scholarly journals Study of the Microstructure and Cracking Mechanisms of Hastelloy X Produced by Laser Powder Bed Fusion

Materials ◽  
2018 ◽  
Vol 11 (1) ◽  
pp. 106 ◽  
Author(s):  
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Metals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 996
Author(s):  
Olutayo Adegoke ◽  
Joel Andersson ◽  
Håkan Brodin ◽  
Robert Pederson

This paper reviews state of the art laser powder bed fusion (L-PBF) manufacturing of γ′ nickel-based superalloys. L-PBF resembles welding; therefore, weld-cracking mechanisms, such as solidification, liquation, strain age, and ductility-dip cracking, may occur during L-PBF manufacturing. Spherical pores and lack-of-fusion voids are other defects that may occur in γ′-strengthened nickel-based superalloys manufactured with L-PBF. There is a correlation between defect formation and the process parameters used in the L-PBF process. Prerequisites for solidification cracking include nonequilibrium solidification due to segregating elements, the presence of liquid film between cells, a wide critical temperature range, and the presence of thermal or residual stress. These prerequisites are present in L-PBF processes. The phases found in L-PBF-manufactured γ′-strengthened superalloys closely resemble those of the equivalent cast materials, where γ, γ′, and γ/γ′ eutectic and carbides are typically present in the microstructure. Additionally, the sizes of the γ′ particles are small in as-built L-PBF materials because of the high cooling rate. Furthermore, the creep performance of L-PBF-manufactured materials is inferior to that of cast material because of the presence of defects and the small grain size in the L-PBF materials; however, some vertically built L-PBF materials have demonstrated creep properties that are close to those of cast materials.


Crystals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1064
Author(s):  
Shinya Hibino ◽  
Tsubasa Todo ◽  
Takuya Ishimoto ◽  
Ozkan Gokcekaya ◽  
Yuichiro Koizumi ◽  
...  

The influence of various laser powder bed fusion (LPBF) process parameters on the crystallographic textures and mechanical properties of a typical Ni-based solid-solution strengthened alloy, Hastelloy-X, was examined. Samples were classified into four groups based on the type of crystallographic texture: single crystalline-like microstructure with <100>//build direction (BD) (<100>-SCM), single crystalline-like microstructure with <110>//BD (<110>-SCM), crystallographic lamellar microstructure (CLM), or polycrystalline microstructure (PCM). These four crystallographic textures were realized in Hastelloy-X for the first time here to the best of our knowledge. The mechanical properties of the samples varied depending on their texture. The tensile properties were affected not only by the Schmid factor but also by the grain size and the presence of lamellar boundaries (grain boundaries). The lamellar boundaries at the interface between the <110>//BD oriented main layers and the <100>//BD-oriented sub-layers of CLM contributed to the resistance to slip transmission and the increased proof stress. It was possible to control a wide range of crystallographic microstructures via the LPBF process parameters, which determines the melt pool morphology and solidification behavior.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4305
Author(s):  
Shuzhe Zhang ◽  
Yunpei Lei ◽  
Zhen Chen ◽  
Pei Wei ◽  
Wenjie Liu ◽  
...  

It is of great importance to study the microstructure and textural evolution of laser powder bed fusion (LPBF) formed Hastelloy-X alloys, in order to establish a close relationship between the process, microstructure, and properties through the regulation of the Hastelloy-X formation process parameters. In this paper, components of a Hastelloy-X alloy were formed with different laser energy densities (also known as the volume energy density VED). The densification mechanism of Hastelloy-X was studied, and the causes of defects, such as pores and cracks, were analyzed. The influence of different energy densities on grain size, texture, and orientation was investigated using an electron backscatter diffraction technique. The results show that the average grain size, primary dendrite arm spacing, and number of low angle grain boundaries increased with the increase of energy density. At the same time, the VED can strengthen the texture. The textural intensity increases with the increase of energy density. The best mechanical properties were obtained at the VED of 96 J·mm−3.


2019 ◽  
Vol 762 ◽  
pp. 138081 ◽  
Author(s):  
Ali Keshavarzkermani ◽  
Reza Esmaeilizadeh ◽  
Usman Ali ◽  
Pablo D. Enrique ◽  
Yahya Mahmoodkhani ◽  
...  

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3178 ◽  
Author(s):  
Calignano ◽  
Minetola

The manufacture of highly complex components from nickel-based superalloys with laser powder bed fusion (L-PBF) technology can reduce the production costs parts with comparable microstructural and mechanical properties when compared to casting. The purpose of this study was to investigate the characteristics of samples produced in commercial Hastelloy X (with w% composition of 21Cr-18Fe-9Mo-0.7W-1.5Co-0.1C-1Si-1Mn-0.5Al-0.15Ti-bal.Ni) with an L-PBF process in terms of build density, accuracy, surface roughness, and interface area between the part and the support structures. Samples were obtained with a high density (99.88%), without cracks and with low surface roughness. From the analysis of the support structures, it emerged that the choice of the parameters between support structures, the lower face of the part (down-skin) and the internal area of the part (in-skin) is fundamental to the correct realization of these structures in order to avoid deformation of the components that is induced by thermal stresses during part building.


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