scholarly journals Preparation of Piezo-Resistive Materials by Combination of PP, SEBS and Graphene

2019 ◽  
Vol 3 (2) ◽  
pp. 37 ◽  
Author(s):  
Helga Seyler ◽  
Marián Gómez-Fatou ◽  
Horacio Salavagione
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Electrical Conductivity ◽  
Triblock Copolymer ◽  
Low Cost ◽  
Melt Processing ◽  
Structural Components ◽  
The Matrix ◽  
State Mixing ◽  
Scanning Electron

The use of polyolefins in structural components requires the simultaneous improvement of stiffness and toughness of the matrix, whilst in the case of sensing components during operation, additional functions are needed such as electrical conductivity. However, providing various desired properties without impairing those intrinsic to the materials can be somewhat challenging. In this study we report the preparation of an isotactic polypropylene (iPP)/styrene–ethylene–butylene–styrene triblock copolymer (SEBS)/graphene system that combines enhanced mechanical properties with electrical conductivity. Blends were prepared by solution mixing (SoM) and solution/solid state mixing (SoM/SSM) formulation routes prior to melt processing. The nanocomposites were characterized by scanning electron microscopy (SEM) and thermogravimetric analysis (TGA) and the electrical and mechanical properties were evaluated. The materials prepared via the SoM/SSM route displayed good electrical conductivity while retaining the mechanical properties of iPP, making them attractive materials for low cost and high throughput structural components with sensing capacity.

The Impact Properties of a Polyurethane Composite Filled with Clay

2011 ◽  
Vol 197-198 ◽  
pp. 1100-1103
Author(s):  
Jian Li
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Mechanical Analysis ◽  
Impact Testing ◽  
Impact Properties ◽  
Polyurethane Composite ◽  
The Matrix ◽  
The Impact ◽  
Scanning Electron

A polyurethane/clay (PU/clay) composite was synthesized. The microstructure of the composite was examined by scanning electron microscopy. The impact properties of the composite were characterized by impact testing. The study on the structure of the composite showed that clays could be dispersed in the polymer matrix well apart from a few of clusters. The results from mechanical analysis indicated that the impact properties of the composite were increased greatly in comparison with pure polyurethane. The investigation on the mechanical properties showed that the impact strength could be obviously increased by adding 20 wt% (by weight) clay to the matrix.

Influence of Injection Conditions on the Mechanical Property of MWCNTs/ PC Nanocomposites

2014 ◽  
Vol 983 ◽  
pp. 94-98 ◽  
Author(s):  
Li Jun Wang ◽  
Jian Hui Qiu ◽  
Eiichi Sakai
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Mechanical Property ◽  
Bending Strength ◽  
Surface Hardness ◽  
Interfacial Interaction ◽  
Multiwalled Carbon ◽  
The Matrix ◽  
The Impact ◽  
Scanning Electron

The melting mixing was applied in the preparation of Multiwalled carbon nanotubes/Polycarbonate (MWCNTs/PC) nanocomposites. MWCNTs/PC nanocomposites with different MWCNTs contents were prepared under different injection conditions. The mechanical property of nanocomposites was comparatively investigated. The results demonstrated that: the tensile property of the nanocomposites was slightly improved by MWCNTs content increasing; but as the MWCNTs contents went on to increase to 10wt%, the tensile strength and bending strength were obviously decreased about 35% and 47%, respectively, but the impact strength and hardness were increased. The center hardness of MWCNTs/PC nanocomposites was greater than the surface hardness. Besides, the changes on the mechanical properties of the nanocomposites were studies by changing the injection conditions. By Scanning Electron Microscopy (SEM) observation, the microstructure and morphology of nanocomposites were analyzed, revealing that the center of the nanocomposite distributed more MWNTs, and the injection conditions would affect the MWNTs’ dispersion in the matrix and the interfacial interaction between MWCNTs and PC.

Effect of Ca on Microstructure and Properties of Mg-Al-Si Alloys

2011 ◽  
Vol 194-196 ◽  
pp. 1369-1373 ◽  
Author(s):  
Chun Xiang Xu ◽  
Hui Ju ◽  
Yang Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Chinese Script ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ca Addition ◽  
The Matrix ◽  
Morphology Modification ◽  
Scanning Electron

Effect of Ca addition on the morphology modification in Mg-7Al-0.8Zn-0.2Mn-1Si (AS71) alloys has been investigated using X-ray diffraction (XRD), optical microscopy (OM), and scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and various testing machines. The results show that when adding 0.1 wt% Ca, a small fraction of Mg2Si change from Chinese script type to polygonal type; with the Ca addition up to 0.3 wt%, edges and angles of polygonal type Mg2Si phase are changed; further increase in Ca addition, the morphology of Mg2Si is changed to strip-like or spot-like one. Meanwhile, the addition of Ca results in the morphology of β- Mg17Al12 phase changing from discontinuous net-like to dispersive island-like. Ca exists as solid-soluting atomic in the matrix with small Ca addition while in the form of CaSi2 with large Ca addition. Optimal mechanical properties can be achieved when Ca addition is 0.3 wt%.

Characterization of Polycarbonate/Multiwalled Carbon Nanotube Composites

2006 ◽  
Vol 326-328 ◽  
pp. 1829-1832 ◽  
Author(s):  
Hun Sik Kim ◽  
Byung Hyun Park ◽  
Min Sung Kang ◽  
Jin San Yoon ◽  
Hyoung Joon Jin
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Multiwalled Carbon ◽  
Melt Compounding ◽  
Matrix Strength ◽  
The Matrix ◽  
Nanotube Composites ◽  
Carbon Nanotube Composites ◽  
Scanning Electron

Polycarbonate/multiwalled carbon nanotubes (PC/MWNT) nanocomposites with different contents of MWNT were successfully prepared by melt compounding. The mechanical properties of the PC/MWNT nanocomposites were effectively increased due to the incorporation of MWNTs. The composites were characterized using scanning electron microscopy in order to obtain the information on the dispersion of MWNT in the polymeric matrix. In case of 0.3 wt% of MWNT in the matrix, strength and modulus of the composite increased by 30% and 20%, respectively. In addition, the dispersion of MWNTs in the PC matrix resulted in substantial decrease in the electrical resistivity of the composites as the MWNTs loading was increased from 1.0 wt% to 1.5 wt%.

Development of Al-Fe-(Cu) Series Alloys for Aluminum Cables and the Related Annealing Behaviors

2018 ◽  
Vol 941 ◽  
pp. 937-942
Author(s):  
Hua Chen ◽  
Rong Kai Yang ◽  
Xiao Dong Wu ◽  
Yuan Yuan ◽  
Bing Zhang ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Heat Treatment ◽  
Electrical Conductivity ◽  
Electron Backscattered Diffraction ◽  
Cu Alloy ◽  
Cu Alloys ◽  
Backscattered Electron ◽  
Ebsd Technique ◽  
Scanning Electron

In this work, Al-Fe-(Cu) alloys for aluminum cables were designed and the related annealing behaviors were discussed in detail to help understand the influence of processing and heat treatment on the electrical conductivity and mechanical properties of the studied alloys. The interaction between different solute elements was tracked by using hardness and electrical conductivity testing. The microstructure was investigated by using Electron Backscattered Diffraction (EBSD) technique, along with Scanning Electron Microscopy with Backscattered Electron Detector (BSE). The results show that the conductivities of Al-Fe-Cu alloy increased with the elongated annealing time, and reaches its maximum at 6 h, when annealed at temperatures from 275 °C to 375 °C. The addition of Fe to Al can strengthen the alloy and decrease its conductivity slightly, while the addition of Cu will influence the alloy conductivity significantly. The morphologies of precipitates will change with different amount of alloying elements as well.

Development and Evaluation of Mechanical Properties of Al/Ilmenite Nanocomposite

2014 ◽  
Vol 704 ◽  
pp. 32-38
Author(s):  
Lanka Rasidhar ◽  
A. Rama Krishna ◽  
Ch. Srinivasa Rao ◽  
K. Vijaya Lakshmi
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Secondary Phase ◽  
Stir Casting ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Matrix ◽  
Scanning Electron

In the present investigation, microstructure and mechanical properties of nanocomposites fabricated via stir casting were evaluated. The composites were based on Al (99.7) reinforced with ilmenite nanoparticles. The characterization of the nanoparticles and nanocomposites was investigated by scanning electron microscopy (SEM) and X-ray diffraction (XRD) facilities. Microstructure of specimens show that reasonable distribution of FeTiO3 nanoparticles in the matrix, secondary phase FeAl3 observed in the microstructure. Ultimate tensile strength and compression tests were carried out in order to identify the mechanical properties. The hardness of the composites is enhanced with the addition of nanoparticles. The optimum value for ultimate tensile and compression strength are obtained with the addition of 3 % ilmenite nanoparticles. Ductile fracture in tensile fractured samples was observed by fractrography examination.

scholarly journals Development of Sustainable and Eco-Friendly Materials from Termite Hill Soil Stabilized with Cement for Low-Cost Housing in Chad

Buildings ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 86
Author(s):  
Assia Aboubakar Mahamat ◽  
Numfor Linda Bih ◽  
Olugbenga Ayeni ◽  
Peter Azikiwe Onwualu ◽  
Holmer Savastano ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Scanning Electron Microscopy ◽  
Low Cost ◽  
Sub Saharan Africa ◽  
Ex Situ ◽  
Termite Mound ◽  
X Ray ◽  
Scanning Electron

This paper explores the effects of cement stabilization (5, 10, 15 and 20 wt%) on the structural and mechanical properties (compressive/flexural strengths and fracture toughness) of abandoned termite mound soil. The crystal structures and crystallinity of the constituents were determined using X-ray diffraction (XRD), while the microstructure was characterized via scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDS). The functional groups were also identified using Fourier transform infra-red spectroscopy (FTIR). The compressive/flexural strengths of the stabilized and un-stabilized termite mound soil were also studied after curing for 7, 14 and 28 days. The fracture toughness mechanism was analyzed with the aid of the R-curve method. Additionally, the underlying deformation and cracking mechanisms are elucidated via in-situ/ex-situ optical and scanning electron microscopy. The stabilized termite mound soil displayed the highest mechanical properties of 13.91 MPa, 10.25 MPa and 3.52 kPa·m1/2 for compressive strength, flexural strength and fracture toughness, respectively. Besides displaying good mechanical properties and being locally available at no cost, renewable and an eco-friendly material, the termite mound soil will contribute to lowering the cost of housing in Sub-Saharan Africa, particularly in Chad.

Influence of Microwave on the Structure and Properties of Nanomodified Fluoroplastic

2021 ◽  
Vol 887 ◽  
pp. 10-16
Author(s):  
D.O. Zavrazhin ◽  
A.A. Chuprikova ◽  
Ju.S. Povetkina
Keyword(s):  
Electron Microscopy ◽  
Electrical Conductivity ◽  
Polymer Matrix ◽  
Carbon Nanomaterials ◽  
Microwave Treatment ◽  
Heating Time ◽  
Structure And Properties ◽  
The Matrix ◽  
Scanning Electron ◽  
Polar Polymer

Polymers modified with carbon nanomaterials exhibit enhanced electrical conductivity. The modifier, which is qualitatively distributed in the polymer matrix, actively absorbs microwave waves even with an extremely small introduced volume (up to 1.5 mass parts). Photographs obtained by scanning electron microscopy indicate a uniform distribution of carbon nanotubes in the matrix of fluoroplastic 4. The microwave treatment of the obtained composites showed a significant increase in the temperature of the samples with a heating time of up to 100 sec. even with minimal amounts of modifier added. Strength characteristics for a uniaxial plant of modified materials after microwave increase by 40-50%. The obtained modified materials based on a non-polar polymer matrix have enhanced characteristics of absorption of microwave radiation.

scholarly journals Fabrication and Mechanical Testing of Egg Shell Particles Reinforced Al-Si Composites

2017 ◽  
Vol 2 (1) ◽  
pp. 53-62 ◽  
Author(s):  
Anjali, Razia Anjali, Razia ◽  
Shivani Bhandari ◽  
Ankur Pant ◽  
Arpit Saxena ◽  
Seema ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Waste Materials ◽  
The Matrix ◽  
Egg Shells ◽  
Egg Shell ◽  
Shell Particles ◽  
Industrial Level ◽  
Chicken Eggs ◽  
Scanning Electron

The production of chicken eggs on a widespread industrial level has led to the generation of a large amount of egg shells. These egg shells are considered to be bio-hazardous waste materials although they are a rich source of amino acids and minerals. In the present investigation, effort has been made to incorporate waste poultry egg shell particles (ESP) both in carbonized (C) as well as uncarbonized (UC) form into the matrix of an Aluminum-Silicon (Al-Si) alloy to improve its mechanical properties. Various mechanical properties of the resulting composites such as tensile strength, modulus of elasticity, hardness, toughness, impact and compressive strengths have been determined and found to increase after the addition of the ESPs confirming that the incorporation of waste ESPs in the Al-Si matrix serve as reinforcements. The increase in mechanical properties such as the hardness (10.2% - UC, 19% - C), tensile (6.61% - UC, 10.61% - C), compressive (9.12% - UC, 63.94% - C) and impact strengths (30.07% - UC, 302.35% - C) is more pronounced in the case of carbonized ESPs. Field-Emission Scanning Electron Microscopy (FE-SEM) has been conducted to determine the compositions of the matrix materials as well as the composites.

scholarly journals The Influence of Heat Input on the Microstructure and Properties of Wire-Arc-Additive-Manufactured Al-Cu-Sn Alloy Deposits

Metals ◽  
2020 ◽  
Vol 10 (1) ◽  
pp. 79
Author(s):  
Shuai Wang ◽  
Huimin Gu ◽  
Wei Wang ◽  
Chengde Li ◽  
Lingling Ren ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Grain Boundary ◽  
Heat Input ◽  
Raw Material ◽  
Layer Height ◽  
Transmission Electron ◽  
The Matrix ◽  
Wire Arc Additive Manufacturing ◽  
Scanning Electron

In this experiment, Al-Cu-Sn alloy was used as raw material to form deposits with different heat input using the wire-arc additive manufacturing (WAAM) process. The effects of heat input on microstructure and mechanical properties of Al-Cu-Sn alloy deposits were investigated by metallography, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and transmission electron microscopy (TEM) and mechanical properties tests. The results show that with increased of heat input, the thickness of the deposits increased and the layer height of the deposits increased. The number and size of pores in the deposits also improved with the increased heat input. The grain size of the deposits in the as-deposited state gradually increased and changed from isometric crystals to columnar crystals, the precipitated θ phases gradually converged on the grain boundary from within the grains. After T6 heat treatment, with increased heat input, the number of unsolved θ phases on the grain boundary increased, and the number of θ phases precipitated out of the matrix decreased as the phase spacing increased. With the increased heat input, the mechanical properties of the deposits gradually decreased, and the fracture mode changed from ductile fracture to brittle fracture.

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