scholarly journals Selective Laser Melting of Duplex Stainless Steel 2205: Effect of Post-Processing Heat Treatment on Microstructure, Mechanical Properties, and Corrosion Resistance

Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2468 ◽  
Author(s):  
Papula ◽  
Song ◽  
Pateras ◽  
Chen ◽  
Brandt ◽  
...  

Additive manufacturing (AM) is a rapidly growing field of technology. In order to increase the variety of metal alloys applicable for AM, selective laser melting (SLM) of duplex stainless steel 2205 powder and the resulting microstructure, density, mechanical properties, and corrosion resistance were investigated. An optimal set of processing parameters for producing high density (>99.9%) material was established. Various post-processing heat treatments were applied on the as-built predominantly ferritic material to achieve the desired dual-phase microstructure. Effects of annealing at temperatures of 950 °C, 1000 °C, 1050 °C, and 1100 °C on microstructure, crystallographic texture, and phase balance were examined. As a result of annealing, 40–46 vol.% of austenite phase was formed. Annealing decreased the high yield and tensile strength values of the as-built material, but significantly increased the ductility. Annealing also decreased the residual stresses in the material. Mechanical properties of the SLM-processed and heat-treated materials outperformed those of conventionally produced alloy counterparts. Using a scanning strategy with 66° rotation between layers decreased the strength of the crystallographic texture. Electrochemical cyclic potentiodynamic polarization testing in 0.6 M NaCl solution at room temperature showed that the heat treatment improved the pitting corrosion resistance of the as-built SLM-processed material.

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1012 ◽  
Author(s):  
Feng Shang ◽  
Xiaoqiu Chen ◽  
Zhiyong Wang ◽  
Zuchun Ji ◽  
Fei Ming ◽  
...  

UNS S32707 hyper-duplex stainless steel (HDSS) parts with complex shapes for ocean engineering were prepared by selective laser melting (SLM) process. In the process of SLM, the balance between austenite and ferrite was undermined due to the high melting temperature and rapid cooling rate, resulting in poor ductility and toughness. The solution annealing was carried out with various temperatures (1050–1200 °C) for one hour at a time. The evolution of microstructures, mechanical properties, and corrosion resistance of UNS S32707 samples prepared by SLM was comprehensively investigated. The results indicate that a decrease in nitrogen content during the SLM process reduced the content of austenite, and a nearly balanced microstructure was obtained after appropriate solution annealing. The ratio between ferrite and austenite was approximately 59.5:40.5. The samples with solution treated at 1150 °C and 1100 °C exhibited better comprehensive mechanical properties and pitting resistance, respectively.


2018 ◽  
Vol 941 ◽  
pp. 698-703 ◽  
Author(s):  
Milad Ghayoor ◽  
Sunil B. Badwe ◽  
Harish Irrinki ◽  
Sundar V. Atre ◽  
Somayeh Pasebani

Water atomized and gas atomized 17-4 PH stainless steel powder were used as feedstock in selective laser melting process. Gas atomized powder revealed single martensitic phase after printing and heat treatment. As-printed water atomized powder contained dual martensitic and austenitic phase. The H900 heat treatment cycle was not effective in enhancing mechanical properties of the water atomized powder after laser melting. However, after solutionizing at 1315 oC and aging at 482oC fully martensitic structure was observed with yield strength of 1000 MPa and ultimate tensile strength of 1261 MPa which are comparable to those of gas atomized, 1254 MPa and 1300 MPa, respectively. Improved mechanical properties in water atomized powder was found to be related to presence of finer martensite. Our results imply that water atomized powder is a promising cheaper feedstock alternative to gas atomized powder.


NANO ◽  
2021 ◽  
Author(s):  
Qingxia Zhang ◽  
Lingtao Meng ◽  
Xiaotian Yin ◽  
Shenghai Wang ◽  
Yong Liu ◽  
...  

In previous studies, the microstructure, mechanical properties and corrosion resistance of Hastelloy X fabricated by selective laser melting (SLM) have been investigated; however, it is hoped that heat treatment will effect on its properties. Therefore, this study is to discuss heat treatment effect on Hastelloy X fabricated by SLM. It is interestingly found that fracture strain greatly increases with heat treatment, and the yield ratio decreases, which demonstrates the material is more reliable. High temperature tensile behavior is discussed; it is worth mentioning that not only fracture strain of the HT sample increases greatly at 550∘C in comparison with SLM sample, but also ultimate tensile strength increases from 632 MPa to 639 MPa; the results show that the mechanical property can be improved at medium and high temperature by heat treatment. The corrosion resistance of HT sample deteriorates slightly, which can be explained by Cr-rich precipitates. In conclusion, the material after heat treatment is suitable for applications requiring high mechanical reliability and medium and high temperature occasions, but it is not befitting for corrosive environments.


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