scholarly journals Microstructure and Corrosion Behavior of Friction Stir-Welded 6061 Al/AZ31 Mg Joints with a Zr Interlayer

Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1115 ◽  
Author(s):  
Yang Zheng ◽  
Xiaomeng Pan ◽  
Yinglei Ma ◽  
Shuming Liu ◽  
Libin Zang ◽  
...  
Keyword(s):  
Corrosion Behavior ◽  
Galvanic Corrosion ◽  
Stir Zone ◽  
Thermal Barrier ◽  
Al Alloy ◽  
X Ray ◽  
Friction Stir ◽  
Base Materials ◽  
Dissimilar Alloys ◽  
Scanning Electron

Friction stir welding (FSW) with a Zr interlayer was employed to join dissimilar alloys of 6061 Al and AZ31 Mg. The microstructures of Al/Mg and Al/Zr/Mg joints were investigated by optical microscopy (OM), scanning electron microscopy (SEM), and energy dispersive X-ray spectrometer (EDS). The results showed that the central part of the Zr interlayer was smashed and intermixed with the base materials in the stir zone, whereas the undamaged part remained stable at the Al/Mg interface. The formation of Al–Mg intermetallic compounds (IMCs) was suppressed by the Zr interlayer due to its synergetic effects of chemical modification and thermal barrier. The electrochemical measurements revealed a differentiated corrosion behavior for each joint, where the corrosion rate of representative regions increased in the order of Al alloy < Mg alloy < heat-affected zone < stir zone. The immersion tests indicated an enhancement in corrosion resistance for the Al/Zr/Mg joint compared with the Al/Mg joint, which is owing to the mitigated galvanic corrosion between the base materials by the Zr interlayer.

Sem Studies of Co-Cr-Mo Surgical Implant Alloy Corrosion Behavior

1982 ◽  
Vol 40 ◽  
pp. 520-521
Author(s):  
Ann Chidester Van Orden ◽  
John L. Chidester ◽  
Anna C. Fraker ◽  
Pei Sung
Keyword(s):  
Electron Microscopy ◽  
Corrosion Behavior ◽  
Anodic Polarization ◽  
Saline Solution ◽  
Saturated Calomel Electrode ◽  
Physiological Saline ◽  
X Ray ◽  
Physiological Saline Solution ◽  
Scanning Electron

The influence of small variations in the composition on the corrosion behavior of Co-Cr-Mo alloys has been studied using scanning electron microscopy (SEM), energy dispersive x-ray analysis (EDX), and electrochemical measurements. SEM and EDX data were correlated with data from in vitro corrosion measurements involving repassivation and also potentiostatic anodic polarization measurements. Specimens studied included the four alloys shown in Table 1. Corrosion tests were conducted in Hanks' physiological saline solution which has a pH of 7.4 and was held at a temperature of 37°C. Specimens were mechanically polished to a surface finish with 0.05 µm A1203, then exposed to the solution and anodically polarized at a rate of 0.006 v/min. All voltages were measured vs. the saturated calomel electrode (s.c.e.).. Specimens had breakdown potentials near 0.47V vs. s.c.e.

scholarly journals The Effect of Vibration during Friction Stir Welding on Corrosion Behavior, Mechanical Properties, and Machining Characteristics of Stir Zone

Metals ◽  
2017 ◽  
Vol 7 (10) ◽  
pp. 421 ◽  
Author(s):  
Sajad Fouladi ◽  
Amir Ghasemi ◽  
Mahmoud Abbasi ◽  
Morteza Abedini ◽  
Amir Khorasani ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Friction Stir Welding ◽  
Corrosion Behavior ◽  
Stir Zone ◽  
Friction Stir ◽  
Machining Characteristics

Where Does the Lithium Go? - A Study of the Precipitates in the Stir Zone of a Friction Stir Weld in a Li-containing 2xxx Series Al Alloy

2010 ◽  
pp. NA-NA ◽  
Author(s):  
Jiancun Rao ◽  
Eric J. Payton ◽  
Christoph Somsen ◽  
Klaus Neuking ◽  
Gunther Eggeler ◽  
...  
Keyword(s):  
Stir Zone ◽  
Friction Stir Weld ◽  
Al Alloy ◽  
Friction Stir

Experimental Estimation of Strain Rate during FSW of Al-Alloy Using Plane-Strain Compression

2008 ◽  
Vol 580-582 ◽  
pp. 299-302 ◽  
Author(s):  
Kunitaka Masaki ◽  
Yutaka S. Sato ◽  
Masakatsu Maeda ◽  
Hiroyuki Kokawa
Keyword(s):  
Strain Rate ◽  
Plane Strain ◽  
Travel Speed ◽  
Plane Strain Compression ◽  
Stir Zone ◽  
Grain Structure ◽  
Al Alloy ◽  
Strain Rates ◽  
Friction Stir ◽  
Grain Structures

Friction stir welding (FSW) makes the stir zone with fine recrystallized grain structure. The recrystallized grains would be formed through dynamic recrystallization at high temperatures and high strain-rate. The present study experimentally simulated the dynamically recrystallized microstructure of a friction stir welded Al alloy 1050 produced at 600 rpm rotation and 100 mm/min travel speed, using combination of the plane-strain compression at various strain rates and the subsequent cooling along the cooling cycle of FSW. The equiaxed grain structures similar to the microstructure of the stir zone were produced at strain rates between 0.1 and 32 s-1; the grain size decreased with increasing strain rate. Strain rate during the FSW could be estimated to be about 1.8 s-1. The present study suggests that plane-strain compression test can simulate the recrystallized grain structure of the friction stir welds.

scholarly journals Double Reinforcement of Al–Fe Intermetallic Composites Fabricated by Friction Stir Processing

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1002
Author(s):  
Chunping Huang ◽  
Yang Xia ◽  
Chun Xia ◽  
Fencheng Liu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Friction Stir Processing ◽  
Volume Fraction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Friction Stir ◽  
Metallurgical Bond ◽  
Aluminum Alloy Surface ◽  
Scanning Electron

A double reinforced layer on an aluminum alloy surface was produced using friction stir processing (FSP) by adding 34CrNiMo6 powder into Al (AA2024) substrate for better wear resistance and gradient transitions. The microstructures of the composites were analyzed using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The phase composition was examined by X-ray diffraction (XRD). The results show that the double reinforced layer of the Al13Fe4 intermetallic compound could be successfully fabricated via FSP. The volume fraction of Al13Fe4 in the double reinforced layer was higher than in the single reinforced layer due to adding 34CrNiMo6 powder and reinforced twice, and the Al13Fe4 particles were dispersed more homogeneously in the double reinforced layer. The interfaces between the double and single reinforced layer had a good metallurgical bond. The microhardness of the double reinforcement layer was significantly increased. Compared with the AA2024 substrate, the microhardness of the double and single reinforced layers increased five- (576 HV) and two-fold (254 HV), respectively.

Study on Corrosion Behavior of Al-Zn-In and Al-Zn-Ga Alloys in NaCl Solution

2011 ◽  
Vol 284-286 ◽  
pp. 1701-1704
Author(s):  
Jing Ling Ma ◽  
Jiu Ba Wen ◽  
Gao Lin Li
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Electrochemical Impedance Spectroscopy ◽  
Corrosion Behavior ◽  
Electrochemical Impedance ◽  
Nacl Solution ◽  
X Ray ◽  
Inductive Loop ◽  
Capacitive Loop ◽  
Scanning Electron

The corrosion behavior of Al-5Zn-0.03In and Al-5Zn-0.03Ga alloys in 3.5 % NaCl solution has been examined by electrochemical methods, scanning electron microscopy, X-ray microanalysis, electrochemical impedance spectroscopy. The results demonstrate that the alloys differ in the microstructure, corroded morphology and electrochemical properties. For Al-5Zn-0.03In alloy, the precipitates enriched in Al and Zn initiates pitting. For Al-5Zn-0.03Ga alloy, corrosion occurs more uniformly, the corrosion of the alloy occurred via the formation of a surface Ga-Al amalgam alloy. The EIS of Al-5Zn-0.03In alloy contains a capacitive loop and an inductive loop; the inductive loop can be attributed to the presence of the pitting. The EIS of Al-5Zn-0.03Ga alloy contains only a capacitive loop.

Microstructural analysis of the stir zone of Al alloy produced by friction stir spot welding

2009 ◽  
Vol 23 (6) ◽  
pp. 403-410 ◽  
Author(s):  
Mitsuo Fujimoto ◽  
Shinji Koga ◽  
Natsumi Abe ◽  
Yutaka S. Sato ◽  
Hiroyuki Kokawa
Keyword(s):  
Spot Welding ◽  
Microstructural Analysis ◽  
Friction Stir Spot Welding ◽  
Stir Zone ◽  
Al Alloy ◽  
Friction Stir

scholarly journals Joining of γ-TiAl Alloy to Ni-Based Superalloy Using Ag-Cu Sputtered Coated Ti Brazing Filler Foil

Metals ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 723 ◽  
Author(s):  
Sónia Simões ◽  
Carlos Tavares ◽  
Aníbal Guedes
Keyword(s):  
Electron Microscopy ◽  
Solid Solution ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Tial Alloy ◽  
Energy Dispersive ◽  
X Ray ◽  
Base Materials ◽  
Intermetallic Particles ◽  
Scanning Electron

Joining γ-TiAl alloy to Ni-based superalloy Hastelloy using Ag-Cu sputtered coated Ti foil as brazing filler was investigated in this study. Brazing experiments were performed at 900, 950, and 980 °C with a dwelling stage of 10 min in vacuum. The microstructure and the chemical composition of the resulting interfaces were analyzed by scanning electron microscopy (SEM) and by energy dispersive X-ray spectroscopy (EDS), respectively. Sound joints were produced after brazing at 980 °C, presenting a multilayered interface, consisting mainly of Ti-Al and Ti-Ni-Al intermetallics close to the γ-TiAl alloy, and of Ti-rich, Ti-Ni, and Cr-Ni-Mo rich phases near Hastelloy. The hardness of the interface, ranging from around 300 to 1100 HV0.01, is higher than both base materials, but no segregation of either Ag solid solution or coarse intermetallic particles was observed. Therefore, the developed brazing filler also avoids the need to perform post-brazing heat treatments that aim to eliminate detrimental extensive segregation of either soft phases or of hard and brittle compounds.

Dissimilar Materials Joining between SSM 356-T6 and AA6061-T651 by Friction Stir Welding

2013 ◽  
Vol 372 ◽  
pp. 478-485 ◽  
Author(s):  
Chaiyoot Meengam ◽  
Muhamad Tehyo ◽  
Prapas Muangjunburee ◽  
Jessada Wannasin
Keyword(s):  
Tensile Strength ◽  
Friction Stir Welding ◽  
Welding Speed ◽  
Rotation Speed ◽  
Stir Zone ◽  
Weld Nugget ◽  
Friction Stir ◽  
Tool Rotation Speed ◽  
Base Materials ◽  
Tool Rotation

The aim of this research is to study the influence of welding parameters on the metallurgical and mechanical properties of friction stir welded butt joints of dissimilar aluminum alloy sheets between Semi-Solid Metal (SSM) 356-T6 and AA6061-T651 by Friction Stir Welding (FSW). The base materials of SSM 356-T6 and AA6061-T651 were located on the advancing side (AS) and on the retreating side (RS) respectively. The base materials were joined under different tool rotation speeds and welding speeds. The material flows from SSM 356 and AA6061-T651 were clearly visible in the weld nugget. In addition, the mixtures of fine equiaxed grain were observed in the stir zone. The increase in tool rotation speed results in the increase in tensile strength of the joints. As for welding speed associated with various tool rotation speeds, an increase in the welding speed affected lesser the base materials tensile strength up to an optimum value; after which its effect increased. Tensile elongation was generally greater at greater tool rotation speed. An averaged maximum tensile strength of 206.3 MPa was derived for a welded specimen produced at the tool rotation speed of 2,000 rpm associated with the welding speed of 80 mm/min. In the weld nugget, higher hardness was observed in the stir zone than in the thermo-mechanically affected zone. Away from the weld nugget, hardness levels increased back to the levels of the base materials.

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