scholarly journals Effect of Ce Addition on Modifying the Microstructure and Achieving a High Elongation with a Relatively High Strength of As-Extruded AZ80 Magnesium Alloy

Materials ◽  
2018 ◽  
Vol 12 (1) ◽  
pp. 76 ◽  
Author(s):  
Zheng Wang ◽  
Jin-Guo Wang ◽  
Ze-Yu Chen ◽  
Min Zha ◽  
Cheng Wang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Dynamic Recrystallization ◽  
Grain Refinement ◽  
High Strength ◽  
Tensile Tests ◽  
Area Fraction ◽  
Schmid Factor ◽  
High Elongation ◽  
Az80 Alloy ◽  
Ce Content

Forming magnesium alloys with rare earth elements (La, Gd, Nd, Y, Ce) is a routine method for modifying their microstructure and properties. In the present work, the effect of Ce addition on the microstructure evolution and the mechanical properties of as-extruded Mg-8Al-0.5Zn (AZ80) alloy was investigated. All of the extruded AZ80-xCe (x = 0, 0.2, 0.8 and 1.4 wt %) alloys exhibited equiaxed grains formed by fully dynamic recrystallization, and the grain size of the extruded AZ80 alloy was remarkably reduced by ~56.7% with the addition of 1.4 wt % Ce. Furthermore, the bulk-shaped Al4Ce phase formed when Ce was first added, with the Ce content rising to 0.8 wt % or higher, and Al4Ce particles in both the nano- and micron sizees were well distributed in the primary α-Mg matrix. The area fraction of the Al4Ce particles expanded with increasing Ce content, providing more nuclei for dynamic recrystallization, which could contribute to the grain refinement. The results of the tensile tests in this study showed that Ce addition effectively improved the room temperature formability of the as-extruded AZ80 alloy, without sacrificing strength. The significantly improved mechanical properties were ascribed to excellent grain refinement, weakened texture strength, an increased Schmid factor, and a reduced area fraction of low-angle grain boundaries, all resulting from Ce addition to the as-extruded AZ80 alloy. The contribution of the nano-Al4Ce precipitates on improving the mechanical properties was also discussed in this paper.

Mechanical Properties and Aging Behavior of Ultrafine Grained Al-Ag Alloy Fabricated by Accumulative Roll-Bonding

2014 ◽  
Vol 794-796 ◽  
pp. 851-856
Author(s):  
Tadashiege Nagae ◽  
Nobuhiro Tsuji ◽  
Daisuke Terada
Keyword(s):  
Mechanical Properties ◽  
Grain Refinement ◽  
Accumulative Roll Bonding ◽  
Precipitation Hardening ◽  
Tensile Elongation ◽  
Solution Treatment ◽  
High Strength ◽  
Subsequent Aging ◽  
Roll Bonding ◽  
Ultrafine Grained

Accumulative roll-bonding (ARB) process is one of the severe plastic deformation processes for fabricating ultrafine grained materials that exhibit high strength. In aluminum alloys, aging heat treatment has been an important process for hardening materials. In order to achieve good mechanical properties through the combination of grain refinement hardening and precipitation hardening, an Al-4.2wt%Ag binary alloy was used in the present study. After a solution treatment at 550°C for 1.5hr, the alloy was severely deformed by the ARB process at room temperature (RT) up to 6 cycles (equivalent strain of 4.8). The specimens ARB-processed by various cycles (various strains) were subsequently aged at 100, 150, 200, 250°C, and RT. The hardness of the solution treated (ST) specimen increased by aging. On the other hand, hardness of the ARB processed specimen decreased after aging at high temperatures such as 250°C. This was probably due to coarsening of precipitates or/and matrix grains. The specimen aged at lower temperature showed higher hardness. The maximum harnesses achieved by aging for the ST specimen, the specimens ARB processed by 2 cycles, 4 cycles and 6 cycles were 55HV, 71HV, 69HV and 65HV, respectively. By tensile tests it was shown that the strength increased by the ARB process though the elongation decreased significantly. However, it was found that the tensile elongation of the ARB processed specimens was improved by aging without sacrificing the strength. The results suggest that the Al-Ag alloy having large elongation as well as high strength can be realized by the combination of the ARB process for grain refinement and the subsequent aging for precipitation hardening.

Investigations on the Mechanical Properties and Formability of Friction Stir Welded Tailored Blanks

2007 ◽  
Vol 344 ◽  
pp. 143-150 ◽  
Author(s):  
Gianluca Buffa ◽  
Livan Fratini ◽  
Marion Merklein ◽  
Detlev Staud
Keyword(s):  
Mechanical Properties ◽  
Stress Condition ◽  
Research Effort ◽  
High Strength Steels ◽  
High Strength ◽  
Tensile Tests ◽  
Friction Stir ◽  
Tailored Blanks ◽  
Sheet Stamping ◽  
Wide Range

Tight competition characterizing automotive industries in the last decades has determined a strong research effort aimed to improve utilized processes and materials in sheet stamping. As far as the latter are regarded light weight alloys, high strength steels and tailored blanks have been increasingly utilized with the aim to reduce parts weight and fuel consumptions. In the paper the mechanical properties and formability of tailored welded blanks made of a precipitation hardenable aluminum alloy but with different sheet thicknesses, have been investigated: both laser welding and friction stir welding have been developed to obtain the tailored blanks. For both welding operations a wide range of the thickness ratios has been considered. The formability of the obtained blanks has been characterized through tensile tests and cup deep drawing tests, in order to show the formability in dependency of the stress condition; what is more mechanical and metallurgical investigations have been made on the welded joints.

scholarly journals Experimental Investigation into Corrosion Effect on Mechanical Properties of High Strength Steel Bars under Dynamic Loadings

2018 ◽  
Vol 2018 ◽  
pp. 1-12 ◽  
Author(s):  
Hui Chen ◽  
Jinjin Zhang ◽  
Jin Yang ◽  
Feilong Ye
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Dynamic Loading ◽  
High Strength Steel ◽  
High Strength ◽  
Tensile Tests ◽  
Reinforcing Steel ◽  
Test Results ◽  
Cross Sectional ◽  
Steel Bars

The tensile behaviors of corroded steel bars are important in the capacity evaluation of corroded reinforced concrete structures. The present paper studies the mechanical behavior of the corroded high strength reinforcing steel bars under static and dynamic loading. High strength reinforcing steel bars were corroded by using accelerated corrosion methods and the tensile tests were carried out under different strain rates. The results showed that the mechanical properties of corroded high strength steel bars were strain rate dependent, and the strain rate effect decreased with the increase of corrosion degree. The decreased nominal yield and ultimate strengths were mainly caused by the reduction of cross-sectional areas, and the decreased ultimate deformation and the shortened yield plateau resulted from the intensified stress concentration at the nonuniform reduction. Based on the test results, reduction factors were proposed to relate the tensile behaviors with the corrosion degree and strain rate for corroded bars. A modified Johnson-Cook strength model of corroded high strength steel bars under dynamic loading was proposed by taking into account the influence of corrosion degree. Comparison between the model and test results showed that proposed model properly describes the dynamic response of the corroded high strength rebars.

scholarly journals Changing in Fatigue Life of 300 M Bainitic Steel After Laser Carburizing and Plasma Nitriding

2018 ◽  
Vol 165 ◽  
pp. 21002 ◽  
Author(s):  
Antonio J. Abdalla ◽  
Douglas Santos ◽  
Getúlio Vasconcelos ◽  
Vladimir H. Baggio-Scheid ◽  
Deivid F. Silva
Keyword(s):  
Mechanical Properties ◽  
Fatigue Life ◽  
Plasma Nitriding ◽  
Fatigue Behavior ◽  
High Strength ◽  
Tensile Tests ◽  
Steel Sample ◽  
Fatigue Tests ◽  
300M Steel ◽  
Structural Applications

In this work 300M steel samples is used. This high-strength steel is used in aeronautic and aerospace industry and other structural applications. Initially the 300 M steel sample was submitted to a heat treatment to obtain a bainític structure. It was heated at 850 °C for 30 minutes and after that, cooled at 300 °C for 60 minutes. Afterwards two types of surface treatments have been employed: (a) using low-power laser CO2 (125 W) for introducing carbon into the surface and (b) plasma nitriding at a temperature of 500° C for 3 hours. After surface treatment, the metallographic preparation was carried out and the observations with optical and electronic microscopy have been made. The analysis of the coating showed an increase in the hardness of layer formed on the surface, mainly, among the nitriding layers. The mechanical properties were analyzed using tensile and fatigue tests. The results showed that the mechanical properties in tensile tests were strongly affected by the bainitic microstructure. The steel that received the nitriding surface by plasma treatment showed better fatigue behavior. The results are very promising because the layer formed on steel surface, in addition to improving the fatigue life, still improves protection against corrosion and wear.

Effect of Plastic Deformation on the Mechanical Properties and Microstructure of Homogenized AZ80 Magnesium Alloy

2010 ◽  
Vol 139-141 ◽  
pp. 180-184
Author(s):  
Yong Xue ◽  
Zhi Min Zhang ◽  
Li Hui Lang
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Grain Boundaries ◽  
Gradual Increase ◽  
Tensile Tests ◽  
Extrusion Ratio ◽  
Extrusion Temperature ◽  
Second Phase ◽  
Strength And Plasticity ◽  
Az80 Alloy

In the present research, the influences of different extrusion ratios (15, 30, 45, 60, and 75) and extrusion temperatures (300°C, 330°C, 360°C, 390°C, 420°C) on the mechanical properties and microstructure of homogenized AZ80 alloy have been investigated through the tensile tests and via metallographic microscope observation. The results show that the alloy’s grain is small and small amounts of black hard and brittle second-phase β (Mg17Al12) are precipitated uniformly along the grain boundary causing the gradual increase of the alloy’s tensile strength at 330°C. When the extrusion temperature is up to 390°C, the grain size increases significantly, but the second phase precipitation along grain boundaries transforms into continuous and uniform-distribution precipitation within the grain. In this case, when the extrusion ratio is 60, the alloy’s tensile strength reaches its peak 390Mpa. As the extrusion temperature increases, inhomogeneous precipitation of the second-phase along grain boundaries increases, causing the decrease of the alloy’s strength. At the same temperature, the tensile strength increases firstly and then decreases as extrusion ratio increases. With the gradual increase of the refinement grain, the dispersed precipitates increase and the alloy’s tensile strength and plasticity reach their peaks when the extrusion temperature is 390°C. As the grain grows, the second phase becomes inhomogeneous distribution, and the alloy’s strength and plasticity gradually decrease.

Effect of the Mg3N2 Sub-Micron Particle on the Grain Refinement of AZ80 Alloy

2022 ◽  
Vol 327 ◽  
pp. 45-53
Author(s):  
Jiehua Li ◽  
Maria Pammer ◽  
Ernst Neunteufl ◽  
Peter Schumacher
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Refinement ◽  
Liquid State ◽  
High Performance ◽  
Great Loss ◽  
Micron Particle ◽  
Deformation Ability ◽  
Semi Solid ◽  
Az80 Alloy

AZ80 alloy has been widely used to produce high performance Mg casting and wrought parts for high-end applications due to its high mechanical properties and deformation ability. However, at least two important issues still need to be solved in order to further improve its mechanical properties and deformation ability. Firstly, the grain size of α-Mg in AZ80 alloy is relatively large (more than 1000 µm) due to a lack of efficient grain refinement methodologies. Secondly, the size of the eutectic Mg17Al12 phase is also large and the distribution of the eutectic Mg17Al12 phase is continuous, which is very harmful for the mechanical properties, in particular to elongation. In this paper, these two important issues are investigated by adding Mg3N2 sub-micron particle into AZ80 alloy and thereby refining the α-Mg and the eutectic Mg17Al12 phase. Firstly, the Mg3N2 sub-micron particle was directly added into AZ80 alloy by using mechanically stirring in the semi-solid state, subsequently the melting temperature was increased above the liquidous temperature, and finally the melting was casted in the liquid state. It was found that the grain size of α-Mg can be refined from 883.8 µm to 169.9 µm. More importantly, the eutectic Mg17Al12 phase was also refined and the distribution became discontinuous. It should be noted that directly adding the Mg3N2 sub-micron particle into AZ80 alloy leads to a great loss of the Mg3N2 sub-micron particle due to the weak wetting behavior between the Mg3N2 sub-micron particle and Mg melt. The second methodology through mixing Mg3N2 sub-micron particles with AZ91 chips using a twin extruder was also used to prepare AZ91 master alloy with 3wt.% Mg3N2 sub-micron particle, which was subsequently added into AZ80 alloy in the liquid state. In this way, a significant grain refinement of α-Mg and a simultaneous refinement of the eutectic Mg17Al12 phase in AZ80 alloy was also achieved. The grain size of α-Mg can be refined from 883.8 µm to 325.9 µm. However, no significant grain refinement by using UST was observed. Instead, the grain size increases from 325.9 µm to 448.6 µm, indicating that the Mg3N2 sub-micron particle may lose its grain refinement potency due to possible aggregation and clustering. This paper provides an efficient and simple methodology for the grain refinement of α-Mg and the simultaneous refinement of the eutectic Mg17Al12 phase in AZ80 alloy.

Tensile properties of the FFF-processed thermoplastic polyurethane (TPU) elastomer

2021 ◽  
Author(s):  
Budi Arifvianto ◽  
Teguh Nur Iman ◽  
Benidiktus Tulung Prayoga ◽  
Rini Dharmastiti ◽  
Urip Agus Salim ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Low Cost ◽  
Thermoplastic Polyurethane ◽  
High Strength ◽  
Tensile Tests ◽  
Uniaxial Tensile ◽  
Fused Filament Fabrication ◽  
Raster Angle ◽  
Manufacturing Techniques

Abstract Fused filament fabrication (FFF) has become one of the most popular, practical, and low-cost additive manufacturing techniques for fabricating geometrically-complex thermoplastic polyurethane (TPU) elastomer. However, there are still some uncertainties concerning the relationship between several operating parameters applied in this technique and the mechanical properties of the processed material. In this research, the influences of extruder temperature and raster orientation on the mechanical properties of the FFF-processed TPU elastomer were studied. A series of uniaxial tensile tests was carried out to determine tensile strength, strain, and elastic modulus of TPU elastomer that had been printed with various extruder temperatures, i.e., 190–230 °C, and raster angles, i.e., 0–90°. Thermal and chemical characterizations were also conducted to support the analysis in this research. The results obviously showed the ductile and elastic characteristics of the FFF-processed TPU, with specific tensile strength and strain that could reach up to 39 MPa and 600%, respectively. The failure mechanisms operating on the FFF-processed TPU and the result of stress analysis by using the developed Mohr’s circle are also discussed in this paper. In conclusion, the extrusion temperature of 200 °C and raster angle of 0° could be preferred to be applied in the FFF process to achieve high strength and ductile TPU elastomer.

Effect of Quenching and Partitioning Processing on Microstructure and Mechanical Properties of a Low Alloyed Steel

2018 ◽  
Vol 941 ◽  
pp. 52-57
Author(s):  
Bernd Pfleger ◽  
Marina Gruber ◽  
Gerald Ressel ◽  
Peter Gruber ◽  
Matthew Galler ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Strength ◽  
Phase Evolution ◽  
Tensile Tests ◽  
Austenite Phase ◽  
Phase Fraction ◽  
Quenching Temperature ◽  
Quenching And Partitioning ◽  
Low Alloyed Steel ◽  
A Minor

The concept of quenching and partitioning (Q&P) is a tool to generate steels with high strength and high ductility resulting from a relatively high amount of martensite and austenite. As the parameters of the Q&P treatment influence the strength and ductility properties, the goal of this work was to analyze the effects of varying quenching and partitioning temperatures on the phase evolution, on the retained austenite phase fraction and on the mechanical properties. The phase evolution during heat treatment was analyzed by dilatometer and the microstructure after processing was characterized by light microscopy in combination with color etching according to Klemm. The austenite phase fraction and its carbon content were determined by X-Ray diffraction and the mechanical properties were evaluated by tensile tests. It is shown that the quenching temperature has a minor impact on the phase fraction of austenite as well as its stabilization by carbon and thus, also the mechanical properties. Furthermore, austenite transformation during the partitioning treatment is illustrated.

scholarly journals Effect of Intercritical Annealing and Austempering on the Microstructure and Mechanical Properties of a High Silicon Manganese Steel

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1448 ◽  
Author(s):  
Mattia Franceschi ◽  
Luca Pezzato ◽  
Claudio Gennari ◽  
Alberto Fabrizi ◽  
Marina Polyakova ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Intercritical Annealing ◽  
High Strength ◽  
Xrd Analysis ◽  
Tensile Tests ◽  
Manganese Steel ◽  
Microstructure And Mechanical Properties ◽  
Martensitic Microstructure ◽  
Steel Grades ◽  
High Silicon

High Silicon Austempered steels (AHSS) are materials of great interest due to their excellent combination of high strength, ductility, toughness, and limited costs. These steel grades are characterized by a microstructure consisting of ferrite and bainite, accompanied by a high quantity retained austenite (RA). The aim of this study is to analyze the effect of an innovative heat treatment, consisting of intercritical annealing at 780 °C and austempering at 400 °C for 30 min, on the microstructure and mechanical properties of a novel high silicon steel (0.43C-3.26Si-2.72Mn wt.%). The microstructure was characterized by optical and electron microscopy and XRD analysis. Hardness and tensile tests were performed. A multiphase ferritic-martensitic microstructure was obtained. A hardness of 426 HV and a tensile strength of 1650 MPa were measured, with an elongation of 4.5%. The results were compared with those ones obtained with annealing and Q&T treatments.

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