scholarly journals Correction: Mierzejewska, Z.A. Effect of Laser Energy Density, Internal Porosity and Heat Treatment on Mechanical Behavior of Biomedical Ti6Al4V Alloy Obtained with DMLS Technology. Materials 2019, 12, 2331

Materials ◽  
2019 ◽  
Vol 12 (18) ◽  
pp. 2928
Author(s):  
Żaneta Anna Mierzejewska
Keyword(s):  
Heat Treatment ◽  
Energy Density ◽  
Mechanical Behavior ◽  
Laser Energy ◽  
Ti6al4v Alloy ◽  
Laser Energy Density ◽  
Internal Porosity

The authors wish to make the following correction to this paper [...]

Electrical Properties of Solid Phase Crystallized Silicon Films

2001 ◽  
Vol 664 ◽  
Author(s):  
Tadashi Watanabe ◽  
Hajime Watakabe ◽  
Toshiyuki Sameshima
Keyword(s):  
Heat Treatment ◽  
Electrical Conductivity ◽  
Energy Density ◽  
Laser Irradiation ◽  
Carrier Mobility ◽  
Crystalline Silicon ◽  
Solid Phase ◽  
Laser Energy ◽  
Silicon Films ◽  
Laser Energy Density

ABSTRACTIn this study, the carrier mobility and density for solid phase crystallized (SPC) silicon films fabricated at 600 °C for 48 hours are analyzed by free carrier optical absorption. The carrier mobility is 40 cm2/Vs for SPC films doped with 6×1019-cm−3-phosphorus atoms. This analysis suggests the SPC films have fine crystalline grains closed to single crystalline silicon. In addition, initial carrier density was 3×1019 cm−3, which increased to 6×1019 cm−3by XeCl excimer laser irradiation of 500mJ/cm2. The inactivated regions in SPC films are reduced by laser irradiation. However, the electrical conductivity after laser irradiation for SPC films doped with 6×1018-cm−3-phosphorus atoms decreased from 3.3 to 0.018 S/cm as laser energy density increased to 500mJ/cm2. On the other hand, the electrical conductivity increased from 14.7 to 31.3 S/cm with similar increase of laser energy density after H2O vapor heat treatment at 260°C for 3 hours with 1.3 MPa. Furthermore, the characteristics of n-channel TFTs fabricated with initial SPC films as well as SPC films which was irradiated by laser at 425mJ/cm2 are also researched. The threshold voltage is decreased from 3.8 to 2.0 V by laser irradiation. Threshold voltages of both cases are decreased from 3.8 to 2.4 V for no-laser irradiation and from 2.0 to 0.8 V for laser irradiation, after H2O vapor heat treatment at 310°C for 1 hour with 9.0MPa. Based on the above trial, the defect reduction method combining laser irradiation and H2O vapor heat treatment has proved to be very effective for SPC films and SPC TFTs.

Microstructure and mechanical property of selective laser melted Ti6Al4V dependence on laser energy density

2017 ◽  
Vol 23 (2) ◽  
pp. 217-226 ◽  
Author(s):  
Jie Han ◽  
Jingjing Yang ◽  
Hanchen Yu ◽  
Jie Yin ◽  
Ming Gao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Energy Density ◽  
Laser Energy ◽  
Ti6al4v Alloy ◽  
Laser Energy Density ◽  
Future Application ◽  
Content Type ◽  
Processing Window ◽  
Columnar Grains ◽  
Columnar Grain

Purpose This paper aims to investigate the influence of laser energy density on microstructure and mechanical properties of the selective laser melted (SLMed) Ti6Al4V to complement the existing knowledge in additive manufacturing of Ti6Al4V for future application of selective laser melting (SLM) in fabricating Ti6Al4V parts. Design/methodology/approach Ti6Al4V alloy is fabricated by SLM by adopting various energy densities. Microstructures and mechanical properties of the Ti6Al4V deposited using different energy densities are characterized. Findings Both high relative densities and microhardness can be obtained in the optimized processing window. The decrease of martensite width and spacing can improve the microhardness on both XOY and XOZ sections when the applied EV (defined as the laser energy per unit volume) increases. The width of the columnar grain increases with EV, resulting in a stronger anisotropy in microhardness between XOY and XOZ sections. Residual tensile stresses exist in the SLMed Ti6Al4V and increase with an increasing EV. A tensile strength of 1,268 MPa, a yield strength of 1,030 MPa, and an elongation of 4% can be obtained by using the optimized range of EV. Originality/value The microstructure of SLMed Ti6Al4V is quantitatively analysed by measuring the size of columnar grains and the martensites. The anisotropy of microstructures and properties in SLMed Ti6Al4V is characterized and its dependence on laser energy density is established. The residual stress in SLMed Ti6Al4V is characterized and its dependence on laser energy density is established. An optimized processing window to deposit Ti6Al4V alloy by SLM is proposed.

scholarly journals Effect of Laser Energy Density, Internal Porosity and Heat Treatment on Mechanical Behavior of Biomedical Ti6Al4V Alloy Obtained with DMLS Technology

Materials ◽  
2019 ◽  
Vol 12 (14) ◽  
pp. 2331 ◽  
Author(s):  
Żaneta Anna Mierzejewska
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Energy Density ◽  
Laser Energy ◽  
Xrd Analysis ◽  
Laser Energy Density ◽  
Simultaneous Increase ◽  
Direct Metal Laser Sintering ◽  
X Ray Diffraction ◽  
Elongation At Break

The purpose of this paper was to determine the influence of selected parameters of Direct Metal Laser Sintering and various heat treatment temperatures on the mechanical properties of Ti6Al4V samples oriented vertically (V, ZX) and horizontally (H, XZ). The performed micro-CT scans of as-build samples revealed that the change in laser energy density significantly influences the change in porosity of the material, which the parameters (130–210 W; 300–1300 mm/s), from 9.31% (130 W, 1300 mm/s) to 0.16% (190 W, 500 mm/s) are given. The mechanical properties, ultimate tensile strength (UTS, Rm) and yield strength (YS, Re) of the DMLS as-build samples, were higher than the ASTM F 1472 standard suggestion (UTS = 1100.13 ± 126.17 MPa, YS = 1065.46 ± 127.91 MPa), and simultaneously, the elongation at break was lower than required for biomedical implants (A = 4.23 ± 1.24%). The low ductility and high UTS were caused by a specific microstructure made of α’ martensite and columnar prior β grains. X-Ray Diffraction (XRD) analysis revealed that heat treatment at 850 °C for 2 h caused the change of the microstructure intothe α + β combination, affecting the change of strength parameters—a reduction of UTS and YS with the simultaneous increase in elongation (A). Thus, properties similar to those indicated by the standard were obtained (UTS = 908.63 ± 119.49 MPa, YS = 795.9 ± 159.32 MPa, A = 8.72 ± 2.51%), while the porosity remained almost unchanged. Moreover, the heat treatment at 850 °C resulted in the disappearance of anisotropic material properties caused by the layered structure (UTSZX = 908.36 ± 122.79 MPa, UTSXZ = 908.97 ± 118.198 MPa, YSZX = 807.83 ± 124.05 MPa, YSXZ = 810.56 ± 124.05 MPa, AZX = 8.75 ± 2.65%, and AXZ = 8.68 ± 2.41%).

scholarly journals Influence of Effective Laser Energy on the Structure and Mechanical Properties of Laser Melting Deposited Ti6Al4V Alloy

Materials ◽  
2020 ◽  
Vol 13 (4) ◽  
pp. 962 ◽  
Author(s):  
Daojian Fu ◽  
Xiaoqiang Li ◽  
Minai Zhang ◽  
Min Wang ◽  
Zhen Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Energy Density ◽  
Laser Energy ◽  
Ti6al4v Alloy ◽  
Laser Energy Density ◽  
Coefficient Of Determination ◽  
Structure Property ◽  
Laser Melting ◽  
Process Structure ◽  
Am Processes

The laser energy density (ED) is often utilized in many additive manufacturing (AM) processes studies to help researchers to further investigate the process-structure-property correlations of Ti6Al4V alloys. However, the reliability of the ED is still questionable. In this work, a specific empirical calculation equation of the effective laser energy (Ee), which is a dimensionless parameter in laser melting deposition (LMD) processing, was proposed based on the molten pool temperature. The linear regression results and the coefficient of determination prove the feasibility of the Ee equation, which indicates that Ee can more accurately reflect the energy-temperature correlations than the commonly used laser energy density (ED) equation. Additionally, Ti6Al4V components were fabricated by the LMD process with different Ee to investigate the influence of Ee on their structure and mechanical properties. Experimental results show that the detrimental columnar prior β meso-structure can be circumvented and the uniform α + β laths micro-structure can be obtained in LMD Ti6Al4V by a judicious combination of the process parameter (P = 2000 W, V = 12 mm/s, and F = 10.5 g/min) and Ee (7.98 × 105) with excellent tensile strength (1006 ± 25 MPa) and elongation (14.9 ± 0.6%). Overall, the present work provides an empirical calculation equation to obtain a clearer understanding of the influence of different process parameters and indicates the possibility to fabricate the Ti6Al4V alloy with excellent mechanical properties by parameter optimization in the LMD process.

Fundamentals of radiation heat transfer in AlSi10Mg powder bed during selective laser melting

2019 ◽  
Vol 25 (9) ◽  
pp. 1506-1515 ◽  
Author(s):  
Pei Wei ◽  
Zhengying Wei ◽  
Zhne Chen ◽  
Jun Du ◽  
Yuyang He ◽  
...  
Keyword(s):  
Heat Transfer ◽  
Energy Density ◽  
Negative Impact ◽  
Laser Energy ◽  
Melting Process ◽  
Laser Energy Density ◽  
Granular System ◽  
Laser Melting ◽  
Content Type ◽  
Powder Bed

Purpose This paper aims to study numerically the influence of the applied laser energy density and the porosity of the powder bed on the thermal behavior of the melt and the resultant instability of the liquid track. Design/methodology/approach A three-dimensional model was proposed to predict local powder melting process. The model accounts for heat transfer, melting, solidification and evaporation in granular system at particle scale. The proposed model has been proved to be a good approach for the simulation of the laser melting process. Findings The results shows that the applied laser energy density has a significantly influence on the shape of the molten pool and the local thermal properties. The relative low or high input laser energy density has the main negative impact on the stability of the scan track. Decreasing the porosity of the powder bed lowers the heat dissipation in the downward direction, resulting in a shallower melt pool, whereas pushing results in improvement in liquid track quality. Originality/value The randomly packed powder bed is calculated using discrete element method. The powder particle information including particle size distribution and packing density is taken into account in placement of individual particles. The effect of volumetric shrinkage and evaporation is considered in numerical model.

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