scholarly journals Study on Bainitic Transformation by Dilatometer and In Situ LSCM

Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1534
Author(s):  
Xiaoyan Long ◽  
Fucheng Zhang ◽  
Zhinan Yang ◽  
Ming Zhang
Keyword(s):  
Grain Boundary ◽  
Bainitic Ferrite ◽  
Two Dimensions ◽  
Bainitic Transformation ◽  
Transformation Rate ◽  
Bainitic Steel ◽  
Ferrite Growth ◽  
Austenite Grain ◽  
Austenite Grain Boundary

This study investigates the bainitic transformation kinetics of carbide-free bainitic steel with Si + Al and carbide-bearing bainitic steel without Si + Al, as well as the phase transformation and microstructure through in situ high-temperature laser scanning confocal microscopy. Results show that bainitic ferrite plates preferentially nucleate at the grain boundary. New plates nucleate on previously formed ones, including two dimensions which appear on a plane where a three-dimensional space of bainitic ferrite forms. Nucleation on the formed bainitic ferrite is faster than that at the grain boundary in some grains. The bainitic ferrite growth at the austenite grain boundary is longer and has a faster transformation rate. The bainitic ferrite growth on the formed bainitic ferrite plate is shorter and has a slower transformation rate. The location and number of nucleation sites influence the thickness of the bainitic ferrite. The higher the number of plates preferentially nucleating at the original austenite grain boundary, the greater the thickness of the bainitic ferrite.

Formation of Martensite Austenite Constituent in Continuously Cooled Nb-Bearing Low Carbon Steels

2010 ◽  
Vol 638-642 ◽  
pp. 3080-3085 ◽  
Author(s):  
Naoki Takayama ◽  
Goro Miyamoto ◽  
Naoya Kamikawa ◽  
Hidenori Nako ◽  
Tadashi Maki ◽  
...  
Keyword(s):  
Grain Boundary ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Carbon Steels ◽  
Low Carbon ◽  
Cooling Rates ◽  
Microstructure Observation ◽  
Austenite Grain ◽  
Austenite Grain Boundary ◽  
Nb Addition

Fe-0.15%C-1.5%Mn-0.2%Si (Nb-free alloy) and Fe-0.15%C-1.5%Mn-0.2%Si-0.03%Nb (Nb-added alloy) were continuously cooled to room temperature at constant cooling rates in the range from 0.1 to 20K/s. At lower cooling rates, such as 0.1K/s, the Nb addition retards the ferrite transformation, resulting in a decrease in the transformation temperature and an increase in the volume fraction of bainite. The fraction of martensite-austenite constituent (MA) increases by the Nb addition and the largest fraction of MA, about 0.5 %, is observed in the Nb-added specimen cooled at 5K/s. In the specimens cooled at 5K/s, relatively coarse bainite without cementite precipitation is formed near the austenite () grain boundary in both alloys. Most of MA is localized between such relatively coarse bainitic ferrite (BF). On the other hand, MA is hardly observed in the bainite formed with cementite precipitation in  grain. Based on microstructure observation of the continuously cooled specimens down to intermediate temperatures followed by quenching, it is concluded that small-sized untransformed  near  grain boundary partly remains as MA whereas relatively larger untransformed  in the  grain decompose into bainite with cementite precipitation.

scholarly journals Anisotropic Pinning-Effect of Inclusions in Mg-Based Low-Carbon Steel

Materials ◽  
2018 ◽  
Vol 11 (11) ◽  
pp. 2241
Author(s):  
Chi-Kang Lin ◽  
Hsuan-Hao Lai ◽  
Yen-Hao Su ◽  
Guan-Ru Lin ◽  
Weng-Sing Hwang ◽  
...  
Keyword(s):  
Grain Size ◽  
Carbon Steel ◽  
Grain Boundary ◽  
Low Carbon Steel ◽  
In Situ Observation ◽  
Low Carbon ◽  
Austenite Grain Size ◽  
Austenite Grain ◽  
Austenite Grain Boundary

In this study, the effect of austenite grain size on acicular ferrite (AF) nucleation in low-carbon steel containing 13 ppm Mg is determined. The average austenite grain size was calculated using OM Leica software. Results show that the predicted and experimental values of austenite grain size are extremely close, with a deviation of less than 20 µm. AF formation is difficult to induce by either excessively small and large austenite grain sizes; that is, an optimal austenite grain size is required to promote AF nucleation probability. The austenite grain size of 164 µm revealed the highest capacity to induce AF formation. The effects of the maximum distance of carbon diffusion and austenite grain size on the microstructure of Mg-containing low carbon steel are also discussed. Next, the pinning ability of different inclusion types in low-carbon steel containing 22 Mg is determined. The in situ observation shows that not every inclusion could inhibit austenite grain migration; the inclusion type influences pinning ability. The grain mobility of each inclusion was calculated using in situ micrographs of confocal scanning laser microscopy (CSLM) for micro-analysis. Results show that the austenite grain boundary can strongly be pinned by Mg-based inclusions. MnS inclusions are the least effective in pinning austenite grain boundary migration.

scholarly journals A New Systematic Approach Based on Dilatometric Analysis to Track Bainite Transformation Kinetics and the Influence of the Prior Austenite Grain Size

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 324
Author(s):  
David San-Martin ◽  
Matthias Kuntz ◽  
Francisca G. Caballero ◽  
Carlos Garcia-Mateo
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Prior Austenite ◽  
Bainitic Transformation ◽  
Transformation Rate ◽  
Transformation Kinetics ◽  
Austenite Grain Size ◽  
Austenite Grain ◽  
Prior Austenite Grain Size ◽  
Prior Austenite Grain

This investigation explores the influence of the austenitisation heat treatment and thus, of the prior austenite grain size (PAGS), on the kinetics of the bainitic transformation, using as A case study two high-carbon, high-silicon, bainitic steels isothermally transformed (TIso = 250, 300, 350 °C), after being austenised at different temperatures (γTγ = 925–1125 °C). A methodology, based on the three defining dilatometric parameters extracted from the derivative of the relative change in length, was proposed to analyse the transformation kinetics. These parameters are related to the time to start bainitic transformation, the time lapse for most of the transformation to take place and the transformation rate at the end of the transformation. The results show that increasing the PAGS up to 70 µm leads to an increase in the bainite nucleation rate, this effect being more pronounced for the lowest TIso. However, the overall transformation kinetics seems to be weakly affected by the applied heat treatment (γTγ and TIso). In one of the steels, PAGS > 70 µm (γTγ > 1050 °C), which weakly affects the progress of the transformation, except for TIso = 250 °C, for which the enhancement of the autocatalytic effect could be the reason behind an acceleration of the overall transformation.

Cavitation control in steels of high residual element content

1980 ◽  
Vol 295 (1413) ◽  
pp. 305-305 ◽  
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Prior Austenite ◽  
Low Alloy Steels ◽  
Boundary Zone ◽  
Austenite Grain ◽  
Alloy Steels ◽  
Austenite Grain Boundary ◽  
Prior Austenite Grain ◽  
Transverse Boundary

The cavitational mode of failure of prior austenite grain boundaries in bainitic creep-resisting low alloy steels is now well established as a principal factor in the high incidence of cracking problems which has developed on modern power plant in recent years. The microstructural features dominating the cavitation process at the reheat temperature in a ½CMV bainitic steel of high classical residual level have been determined. The prior austenite grain boundaries become zones of comparative weakness ca . 1 pm thick at 700 °C and are incapable of sustaining significant shear loads. Deformation is therefore initiated by a relaxation of load, through a process of prior austenite grain boundary zone shear, from inclined to transverse boundaries such that a concentration of normal stress develops across the latter. The overall deformation is thereafter determined by cavitation of the transverse boundary zones, the necessary inclined boundary displacements being accommodated by further grain boundary zone shear. Transverse boundary cavitation is shown to be an essentially time-independent process of localized ductile microvoid coalescence resulting from the plastic deformation of the boundary zone.

scholarly journals Effect of Two-Step Austempering Process on Transformation Kinetics of Nanostructured Bainitic Steel

Materials ◽  
2019 ◽  
Vol 12 (1) ◽  
pp. 166 ◽  
Author(s):  
Chunhe Chu ◽  
Yuman Qin ◽  
Xuemei Li ◽  
Zhinan Yang ◽  
Fucheng Zhang ◽  
...  
Keyword(s):  
Activation Energy ◽  
Energy Barrier ◽  
Bainitic Ferrite ◽  
Transformation Process ◽  
Transformation Rate ◽  
Bainitic Steel ◽  
Transformation Kinetics ◽  
Activation Energy Barrier ◽  
Quenching Process ◽  
Kinetics Of

The two-step austempering process has been reported to be an effective method to accelerate the bainitic transformation process by introducing martensite (Q-M-B). However, in this study, it was found that the Q-M-B process reduced the incubation time, but the transformation duration remained nearly unchanged. The notably reduced activation energy barrier for nucleation of bainitic ferrite on the preformed martensite should be responsible for the reduced duration time of the Q-M-B process. A process that both of the two steps were above, Ms (Q-B-B), has been demonstrated to increase transformation rate and improve the amount of bainitic ferrite, which probably results from the additional hysteresis free energy provided by the first quenching process.

Isothermal Transformation, Microstructure and Mechanical Properties of Ausformed Low-Carbon Carbide-Free Bainitic Steel

2018 ◽  
Vol 941 ◽  
pp. 329-333 ◽  
Author(s):  
Jiang Ying Meng ◽  
Lei Jie Zhao ◽  
Fan Huang ◽  
Fu Cheng Zhang ◽  
Li He Qian
Keyword(s):  
Mechanical Properties ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Bainitic Ferrite ◽  
Isothermal Transformation ◽  
Bainitic Transformation ◽  
Isothermal Treatment ◽  
Bainitic Steel ◽  
Low Carbon ◽  
Microstructure And Mechanical Properties

In the present study, the effects of ausforming on the bainitic transformation, microstructure and mechanical properties of a low-carbon rich-silicon carbide-free bainitic steel have been investigated. Results show that prior ausforming shortens both the incubation period and finishing time of bainitic transformation during isothermal treatment at a temperature slightly above the Mspoint. The thicknesses of bainitic ferrite laths are reduced appreciably by ausforming; however, ausforming increases the amount of large blocks of retained austenite/martenisite and decreases the volume fraction of retained austenite. And accordingly, ausforming gives rise to significant increases in both yield and tensile strengths, but causes noticeable decreases in ductility and impact toughness.

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