scholarly journals Influence of Melt-Pool Stability in 3D Printing of NdFeB Magnets on Density and Magnetic Properties

Materials ◽  
2019 ◽  
Vol 13 (1) ◽  
pp. 139 ◽  
Author(s):  
Mateusz Skalon ◽  
Michael Görtler ◽  
Benjamin Meier ◽  
Siegfried Arneitz ◽  
Nikolaus Urban ◽  
...  

The current work presents the results of an investigation focused on the influence of process parameters on the melt-track stability and its consequence to the sample density printed out of NdFeB powder. Commercially available powder of Nd7.5Pr0.7Fe75.4Co2.5B8.8Zr2.6Ti2.5 alloy was investigated at the angle of application in selective laser melting of permanent magnets. Using single track printing the stability of the melt pool was investigated under changing process parameters. The influence of changing laser power, scanning speed, and powder layer thickness on density, porosity structure, microstructure, phase composition, and magnetic properties were investigated. The results showed that energy density coupled with powder layer thickness plays a crucial role in melt-track stability. It was possible to manufacture magnets of both high relative density and high magnetic properties. Magnetization tests showed a significant correlation between the shape of the demagnetization curve and the layer height. While small layer heights are beneficial for sufficient magnetic properties, the remaining main parameters tend to affect the magnetic properties less. A quasi-linear correlation between the layer height and the magnetic properties remanence (Jr), coercivity (HcJ) and maximum energy product ((BH)max) was found.

2010 ◽  
Vol 43 ◽  
pp. 578-582 ◽  
Author(s):  
C.Y. Wang ◽  
Q. Dong ◽  
X.X. Shen

Warpage is a crucial factor to accuracy of sintering part in selective laser sintering (SLS) process. In this paper, The influence of process parameters on warpage when sintering polystyrene(PS) materials in SLS are investigated. The laser power, scanning speed, hatch spacing, layer thickness as well as temperature of powder are considered as the main process parameters. The results showed that warpage increases with the increase of hatch space. Contary to it, warpage decreases with the increase of laser power. Warpage decreases with the increase of layer thickness between 0.16~0.18mm and changes little with increase of the thickness. Warpage increases along with the increase of scanning speed but decreases when the speed is over about 2000mm/s. When the temperature changes between 82°C-86°C, warpage decreases little with the increase of temperature. But further increase of temperature leads to warpage decreasing sharply when the temperature changes between 86°C-90°C.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 876 ◽  
Author(s):  
Sapam Ningthemba Singh ◽  
Sohini Chowdhury ◽  
Yadaiah Nirsanametla ◽  
Anil Kumar Deepati ◽  
Chander Prakash ◽  
...  

Investigation of the selective laser melting (SLM) process, using finite element method, to understand the influences of laser power and scanning speed on the heat flow and melt-pool dimensions is a challenging task. Most of the existing studies are focused on the study of thin layer thickness and comparative study of same materials under different manufacturing conditions. The present work is focused on comparative analysis of thermal cycles and complex melt-pool behavior of a high layer thickness multi-layer laser additive manufacturing (LAM) of pure Titanium (Ti) and Inconel 718. A transient 3D finite-element model is developed to perform a quantitative comparative study on two materials to examine the temperature distribution and disparities in melt-pool behaviours under similar processing conditions. It is observed that the layers are properly melted and sintered for the considered process parameters. The temperature and melt-pool increases as laser power move in the same layer and when new layers are added. The same is observed when the laser power increases, and opposite is observed for increasing scanning speed while keeping other parameters constant. It is also found that Inconel 718 alloy has a higher maximum temperature than Ti material for the same process parameter and hence higher melt-pool dimensions.


Micromachines ◽  
2021 ◽  
Vol 12 (5) ◽  
pp. 538
Author(s):  
Dagmar Goll ◽  
Felix Trauter ◽  
Timo Bernthaler ◽  
Jochen Schanz ◽  
Harald Riegel ◽  
...  

Lab scale additive manufacturing of Fe-Nd-B based powders was performed to realize bulk nanocrystalline Fe-Nd-B based permanent magnets. For fabrication a special inert gas process chamber for laser powder bed fusion was used. Inspired by the nanocrystalline ribbon structures, well-known from melt-spinning, the concept was successfully transferred to the additive manufactured parts. For example, for Nd16.5-Pr1.5-Zr2.6-Ti2.5-Co2.2-Fe65.9-B8.8 (excess rare earth (RE) = Nd, Pr; the amount of additives was chosen following Magnequench (MQ) powder composition) a maximum coercivity of µ0Hc = 1.16 T, remanence Jr = 0.58 T and maximum energy density of (BH)max = 62.3 kJ/m3 have been achieved. The most important prerequisite to develop nanocrystalline printed parts with good magnetic properties is to enable rapid solidification during selective laser melting. This is made possible by a shallow melt pool during laser melting. Melt pool depths as low as 20 to 40 µm have been achieved. The printed bulk nanocrystalline Fe-Nd-B based permanent magnets have the potential to realize magnets known so far as polymer bonded magnets without polymer.


2020 ◽  
Vol 26 (1) ◽  
pp. 100-106 ◽  
Author(s):  
Tobias Kolb ◽  
Reza Elahi ◽  
Jan Seeger ◽  
Mathews Soris ◽  
Christian Scheitler ◽  
...  

Purpose The purpose of this paper is to analyse the signal dependency of the camera-based coaxial monitoring system QMMeltpool 3D (Concept Laser GmbH, Lichtenfels, Germany) for laser powder bed fusion (LPBF) under the variation of process parameters, position, direction and layer thickness to determine the capability of the system. Because such and similar monitoring systems are designed and presented for quality assurance in series production, it is important to present the dominant signal influences and limitations. Design/methodology/approach Hardware of the commercially available coaxial monitoring QMMeltpool 3D is used to investigate the thermal emission of the interaction zone during LPBF. The raw images of the camera are analysed by means of image processing to bypass the software of QMMeltpool 3D and to gain a high level of signal understanding. Laser power, scan speed, laser spot diameter and powder layer thickness were varied for single-melt tracks to determine the influence of a parameter variation on the measured sensory signals. The effects of the scan direction and position were also analysed in detail. The influence of surface roughness on the detected sensory signals was simulated by a machined substrate plate. Findings Parameter variations are confirmed to be detectable. Because of strong directional and positional dependencies of the melt-pool monitoring signal a calibration algorithm is necessary. A decreasing signal is detected for increasing layer thickness. Surface roughness is identified as a dominating factor with major influence on the melt-pool monitoring signal exceeding other process flaws. Research limitations/implications This work was performed with the hardware of a commercially available QMMeltpool 3D system of an LPBF machine M2 of the company Concept Laser GmbH. The results are relevant for all melt-pool monitoring research activities connected to LPBF, as well as for end users and serial production. Originality/value Surface roughness has not yet been revealed as being one of the most important origins for signal deviations in coaxial melt-pool monitoring. To the best of the authors’ knowledge, the direct comparison of influences because of parameters and environment has not been published to this extent. The detection, evaluation and remelting of surface roughness constitute a plausible workflow for closed-loop control in LPBF.


Metals ◽  
2019 ◽  
Vol 9 (4) ◽  
pp. 456 ◽  
Author(s):  
Sazzad H. Ahmed ◽  
Ahsan Mian

Selective Laser Melting (SLM) is a popular additive manufacturing (AM) method where a laser beam selectively melts powder layer by layer based on the building geometry. The melt pool peak temperature during build process is an important parameter to determine build quality of a fabricated component by SLM process. The melt pool temperature depends on process parameters including laser power, scanning speed, and hatch space as well as the properties of the build material. In this paper, the sensitivity of melt pool peak temperature during the build process to temperature dependent material properties including density, specific heat, and thermal conductivity are investigated for a range of laser powers and laser scanning speeds. It is observed that the melt pool temperature is most sensitive to melt pool thermal conductivity of the processed material for a set of specific process parameters (e.g., laser power and scan speed). Variations in the other mechanical–physical properties of powder and melt pool such as density and specific heat are found to have minimal effect on melt pool temperature.


Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 877
Author(s):  
Cong Ma ◽  
Xianshun Wei ◽  
Biao Yan ◽  
Pengfei Yan

A single-layer three-dimensional model was created to simulate multi-channel scanning of AlSi25 powder in selective laser melting (SLM) by the finite element method. Thermal behaviors of laser power and scanning speed in the procedure of SLM AlSi25 powder were studied. With the increase of laser power, the maximum temperature, size and cooling rate of the molten pool increase, while the scanning speed decreases. For an expected SLM process, a perfect molten pool can be generated using process parameters of laser power of 180 W and a scanning speed of 200 mm/s. The pool is greater than the width of the scanning interval, the depth of the molten pool is close to scan powder layer thickness, the temperature of the molten pool is higher than the melting point temperature of the powder and the parameters of the width and depth are the highest. To confirm the accuracy of the simulation results of forecasting excellent process parameters, the SLM experiment of forming AlSi25 powder was carried out. The surface morphology of the printed sample is intact without holes and defects, and a satisfactory metallurgical bond between adjacent scanning channels and adjacent scanning layers was achieved. Therefore, the development of numerical simulation in this paper provides an effective method to obtain the best process parameters, which can be used as a choice to further improve SLM process parameters. In the future, metallographic technology can also be implemented to obtain the width-to-depth ratio of the SLM sample molten pool, enhancing the connection between experiment and theory.


2001 ◽  
Vol 674 ◽  
Author(s):  
D. Goll ◽  
W. Sigle ◽  
G.C. Hadjipanayis ◽  
H. Kronmüller

ABSTRACTThe rather complex correlation between the microstructure and the magnetic properties is demonstrated for two types of high-quality RE-TM permanent magnets (pms), namely nanocrystalline RE2Fe14B (RE = Nd,Pr) and nanostructured Sm2(Co,Cu,Fe,Zr)17 pms. The detailed analysis of this correlation for both pm materials leads to a quantitative comprehension of the hardening mechanism enabling the optimization of their magnetic properties and temperature dependences. In the case of RE2Fe14B, isotropic bonded pms are fabricated showing maximum energy products in the order of 90 kJ/m3. In the case of Sm2(Co,Cu,Fe,Zr)17, magnets with excellent high-temperature magnetic properties are tailored. Hereby, the investigations in addition provide important clues to the evolution of the characteristic microstructural and magnetic properties and to the role of the involved elements.


2021 ◽  
Vol 1206 (1) ◽  
pp. 012001
Author(s):  
Umesh Kumar Vates ◽  
Nand Jee Kanu ◽  
Eva Gupta ◽  
Gyanendra Kumar Singh ◽  
Naveen Anand Daniel ◽  
...  

Abstract Rapid prototyping (RP) uses a cycle where a real model is made by explicitly adding material as thin cross-sectional layers. Fused deposition modelling (FDM) 3D printer is being use for synthesis of ABS based bone hammer. Response surface methodology (RSM) based L27 design of experiment were adopted to perform the experiment using four influencing parameters such as layer thickness, infill percentage, orientation and nozzle temperature for the three responses deflection, hardness and weight. Response surface methodology was used for modelling and optimization of considered process parameters. In present investigation, it is evident that bone hammer fabrication process parameters have been optimized on data such as bone hammer weight 19.8091g, hardness 104.5921 BHN, and force of 15 degree deflection 36.0681 N has been produced with RSM prediction with influence of process parameters such as layer thickness 0.250 mm, infill percentage 63.3333, orientation 60 degree, nozzle temperature 240°C.


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