titanium alloy was sensitive to temperature and strain rate. Processing-map exhibited two peak efficiencies of power dissipation; one peak was 49% at 900°C/0.01 s-1, which dynamic recovery occured. The other peak was also 49% at 1050 °C /0.01s-1, which dynamic recrystallization occured in the domain. Besides, there were two instability areas in the processing-map which should be avoided during the extrusion. Therefore, in order to obtain the satisfactory properties, the parameters that 1050 °C and 0.01 s-1 were selected in the extrusion.

Characterization of Hot Deformation Behavior of Udimet720Li Superalloy Using Processing Map

2014 ◽  
Vol 887-888 ◽  
pp. 1161-1168
Author(s):  
Jian Guo Wang ◽  
Dong Liu ◽  
Tao Wang ◽  
Yan Hui Yang
Keyword(s):  
Strain Rate ◽  
Deformation Behavior ◽  
High Strain ◽  
Flow Behavior ◽  
Strain Range ◽  
Peak Stress ◽  
Strain Rate Range ◽  
Hot Working ◽  
Compression Tests ◽  
Hollomon Parameter

The deformation behavior of a Udimet720Li superalloy under hot compression tests was characterized in the temperature range of 1060~1160°C and strain rate range of 0.001~20s-1. Processing maps were conducted at a series of strains to calculate the efficiency of hot working and to recognize the instability regions of the flow behavior. A Zener-Hollomon parameter is given to characterize the dependence of peak stress on temperature and strain rate. The efficiency of power dissipation of the Udimet720Li superalloy obtained in a strain range of 0.1~0.7 are essentially similar, which indicates that strain does not have a significant influence and the instability region shown in high strain and high strain rates at all temperatures. The regions for the full recrystallization can be divided by the dissolution beginning temperature of primary γ'which are the optimum hot working parameters.

Hot Deformation Behaviors of SiCp/Al Composites

2014 ◽  
Vol 1058 ◽  
pp. 165-169 ◽  
Author(s):  
Shi Ming Hao ◽  
Jing Pei Xie
Keyword(s):  
Flow Stress ◽  
Strain Rate ◽  
Hot Deformation ◽  
True Strain ◽  
Constant Strain Rate ◽  
Hot Compression ◽  
Compression Tests ◽  
Sensitive Material ◽  
2024 Aluminum Alloy ◽  
Deformation Behaviors

The hot deformation behaviors of 30%SiCp/2024 aluminum alloy composites was studied by hot compression tests using Gleeble-1500 thermomechanical simulator at temperatures ranging from 350-500°C under strain rates of 0.01-10 s-1. The true stress-true strain curves were obtained in the tests. Constitutive equation and processing map were established. The results show that the flow stress decreases with the increase of deformation temperature at a constant strain rate, and increases with the increase of strain rate at constant temperature, indicating that composite is a positive strain rate sensitive material. The flow stress behavior of composite during hot compression deformation can be represented by a Zener-Hollomon parameter in the hyperbolic sine form. Its activation energy for hot deformation Q is 183.251 kJ/mol. The optimum hot working conditions for this material are suggested.

High Temperature Deformation Mechanisms and Processing Map for Hot Working of Cast-Homogenized Mg-3Sn-2Ca Alloy

2010 ◽  
Vol 638-642 ◽  
pp. 3616-3621 ◽  
Author(s):  
K.P. Rao ◽  
Y.V.R.K. Prasad ◽  
Norbert Hort ◽  
Karl Ulrich Kainer
Keyword(s):  
Strain Rate ◽  
Processing Map ◽  
Volume Fraction ◽  
Flow Instability ◽  
Back Stress ◽  
Hot Working ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Strain Rates ◽  
Compression Tests

The hot working behavior of Mg-3Sn-2Ca alloy has been investigated in the temperature range 300–500 oC and strain rate range 0.0003–10 s-1, with a view to evaluate the mechanisms and optimum parameters of hot working. For this purpose, a processing map has been developed on the basis of the flow stress data obtained from compression tests. The stress-strain curves exhibited steady state behavior at strain rates lower than 0.01 s-1 and at temperatures higher than 350 oC and flow softening occurred at higher strain rates. The processing map exhibited two dynamic recrystallization domains in the temperature and strain rate ranges: (1) 300–420 oC and 0.0003–0.003 s-1, and (2) 420–500 oC and 0.003–1.0 s-1, the latter one being useful for commercial hot working. Kinetic analysis yielded apparent activation energy values of 161 and 175 kJ/mole in domains (1) and (2) respectively. These values are higher than that for self-diffusion in magnesium suggesting that the large volume fraction of intermetallic particles CaMgSn present in the matrix generates considerable back stress. The processing map reveals a wide regime of flow instability which gets reduced with increase in temperature or decrease in strain rate.

Hot Deformation Behaviors and Microstructure Evolution of SiCp/Al Composites

2016 ◽  
Vol 849 ◽  
pp. 430-435 ◽  
Author(s):  
Shi Ming Hao ◽  
Jing Pei Xie ◽  
Li Ben Li ◽  
Ai Qin Wang ◽  
Wen Yan Wang ◽  
...  
Keyword(s):  
Strain Rate ◽  
Structural Changes ◽  
True Strain ◽  
Peak Stress ◽  
Small Strain ◽  
Sensitive Material ◽  
Aluminium Matrix Composite ◽  
Compression Behavior ◽  
High Deformation ◽  
Deformation Behaviors

In order to explore the compressive properties of aluminium matrix composite reinforced with middle content SiC particles, hot compression behavior of 30%SiCp/2024A1 composite was investigated using Gleeble-1500 system at a temperatures range from 350 to 500°C and strain rates from 0.01 to 10 s−1. The associated structural changes were studied by OM, SEM and TEM observations. The results show that the true stress–true strain curves exhibited a peak stress at a small strain (<0.1), after which the flow stresses decreased monotonically until high strains, showing a dynamic flow softening. The stress level decreased with increasing deformation temperature and decreasing strain rate, indicating that the composite is a positive strain rate sensitive material. And therefore there will be a enough time for dynamic recrystallization to complete nucleation and growth at low strain rate and high deformation temperatures.

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